Ansa-Ytterbocenes(+3) with a short bridge and bulky substituents: Synthesis and crystal structure of meso-(CH3)2Si[3-(CH3)3SiC 5H3]2YbCl(THF)

Journal of Organometallic Chemistry

Volumn 571, Issue 2, 1998, Pages 243-249

  Khvostov, Alexei V ^a   Belsky, Vitalii K ^b   Bulychev, Boris M ^a   Sizov, Alexandr I ^a   Ustinov, Boris B ^a  

^a MOSCOW STATE UNIVERSITY   (Russian Federation)

^b KARPOV INSTITUTE OF PHYSICAL CHEMISTRY   (Russian Federation)

Author keywords

Ansa Metallocenes; Crystal structure; Ytterbium

Indexed keywords

EID: 0005310383     PISSN: 0022328X     EISSN: None     Source Type: Journal    
DOI: 10.1016/S0022-328X(98)00822-5     Document Type: Article

References (59)

1. For example, see recent articles: (a) A. Vogel, T. Priermeier, W.A. Herrmann, J. Organomet. Chem. 527 (1997) 297.
2. (b) A.Z. Voskoboynikov, A.Yu. Agarkov, E.A. Chernyshev, I.P. Beletskaya, A.V. Churakov, L.G. Kuz'mina, J. Organomet. Chem. 530 (1997) 75.
3. (c) J.T. Park, B.W. Woo, S.C. Yoon, S.C. Shim, J. Organomet. Chem. 535 (1997) 29.
4. (d) S.C. Yoon, T.K. Han, B.W. Woo, H. Song, S.I. Woo, J.T. Park, J. Organomet. Chem. 534 (1997) 81.
5. (e) V. Varga, J. Hiller, R. Gyepes, M. Polášek, P. Sedmera, U. Thewalt, K. Mach, J. Organomet. Chem. 538 (1997) 63.
6. (f) Y. Obora, C.L. Stern, T.J. Marks, P.N. Nickias, Organometallics 16 (1997) 2503.
7. (g) K. Schmidt, A. Reinmuth, U. Rief, J. Diebold, H.H. Brintzinger, Organometallics 16 (1997) 1724.
8. (h) A. Steinhorst, G. Erker, M. Grehl, R. Fröhlich, J. Organomet. Chem. 542 (1997) 191.
9. (i) A.M. Barriola, A.M. Cano, T. Cuenca, F.J. Fernández, P. Gómez-Sal, A. Manzanero, P. Royo, J. Organomet. Chem. 542 (1997) 247.
10. (j) M.E. Huttenloch, B. Dorer, U. Rief, M.-H. Prosenc, K. Schmidt, H.H. Brintzinger, J. Organomet. Chem. 541 (1997) 219.
11. (k) J.R. Butchard, O.J. Curnow, S.J. Smail, J. Organomet. Chem. 541 (1997) 407.
12. Wiesenfeldt H., Reinmuth A., Barsties E., Evertz K., Brintzinger H.-H. J. Organomet. Chem. 369:1989;359.
13. I.E. Nifant'ev, P.V. Ivchenko, Organometallics 16 (1997) 713 and references therein.
14. Giardello M.A., Conticello V.P., Brard L., Sabat M., Rheingold A.L., Stern C.L., Marks T.J. J. Am. Chem. Soc. 116:1994;10212.
15. (a) G. Jeske, L.E. Schock, P.N. Swepston, H. Schumann, T.J. Marks, J. Am. Chem. Soc. 107 (1985) 8103.
16. (b) T. Akhnoukh, J. Müller, K. Qiao, X.-F. Li, R.D. Fischer, J. Organomet. Chem. 408 (1991) 47 and references therein.
17. (c) W.A. Herrmann, J. Eppinger, M. Spiegler, O. Runte, R. Anwander, Organometallics 16 (1997) 1813.
18. (d) M.A. Giardello, V.P. Conticello, L. Brard, M.R. Gagné, T.J. Marks, J. Am. Chem. Soc. 116 (1994) 10241.
19. Yasuda H., Ihara E. Macromol. Chem. Phys. 196:1995;2417.
20. (a) E.B. Coughlin, J.E. Bercaw, J. Am. Chem. Soc. 114 (1992) 7606.
21. (b) J.P. Mitchell, S. Hajela, S.K. Brookhart, K.I. Hardcastle, L.M. Henling, J.E. Bercaw, J. Am. Chem. Soc. 118 (1996) 1045.
22. (c) H. Yasuda, E. Ihara, Tetrahedron 51 (1995) 4563.
23. Ihara E., Nodono M., Yasuda H., Kanehisa N., Kai Y. Macromol. Chem. Phys. 197:1996;1909.
24. (a) J.N. John, M. Tsutsui, J. Coord. Chem. 10 (1980) 177.
25. (b) J.N. John, M. Tsutsui, Inorg. Chem. 20 (1981) 1602.
26. (c) C. Qian, C. Ye, H. Lu, Y. Li, Y. Huang, J. Organomet. Chem. 263 (1984) 333.
27. (d) S.J. Swamy, J. Loebel, H. Schumann, J. Organomet. Chem. 379 (1989) 51.
28. (e) C. Qian, G. Zou, L. Gao, J. Organomet. Chem. 525 (1996) 23 and references therein.
29. (a) P. Yan, N. Hu, Z. Jin, W. Chen, J. Organomet. Chem. 391 (1990) 313.
30. (b) F.T. Edelmann, M. Rieckhoff, I. Haiduc, I. Silaghi-Dumitrescu, J. Organomet. Chem. 447 (1993) 203.
31. I.E. Nifant'ev, P.V. Ivchenko, L.G. Kuz'mina, Y.N. Luzikov, A.A. Sitnikov, O.E. Sizan, Synthesis 4 (1997) 469 and references therein.
32. Taylor M.D., Carter P.C. J. Inorg. Nucl. Chem. 24:1962;387.
33. A.V. Khvostov, A.I. Sizov, B.M. Bulychev, S. Ya. Knjazhanski, V.K. Belsky, J. Organomet. Chem. 559 (1998) 97.
34. Streltsov V.A., Zavodnik V.E. Sov. Phys. Crystallogr. 34:1989;824.
35. G.M. Sheldrick, SHELXTL User Manual, Nicolet XRD Corp., USA, 1981.
36. G.M. Sheldrick, SHELXL-93 Program for Crystal Structure Refinement, University of Göttingen, Germany, 1993.
37. Khvostov A.V., Belsky V.K., Sizov A.I., Bulychev B.M., Ivchenko N.B. J. Organomet. Chem. 564:1998;5.
38. (a) H. Lueken, J. Schmitz, W. Lamberts, et al., Inorg. Chim. Acta 156 (1989) 119.
39. (b) E.C. Baker, L.D. Brown, K.N. Raymond, Inorg. Chem. 14 (1975) 1376.
40. (c) M.F. Lappert, A. Singh, J.L. Atwood, et al., J. Chem. Soc. Chem. Commun. (1981) 1190.
41. Höck N., Oroschin W., Paolucci G., Risher R.D. Angew. Chem. 98:1986;748.
42. Gun'ko Y.K., Hitchcock P.B., Lappert M.F. J. Organomet. Chem. 499:1995;213.
43. Lin Y.-H., Zeng D.-S., Shen O., Rare Earths. J. Chin. Soc. Rare Earths. 10:1992;170.
44. Belsky V.K., Sizov A.I., Bulychev B.M., Soloveichik G.L. Koord. Khim. 11:1985;1003.
45. (a) C. Eaborn, P.B. Hitchcock, K. Izod, J.D. Smith, J. Am. Chem. Soc. 116 (1994) 12071.
46. (b) P.B. Hitchcock, S.A. Holmes, M.F. Lappert, S. Tian, J. Chem. Soc. Chem. Commun. (1994) 2691.
47. Watson P.L., Whithey J.F., Harlow R.L. Inorg. Chem. 20:1981;3271.
48. Shen Q., Qi M., Guan J., Lin Y. J. Organomet. Chem. 406:1991;353.
49. H. Yasuda, H. Yamamoto, K. Yokota, A. Nakamura, Chem. Lett. (1989) 1309.
50. Tilley T.D., Andersen R.A., Spencer B., Ruben H., Zalkin A., Templeton D.H. Inorg. Chem. 19:1980;2999.
51. Qian C., Wang B., Deng D., Hu J., Chen J., Wu G., Zheng P. Inorg. Chem. 33:1994;3382.
52. Hitchcock P.B., Lappert M.F., Prashar S. J. Organomet. Chem. 413:1991;79.
53. E. Baraniak, R.St.L. Bruce, H.C. Freeman, N.J. Hair, J. James, Inorg. Chem. 15 (1976) 2226.
54. Evans W.J., Ulibarri T.A., Chamberlain L.R., Ziller J.W., Alvarez D. Organometallics. 9:1990;2124.
55. Deelman B.-J., Booij M., Meetsma A., Teuben J.H., Kooijman H., Spek A.L. Organometallics. 14:1995;2306.
56. Evans W.J., Boyle T.J., Ziller J.W. Organometallics. 12:1993;3998.
57. Deelman B.-J., Wierda F., Meetsma A., Teuben J.H. Appl. Organomet. Chem. 9:1995;483.
58. Evans W.J., Sollberger M.S., Shreeve J.L., Olofson J.M., Hain J.H., Ziller J.W. Inorg. Chem. 31:1992;2492.
59. Evans W.J., Dominguez R., Hanusa T.P. Organometallics. 5:1986;1291.