Dynamic and magnetic susceptibility effects on the MAS NMR linewidth of a tetrapeptide bound to different resins

Magnetic Resonance in Chemistry

Volumn 40, Issue 2, 2002, Pages 123-132

  Furrer, Julien ^a   Elbayed, Karim ^a   Bourdonneau, Maryse ^b   Raya, Jésus ^a   Limal, David ^c   Bianco, Alberto ^d   Piotto, Martial ^b  

^a UNIVERSITÉ LOUIS PASTEUR   (France)

^b CNRS   (France)

^c Ecole Nationale Superieure de Chimie de Mulhouse   (France)

^d INSTITUT DE BIOLOGIE MOLÉCULAIRE ET CELLULAIRE   (France)

Author keywords

13C NMR; 1H NMR; High resolution magic angle spinning; Magnetic susceptibility; NMR; Relaxation; Solid phase peptide synthesis

Indexed keywords

LINEWIDTH; MAGIC ANGLE SPINNING; MAGNETIC SUSCEPTIBILITY; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY; PEPTIDES; SYNTHESIS (CHEMICAL);

13C NMR; 1H NMR; CLASSICAL LIQUIDS; HIGH RESOLUTION MAGIC ANGLE SPINNING; MAGIC-ANGLE SPINNING; MAS NMR; NMR SPECTRUM; RELAXATION; SOLID PHASE PEPTIDE SYNTHESIS; TETRA PEPTIDE;

RESINS;

ALANYLISOLEUCYLGLYCYLMETHIONINE; N,N DIMETHYLFORMAMIDE; RESIN; TETRAPEPTIDE; UNCLASSIFIED DRUG;

ARTICLE; CHEMICAL BOND; LIQUID; MAGIC ANGLE SPINNING NUCLEAR MAGNETIC RESONACE SPECTROSCOPY; MAGNETISM; MOLECULAR DYNAMICS; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY; PEPTIDE SYNTHESIS;

EID: 0001661685     PISSN: 07491581     EISSN: None     Source Type: Journal    
DOI: 10.1002/mrc.970     Document Type: Article

References (41)

1. Andrew ER, Bradbury A, Eades RG. Nature (London) 1958; 182: 1659.
2. Lowe IJ. Phys. Rev. Lett. 1959; 2: 285.
3. Lippens G, Bourdonneau M, Dhalluin C, Warras R, Richert T, Seetharaman C, Boutillon C, Piotto M. Curr. Org. Chem. 1999; 3: 147.
4. Filtch WL, Dettre G, Holmes CP, Shoolery J, Keifer PA. J. Org. Chem. 1994; 59: 7955.
5. Anderson RC, Jarema MA, Shapiro MJ, Stokes JP, Zilliox M. J. Org. Chem. 1995; 60: 2650.
6. Anderson RC, Stokes JP, Shapiro MJ. Tetrahedron Lett. 1995; 36: 5311.
7. Keifer PA. J. Org. Chem. 1996; 61: 1558.
8. Pop IE, Dhalluin CF, Déprez BP, Melnyk PC, Lippens G. Tetrahedron 1996; 52: 12209.
9. Dhalluin C, Boutillon C, Tartar A, Lippens G. J. Am. Chem. Soc. 1997; 119: 10494.
10. Jelinek R, Valente AP, Valentine KG, Opella SJ. J. Magn. Reson. 1997; 125: 185-187.
11. Shapiro MJ, Chin J, Marti RE, Jarosinski M. Tetrahedron Lett. 1997; 38: 1333-1336.
12. Furrer J, Piotto M, Bourdonneau M, Guichard G, Limal D, Elbayed K, Raya J, Briand JP, Bianco A. J. Am. Chem. Soc. 2001; 123: 4130.
13. Garroway AN. J. Magn. Reson. 1982; 49: 168.
14. Doskocilova D, Duc Tao D, Schneider B. Czech. J. Phys. B 1975; 25: 202.
15. Gross JD, Costa PR, Dubacq JP, Warschawski DE, Lirsac PN, Devaux PF, Griffin RG. J. Magn. Reson. 1995; 106: 187.
16. Moka D, Vorreuter R, Schicha H, Spraul M, Humpfer E, Lipinsky M, Foxall PJD, Nicholson JK, Lindon JC. Anal. Commun. 1997; 34: 107.
17. Chang LL, Lean CL, Bogdanova A, Wright SC. Magn. Reson. Med. 1996; 36: 653.
18. Elbayed K, Bourdonneau M, Furrer J, Richert T, Raya J, Hirschinger J, Piotto M. J. Magn. Reson. 1999; 136: 127.
19. Meldal M. Tetrahedron Lett. 1992; 33: 3077.
20. Renil M, Meldal M. Tetrahedron Lett. 1996; 37: 6185.
21. Schmidt-Rohr K, Spiess HW. Multidimensional Solid-state NMR and Polymers. Academic Press: London, 1999.
22. Carr HY, Purcell EM. Phys. Rev. 1954; 94: 630.
23. Meiboom S, Gill D. Rev. Sci. Instrum. 1958; 29: 688.
24. Vanderhart DL, Earl WL, Garroway AN. J. Magn. Reson. 1981; 44: 361.
25. Earl WL, Vanderhart DL. J. Magn. Reson. 1982; 48: 35.
26. Leu G, Tang XW, Peled S, Maas W, Singer S, Cory DG, Sen PN. Chem. Phys. Lett. 2000; 332: 344.
27. Andrew ER. In Encyclopedia of Nuclear Magnetic Resonance, Grant DM, Harris RK (eds). Wiley: New York, 1996; 2891-2901.
28. de Swiet TM, Tomaselli M, Hürlimann MD, Pines A. J. Magn. Reson. 1998; 133: 385.
29. Vanderhart DL. In Encyclopedia of Nuclear Magnetic Resonance, Grant DM, Harris RK (eds). Wiley: New York, 1996; 2938.
30. Goldman M. Quantum Description of High-Resolution NMR in Liquids. Clarendon Press: Oxford, 1988.
31. Jeener J, Meier BH, Bachman P, Ernst RR. J. Chem. Phys. 1979; 71: 4546.
32. Kay L, Torchia DA, Bax A. Biochemistry 1989; 28: 8972.
33. Aue WP, Karhan J, Ernst RR. J. Chem. Phys. 1976; 64: 4266.
34. Grøtli M, Gotfresden CH, Rademann J, Buchardt J, Clark AJ, Duus JØ, Meldal M. J. Comb. Chem. 2000; 2: 108.
35. Bianco A, Furrer J, Limal D, Guichard G, Elbayed K, Raya J, Piotto M, Briand JP. J. Comb. Chem. 2000; 6: 681.
36. IUPAC-IUB Commission of Nomenclature. J. Biol. Chem. 1972; 247: 977.
37. Braunschweiler L, Ernst RR. J. Magn. Reson. 1983; 53: 521.
38. Bax A, Davis DG. J. Magn. Reson. 1985; 65: 355.
39. Piotto M, Bourdonneau M, Furrer J, Bianco A, Raya J, Elbayed K. J. Magn. Reson. 2001; 149: 114.
40. Shaka AJ, Keeler J, Frenkiel T, Freeman R. J. Magn. Reson. 1983; 52: 335.
41. Marion D, Ikura M, Tschudin R, Bax A. J. Magn. Reson. 1989; 85: 393.