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0040451473
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note
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22: C, 34.94; H, 3.77; N, 3.88%
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18
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0039266776
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note
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2). The final R1 = 0.033 and wR = 0.078 for 4094 observed reflections (I > 2.00σ(I)).
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19
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0039858445
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note
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-1. Measurements were carried out on an Enraf-Nonius CAD4 diffractometer. The structure was solved by direct methods and refined by full-matrix least squares (on F). The atom O3 of the chelating nitrate is disordered over two sites having relative occupancies 0.60/0.40. The final R1 = 0.052 and Rw = 0.062 for 3340 observed reflections (1 > 3.00σ(I)).
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