A 3-D Organically Templated Mixed Valence (Fe2+/Fe3+) Iron Phosphate with Oxide-Centered Fe4O(PO4)4 Cubes: Hydrothermal Synthesis, Crystal Structure, Magnetic Susceptibility, and Mössbauer Spectroscopy of [H3NCH2CH2NH3]2[Fe 4O(PO4)4]·H2O

Chemistry of Materials

Volumn 9, Issue 9, 1997, Pages 1994-1998

  DeBord, Jeffrey R D ^a   Reiff, William M ^b   Warren, Christopher J ^a,d   Haushalter, Robert C ^a,d   Zubieta, Jon ^c  

^a NEC LABORATORIES AMERICA   (United States)

^b NORTHEASTERN UNIVERSITY   (United States)

^c SYRACUSE UNIVERSITY   (United States)

^d SYMYX TECHNOLOGIES   (United States)

Author keywords

[No Author keywords available]

Indexed keywords

EID: 0001710895     PISSN: 08974756     EISSN: None     Source Type: Journal    
DOI: 10.1021/cm970125b     Document Type: Article

References (63)

1. Haushalter, R.; Mundi, L. Chem. Mater. 1992, 4, 31.
2. (a) Soghomonian, V.; Chen, Q.; Haushalter, R; Zubieta, J. Chem. Mater. 1993, 5, 1690.
3. (b) Haushalter, R.; Wang, Z.; Thompson, M.; Zubieta, J.; O'Connor, C. Inorg. Chem. 1993, 32, 3966.
4. (c) Soghomonian, V.; Chen, Q.; Haushalter, R.; Zubieta, J.; O'Connor, C. Science 1993, 259, 1596.
5. (d) Soghomonian, V.; Chen, Q.; Haushalter, R.; Zubieta, J. Chem. Mater. 1993, 5, 1595.
6. (e) Soghomonian, V.; Chen, Q.; Haushalter, R.; Zubieta, J. Angew. Chem., Int. Ed. Engl. 1993, 32, 610.
7. (f) Haushalter, R.; Chen, Q.; Soghomonian, V.; Zubieta, J.; O'Connor, C. J. Solid State Chem. 1994, 108, 128.
8. (g) Soghomonian, V.; Haushalter, R.; Zubieta, J. Inorg. Chem. 1994, 33, 3, 1700.
9. (h) Zhang, Y.; Clearfield, A.; Haushalter, R. J. Solid State Chem. 1994, 117, 157.
10. (i) Zhang, Y.; Clearfield, A.; Haushalter, R. Chem. Mater. 1995, 7, 1221.
11. (j) Soghomonian, V.; Chen, Q.; Haushalter, R.; O'Connor, C.; Tao, C.; Zubieta, J. Inog. Chem. 1995, 34, 3509.
12. (k) Khan, M.; Meyer, L.; Haushalter, R.; Zubieta, J.; Dye, J. Chem. Mater. 1996, 8, 43.
13. (l) Soghomonian, V.; Haushalter, R.; Zubieta, J.; O'Connor, C. Inorg. Chem. 1996, 35, 2826.
14. (m) Johnson, J. W.; Jacobson, A. J. Angew. Chem., Int. Ed. Engl. 1985, 22, 412.
15. (n) Huan, G.; Jacobson, A. J.; Johnson, J. W.; Corcdan, E. W. Chem. Mater. 1990, 2, 91.
16. (o) Riou, D.; Ferey, G. Eur. J. Solid State Inorg. Chem. 1994, 31, 25.
17. (a) Kahn, M.; Lee, Y.; O'Connor, C.; Haushalter, R.; Zubieta, J. J. Am. Chem. Soc. 1994, 116, 4525.
18. (b) Khan, M.; Lee, Y.; O'Connor, C.; Haushalter, R.; Zubieta, J. Inorg. Chem. 1994, 33, 3855.
19. (c) Soghomonian, V.; Diaz, R.; Haushalter, R.; O'Connor, C.; Zubieta, J. Inorg. Chem. 1995, 34, 4460.
20. (d) Soghomonian, V.; Haushalter, R.; Zubieta, J. Chem. Mater. 1995, 7, 1648.
21. (e) Soghomonian, V.; Chen, Q.; Haushalter, R.; Zubieta, J. Angew. Chem., Int. Ed. Engl. 1995, 34, 223.
22. (f) Bonavia, G.; Haushalter, R.; O'Connor, C.; Zubieta, J. Inorg. Chem. 1996, 35, 5603.
23. Zapf, P.; Rose, D.; Haushalter, R.; Zubieta, J. J. Solid State Chem. 1996, 125, 182.
24. (a) DeBord, J.; Haushalter, R.; Zubieta, J. J. Solid State Chem. 1996, 125, 270.
25. (b) Chen, J.; Jones, R.; Natarajan, S.; Hursthouse, M.; Thomas, M. Angew. Chem., Int. Ed. Engl. 1994, 33, 639.
26. Dhingra, S.; Haushalter, R. J. Chem. Soc., Chem. Commun. 1993, 21, 1665.
27. (a) Zhang, Y.; O'Connor, C.; Clearfield, A.; Haushalter, R. Chem. Mater. 1996, 8, 595.
28. (b) Zhang, Y.; DeBord, J.; O'Connor, C.; Haushalter, R.; Clearfield, A.; Zubieta, J. Angew. Chem., Int. Ed. Engl. 1996, 35, 989.
29. (c) DeBord, J.; Zhang, Y.; Haushalter, R.; Zubieta, J.; O'Connor, C. J. Solid State Chem. 1996, 122, 251.
30. (d) Zhang, Y.; Haushalter, R.; Clearfield, A. J. Chem. Soc., Chem. Commun. 1996, 9, 1055.
31. (e) Zhang, Y.; Haushalter, R.; Clearfield, A. Inorg. Chem. 1996, 35, 4950.
32. (f) Whittingham, M. S.; Guo, J. D.; Chen, R.; Chirayil, Th.; Janauer, G.; Zavalij, P. Solid State Ionics, 1995, 75, 257.
33. (g) Duan, C. Y.; Tiang, Y. P.; Lu, Z. L.; You, Y. Z. Inorg. Chem. 1995, 34, 1.
34. (h) Riou, D.; Ferey, G. Inorg. Chem. 1995, 34, 6520.
35. (i) Pecharsky, V. P.; Jacobson, R. A. Z. Kristallogr. 1996, 211.
36. (j) Nazar, L. F.; Koene, B. E.; Britten, J. F. Chem. Mater. 1996, 8, 327.
37. (a) Cavellec, M.; Riou, D.; Ferey, G. Acta Crtstallogr. 1995, C51, 2242.
38. (b) DeBord, J.; Reiff, W.; Haushalter, R.; Zubieta, J. J. Solid State Chem. 1996, 125, 186.
39. (a) Moore, P.; Kampf, A. Z. Kristallogr. 1992, 201, 263.
40. (b) Moore, P. Am. Miner. 1972, 57, 397.
41. (c) Moore, P. Am. Miner. 1970, 55, 135.
42. (d) Moore, P.; Araki, T. Inorg. Chem. 1976, 15, 316.
43. (e) Moore, P. The 2nd International Congress on Phosphorus Compounds Proceedings, April 21-25, 1980; p 105.
44. (f) Moore, P.; Shen, J. Nature 1983, 306, 356.
45. (a) Lii, K.; Huang, C. J. Chem. Soc., Dalton Trans. 1995, 571.
46. (b) Gabelica-Robert, M.; Goreaud, M.; Labbe, Ph.; Raveau, B. J. Solid State Chem. 1982, 45, 389.
47. (c) Pintard-Screpel, M.; D'Yvoire, F.; Durand, J. Acta Crystallogr. 1983, C39, 9.
48. (d) Riou, D.; Labbe, Ph.; Goreaud, M. Eur. J. Solid State Inorg. Chem. 1988, 25, 215.
49. (e) Reiff, W.; Torardi, C. Hyperfine Interact. 1990, 53, 403.
50. (a) Cavellec, M.; Riou, D.; Ninclaus, C.; Greneche, J.; Ferey, G. Zeolites 1996, 17, 250.
51. (b) Cavellec, M.; Riou, D.; Greneche, J. M.; Ferey, G. J. Magn. Mater. 1996, 163, 173.
52. (c) Cavellec, M.; Riou, D.; Greneche, J. M.; Ferey, G. Microporous Mater. 1997, 8, 3.
53. (a) Estermann, M.; McCusker, L. B.; Merrouche, A.; Kessler, H. Nature 1991, 352, 320.
54. (b) Linde, A.; Simmen, A.; Patrin, J.; Baerlocher, C. Proceedings of the 9th International Zeolite Conference, Montreal; Von Balmoos, R., et al., Eds.; 1992; p 433.
55. (c) Loiseau, T.; Ferey, G. J. Solid State Chem. 1994, 111, 403.
56. Chang, C.; Reiff, W. Inorg. Chem. 1977, 16, 2097.
57. Bancroft, G.; Maddock, A.; Ong, W.; Prince, R.; Stone, A. J. Chem. Soc. A 1967, 1966.
58. Walker, N.; Stuart, D. Acta Crystallogr. 1983, A39, 158.
59. teXsan Single-Crystal Structure Analysis Software Package, Version 1.7-1; Molecular Structure Corporation: The Woodlands, TX, 1995.
60. Brown, I. Structure and Bonding in Crystals; O'Keeffe, M., Navrotsky, A., Eds.; Academic Press: New York, 1981; Vol. II.
61. Greenwood, N.; Gibb, T. Mössbauer Spectroscopy; Chapman and Hall: London, 1982.
62. Reiff, W.; Kwiecien, M.; Jakeman, R.; Cheetham, A.; Torardi, C. J. Solid State Chem. 1993, 107, 401.
63. Cullity, B. Introduction to Magnetic Materials; Addison-Wesley: Reading, MA, 1972.