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Volumn 8, Issue 3, 1996, Pages 595-597

An organically templated layered vanadium oxide: Hydrothermal synthesis, single-crystal structure, and magnetic properties of (H3N(CH2)3NH3)[V4O 10]

Author keywords

[No Author keywords available]

Indexed keywords


EID: 0000295348     PISSN: 08974756     EISSN: None     Source Type: Journal    
DOI: 10.1021/cm9503846     Document Type: Article
Times cited : (110)

References (28)
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    • note
    • 2O (10 mL) in a molar ratio of 1:12.3: 1.5:341 heated in a 23-mL acid digestion bomb at 170°C for 66 h gave 0.20 g black plates of 1.
  • 22
    • 2842582552 scopus 로고    scopus 로고
    • note
    • 3, and Z = 4. Data were collected on an AFC7R diffractometer with Mo Ka radiation (λ = 0.7106 Å) and a 18 kW rotating anode generator at room temperature. Structure solution and refinement by full-matrix least-squares using teXsan program package based on 1977 reflections with I ≥ 3σ(1) and 172 variables gave R(Rw) = 0.040 (0.043). All of the non-hydrogen atoms were refined anisotropically All of the hydrogen atoms were located from difference Fourier maps and included in the refinement with fixed positional and thermal parameters.


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