Synthesis and spectroscopic data of para-substituted (3-phenyl-2H-azaphosphirene)tungsten complexes

European Journal of Inorganic Chemistry

Volumn , Issue 2, 1998, Pages 257-261

  Streubel, Rainer ^a   Ostrowski, Annette ^a   Priemer, Siegfried ^a   Rohde, Udo ^a   Jeske, Jörg ^a   Jones, Peter G ^a  

^a TECHNICAL UNIVERSITY OF BRAUNSCHWEIG   (Germany)

Author keywords

2H Azaphosphirene complexes; Cyclizations; Oarbene complexes; Phosphorus heterocycles; Tungsten

Indexed keywords

MASS SPECTROMETRY; TUNGSTEN COMPOUNDS;

2H-AZAPHOSPHIRENE COMPLEX; CYCLIZATIONS; HIGH YIELD SYNTHESIS; MULTISTEPS; OARBENE COMPLEX; PENTACARBONYL; PHOSPHORUS HETEROCYCLES; REARRANGEMENT REACTIONS; SPECTROSCOPIC DATA; TUNGSTEN COMPLEX;

SYNTHESIS (CHEMICAL);

EID: 0002658592     PISSN: 14341948     EISSN: None     Source Type: Journal    
DOI: 10.1002/(SICI)1099-0682(199802)1998:2<257::AID-EJIC257>3.0.CO;2-H     Document Type: Article

References (29)

1. H. Wilkens, J. Jeske, P. G. Jones, R. Streubel, J. Chem. Soc., Chem. Commun., in press.
2. A. Pawda, A. D. Woolhouse in A. R. Katritzky, C. W. Rees (Eds.) Comprehensive Heterocyclic Chemistry, vol. 7, Pergamon Press, Oxford, 1984, p. 47.
3. G. Bertrand, C. Wentrup, Angew. Chem. 1994, 106, 549-568; Angew. Chem Int. Ed. Engl. 1994, 33, 527-546.
4. G. Bertrand, C. Wentrup, Angew. Chem. 1994, 106, 549-568; Angew. Chem Int. Ed. Engl. 1994, 33, 527-546.
5. R. M. Paton, Chem. Soc. Rev. 1989, 18, 33-52.
6. [5a] S. Fischer, C. Wentrup, J. Chem. Soc., Chem. Commun. 1980, 502-503.
7. [5b] R. A. Moss, J. Terpinski, D. P. Cox, D. Z. Denney, K. J. Krogh-Jespersen, J. Am. Chem. Soc. 1985, 107, 2743-2748.
8. N. Dubau-Assibat, A. Baceiredo, G. Bertrand, J. Am. Chem. Soc. 1996, 118, 5216-5220.
9. [7a] A. Holm, N. Harrit, I. Trabjerg, J. Chem. Soc., Perkin Trans. I 1978, 746-750.
10. [7b] A. Holm, J. J. Christiansen, C. Lohse, J. Chem. Soc. Perkin Trans 1 1979. 1, 960-962.
11. G. Alcaraz, V. Piquet, A. Baceiredo, F. Dahan, W. W. Schoeller, G. Bertrand, J. Am. Chem. Soc. 1996, 118, 1060-1065.
12. [9a] A. E. Reed. P. v. R. Schleyer, J. Am. Chem. Soc. 1990, 112, 1434-1445.
13. [9b] D. G. Gilheany, Chem Rev 1994, 94, 1339-1374.
14. W. A. Lathan, L. Radom, P. C. Hariharan, W. J. Hehre, J. A. Pople, Top. Curr. Chem. 1973, 40, 1-45.
15. [11a] M. Rahmoune, Y. Y. C. Yeung Lam Ko, F. Tonnard, R. Carrie, PSI-BLOCS Conference, Palaiseau, France, 1988, poster abstract.
16. [11b] M. Rahmoune, Y. Y. C. Yeung Lam Ko, R. Carrie, F. Tonnard. New J. Chem. 1989, 13, 891-898; comment: This paper neither describes nor mentions non-coordinated 2H-azaphosphirenes.
17. R. Streubel, J. Jeske, P. G. Jones, R. Herbst-Irmer, Angew. Chem 1994, 106, 115-117; Angew. Chem. Int. Ed. Engl. 1994, 33, 80-82.
18. R. Streubel, J. Jeske, P. G. Jones, R. Herbst-Irmer, Angew. Chem 1994, 106, 115-117; Angew. Chem. Int. Ed. Engl. 1994, 33, 80-82.
19. R. Streubel, H. Wilkens, A. Ostrowski, C. Neumann, F. Ruthe, P. G. Jones, Angew. Chem. 1997, 109, 1549-1550; Angew. Chem. Int. Ed. Eng. 1997, 36, 1492-1493.
20. R. Streubel, H. Wilkens, A. Ostrowski, C. Neumann, F. Ruthe, P. G. Jones, Angew. Chem. 1997, 109, 1549-1550; Angew. Chem. Int. Ed. Eng. 1997, 36, 1492-1493.
21. G. M. Bodner, S. B. Kahl, K. Bork, B. N. Storhoff, J. E. Wuller, L. J. Todd, Inorg. Chem 1973, 12, 1071-1074.
22. R. Appel, A. Westerhaus, Tetrahedron Lett. 1981, 22, 2159-2160.
23. R. Streubel, unpublished results
24. C. Hansch, A. Leo, S. H. Unger, K. H. Kim, D. Nikaitani, E. J. Lien. J. Med. Chem 1973, 16, 1207-1216.
25. Crystallographic data (excluding structure factors) for the structure reported in this paper have been deposited with the Cambridge Crystallographic Data Centre as supplementary publication no. CCDC-100687. Copies of the data can be obtained free of charge on application to The Director, CCDC, 12 Union Road, UK-Cambridge CB2 1EZ [fax: int. code + 44(1223)336-033; E-mail: deposit@chemcrys.cam.ac.uk].
26. R. Streubel, A. Ostrowski, H. Wilkens, F. Ruthe, J. Jeske, P. G. Jones, Angew. Chem. 1997, 109, 409-413; Angew. Chem. Int. Ed. Engl. 1997, 36, 378-381.
27. R. Streubel, A. Ostrowski, H. Wilkens, F. Ruthe, J. Jeske, P. G. Jones, Angew. Chem. 1997, 109, 409-413; Angew. Chem. Int. Ed. Engl. 1997, 36, 378-381.
28. [20a] E. O. Fischer H. J. Kollmeier, Chem. Ber. 1971, 104, 1339-1346.
29. [20b] E. O. Fischer, M. Leupold, Chem. Ber. 1972, 105, 599-608.