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24
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85153262280
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note
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Data sets were collected with an Enraf Nonius CAD4 diffractometer using an FR591 rotating anode generator. Programs used: data reduction MoIEN, structure solution SHELXS-86, structure refinement SHELXL-93, graphics DIAMOND.
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25
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85153281075
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note
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Crystallographic data (excluding structure factors) for the structures reported have been deposited with the Cambridge Crystallographic Data Centre. Copies of the data can be obtained free of charge by quoting the depository numbers CCDC-102622, -102623 and -102624, the names of the authors, and the journal citation on application to CCDC, 12 Union Road, Cambridge CB2 1EZ, UK [fax: int code + 44-12238 336-033, e-mail: deposit@ccdc.cam.ac.ukl.
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