Fluorinated Bis(enyl) Ligands by Metal-Induced Dimerization of Fluorinated Allenes

Angewandte Chemie - International Edition

Volumn 40, Issue 11, 2001, Pages 2087-2091

  Lentz, Dieter ^a   Willemsen, Stefan ^a  

^a FREIE UNIVERSITÄT BERLIN   (Germany)

Author keywords

[No Author keywords available]

Indexed keywords

EID: 0001426001     PISSN: 14337851     EISSN: None     Source Type: Journal    
DOI: 10.1002/1521-3773(20010601)40:11<2087::AID-ANIE2087>3.0.CO;2-8     Document Type: Article

References (32)

1. C. Elschenhroich, A. Salzer, Organometallichemie, Teubner, Stuttgart, 1986; C. Elschenbroich, A. Salzer, Organometallics, 2nd ed., VCH, weinheim, 1992; J. P. Collman, L. S. Hegedus, J. R. Norton, R. G. Finke, Principles and Applications of Organotransition Metal Chemistry, University Science Books. Mill Valley, CA, 1987.
2. C. Elschenhroich, A. Salzer, Organometallichemie, Teubner, Stuttgart, 1986; C. Elschenbroich, A. Salzer, Organometallics, 2nd ed., VCH, weinheim, 1992; J. P. Collman, L. S. Hegedus, J. R. Norton, R. G. Finke, Principles and Applications of Organotransition Metal Chemistry, University Science Books. Mill Valley, CA, 1987.
3. C. Elschenhroich, A. Salzer, Organometallichemie, Teubner, Stuttgart, 1986; C. Elschenbroich, A. Salzer, Organometallics, 2nd ed., VCH, weinheim, 1992; J. P. Collman, L. S. Hegedus, J. R. Norton, R. G. Finke, Principles and Applications of Organotransition Metal Chemistry, University Science Books. Mill Valley, CA, 1987.
4. G. Paprott, S. Lehmann, K. Seppelt, Chem. Ber. 1988, 121, 727; G. Paprott, K. Seppelt, J. Am. Chem. Soc. 1984, 106, 4060.
5. G. Paprott, S. Lehmann, K. Seppelt, Chem. Ber. 1988, 121, 727; G. Paprott, K. Seppelt, J. Am. Chem. Soc. 1984, 106, 4060.
6. O. J. Curnow, R. P. Hughes, J. Am. Chem. Soc. 1992, 114, 5895.
7. T. G. Richmond, Angew. Chem. 2000, 112, 3378; Angew. Chem. Int. Ed. 2000, 39, 3241; J. Burdeniuc, B. Jedlicka, R. H. Crabtree, Chem. Ber. 1997, 130, 145; J. L. Kiplinger, T. G. Richmond, C. E. Osterberg, Chem. Rev. 1994, 94, 373.
8. T. G. Richmond, Angew. Chem. 2000, 112, 3378; Angew. Chem. Int. Ed. 2000, 39, 3241; J. Burdeniuc, B. Jedlicka, R. H. Crabtree, Chem. Ber. 1997, 130, 145; J. L. Kiplinger, T. G. Richmond, C. E. Osterberg, Chem. Rev. 1994, 94, 373.
9. T. G. Richmond, Angew. Chem. 2000, 112, 3378; Angew. Chem. Int. Ed. 2000, 39, 3241; J. Burdeniuc, B. Jedlicka, R. H. Crabtree, Chem. Ber. 1997, 130, 145; J. L. Kiplinger, T. G. Richmond, C. E. Osterberg, Chem. Rev. 1994, 94, 373.
10. T. G. Richmond, Angew. Chem. 2000, 112, 3378; Angew. Chem. Int. Ed. 2000, 39, 3241; J. Burdeniuc, B. Jedlicka, R. H. Crabtree, Chem. Ber. 1997, 130, 145; J. L. Kiplinger, T. G. Richmond, C. E. Osterberg, Chem. Rev. 1994, 94, 373.
11. D. Lentz, S. Willemsen, Organometallics 1999, 18, 3962.
12. G. Frenking, N. Fröhlich, Chem. Rev. 2000, 100, 717.
13. C. G. Kreiter, M. L. Leyendecker, W. S. Sheldrick, J. Organomet. Chem. 1986, 302, 35.
14. J. Sóvágó, M. G. Newton, E. A. Mushina, F. Ungváry, J. Am. Chem. Soc. 1996, 118, 9589.
15. W. W. Schmiegel, ACS Monogr. 1995, 187, 1101 - 1118, and references therein; B. Ameduri, B. Boutevin, J. Fluorine Chem. 2000, 104, 53; Modern Fluoropolymers (Ed.: J. Scheirs), Wiley, New York, 1997; G. Hougham, K. Johns, P. E. Cassidy, T. Davidson, Fluorapolymers: Synthesis and Properties, Plenum, New York. 1999.
16. W. W. Schmiegel, ACS Monogr. 1995, 187, 1101 - 1118, and references therein; B. Ameduri, B. Boutevin, J. Fluorine Chem. 2000, 104, 53; Modern Fluoropolymers (Ed.: J. Scheirs), Wiley, New York, 1997; G. Hougham, K. Johns, P. E. Cassidy, T. Davidson, Fluorapolymers: Synthesis and Properties, Plenum, New York. 1999.
17. W. W. Schmiegel, ACS Monogr. 1995, 187, 1101 - 1118, and references therein; B. Ameduri, B. Boutevin, J. Fluorine Chem. 2000, 104, 53; Modern Fluoropolymers (Ed.: J. Scheirs), Wiley, New York, 1997; G. Hougham, K. Johns, P. E. Cassidy, T. Davidson, Fluorapolymers: Synthesis and Properties, Plenum, New York. 1999.
18. W. W. Schmiegel, ACS Monogr. 1995, 187, 1101 - 1118, and references therein; B. Ameduri, B. Boutevin, J. Fluorine Chem. 2000, 104, 53; Modern Fluoropolymers (Ed.: J. Scheirs), Wiley, New York, 1997; G. Hougham, K. Johns, P. E. Cassidy, T. Davidson, Fluorapolymers: Synthesis and Properties, Plenum, New York. 1999.
19. B. E. Smart, ACS Monogr. 1995, 187, 979-1010, and references therein.
20. T. L. Jacobs, R. S. Bauer, J. Am. Chem. Soc. 1959, 81, 606.
21. 2) = 0.0657 (all data), 361 parameters, anisotropic thermal parameters. 5: triclinic, P1 a = 6.1860(6),
22. 2) = 0.0785 (all data), 153 parameters, anisotropic thermal parameters, H-atoms isotropic. Crystallographic data (excluding structure factors) for the structures reported in this paper have been deposited with the Cambridge Crystallographic Data Centre as supplementary publication nos. CCDC-156869-CCDC-156874. Copies of the data can be obtained free of charge on application to CCDC, 12 Union Road, Cambridge CB2 1EZ, UK (fax: (+44) 1223-336-033; e-mail: deposit@ ccdc.cam.ac.uk).
23. P. W. Sutton, L. F. Dahl., J. Am. Chem. Soc. 1967, 89, 261; K. Bartl, R. Boese, G. Schmid, J. Organomet. Chem. 1981, 206, 331; D. Seyferth, Adv. Organomet. Chem. 1976, 14, 98; K. D. W. Kemmitt, D. K., Russell in Comprehensive Organometallic Chemistry, Vol. 5 (Eds.; G. Wilkinson, F. G. A. Stone, E. W. Abel), Pergamon, Oxford, 1982, pp. 162- 177.
24. P. W. Sutton, L. F. Dahl., J. Am. Chem. Soc. 1967, 89, 261; K. Bartl, R. Boese, G. Schmid, J. Organomet. Chem. 1981, 206, 331; D. Seyferth, Adv. Organomet. Chem. 1976, 14, 98; K. D. W. Kemmitt, D. K., Russell in Comprehensive Organometallic Chemistry, Vol. 5 (Eds.; G. Wilkinson, F. G. A. Stone, E. W. Abel), Pergamon, Oxford, 1982, pp. 162- 177.
25. P. W. Sutton, L. F. Dahl., J. Am. Chem. Soc. 1967, 89, 261; K. Bartl, R. Boese, G. Schmid, J. Organomet. Chem. 1981, 206, 331; D. Seyferth, Adv. Organomet. Chem. 1976, 14, 98; K. D. W. Kemmitt, D. K., Russell in Comprehensive Organometallic Chemistry, Vol. 5 (Eds.; G. Wilkinson, F. G. A. Stone, E. W. Abel), Pergamon, Oxford, 1982, pp. 162- 177.
26. P. W. Sutton, L. F. Dahl., J. Am. Chem. Soc. 1967, 89, 261; K. Bartl, R. Boese, G. Schmid, J. Organomet. Chem. 1981, 206, 331; D. Seyferth, Adv. Organomet. Chem. 1976, 14, 98; K. D. W. Kemmitt, D. K., Russell in Comprehensive Organometallic Chemistry, Vol. 5 (Eds.; G. Wilkinson, F. G. A. Stone, E. W. Abel), Pergamon, Oxford, 1982, pp. 162-177.
27. G. M. Sheldrick, SHELX97 Programs for Crystal Structure Analysis (Release 97-2), Institut für Anorganische Chemie der Universität Göttingen, Germany, 1998.
28. A. C. T. North, D. C. Phillips, F. S. Mathews. Acta Crystallogr. Sect. A 1968, 24, 351. PLATON/PLUTON: a) A. L. Spek. Acta Crystallogr. Sect. A 1990, 46, C34; b) A. L. Spek, PLATON, A Multipurpose Crystallographic Tool, Utrecht University, Utrecht, The Netherlands, 1998.
29. A. C. T. North, D. C. Phillips, F. S. Mathews. Acta Crystallogr. Sect. A 1968, 24, 351. PLATON/PLUTON: a) A. L. Spek. Acta Crystallogr. Sect. A 1990, 46, C34; b) A. L. Spek, PLATON, A Multipurpose Crystallographic Tool, Utrecht University, Utrecht, The Netherlands, 1998.
30. A. C. T. North, D. C. Phillips, F. S. Mathews. Acta Crystallogr. Sect. A 1968, 24, 351. PLATON/PLUTON: a) A. L. Spek. Acta Crystallogr. Sect. A 1990, 46, C34; b) A. L. Spek, PLATON, A Multipurpose Crystallographic Tool, Utrecht University, Utrecht, The Netherlands, 1998.
31. R. H. Blessing, Acta Crystallogr. Sect. A 1995, 51, 33; SADABS, Bruker AXS, 1998.
32. ORTEP3 for Windows; L. J. Farrugia, J. Appl. Crystallogr. 1997, 30, 565.