The First Fused Dimer Metallacrown Ni2II(mcpa)2(CH3OH) 3(H2O)[12-MCNiIIN(shi)2(pko)2-4][12-MC NiIIN(shi)3(pko)-4]

Inorganic Chemistry

Volumn 37, Issue 26, 1998, Pages 6556-6557

  Psomas, George ^a   Dendrinou Samara, Catherine ^a   Alexiou, Maria ^a   Tsohos, Alexandros ^b   Raptopoulou, Catherine P ^b   Terzis, Aris ^b   Kessissoglou, Dimitris P ^a  

^a ARISTOTLE UNIVERSITY OF THESSALONIKI   (Greece)

^b INSTITUTE OF NANOSCIENCE AND NANOTECHNOLOGY   (Greece)

Author keywords

[No Author keywords available]

Indexed keywords

EID: 0001301919     PISSN: 00201669     EISSN: None     Source Type: Journal    
DOI: 10.1021/ic980614t     Document Type: Article

References (26)

1. Pedersen, C. J. J. Am. Chem. Soc. 1967, 89, 7017.
2. Lehn, J.-M. Acc. Chem. Res. 1978, 11, 49.
3. Dietrich, B.; Viout, P.; Lehn, J.-M. Macrocyclic Chemistry: Aspects of Organic and Inorganic Supramolecular Chemistry; VCH: New York, 1993.
4. Nakatsuji, Y.; Nakamura, T.; Okahara, M. Chem. Lett. 1982, 1207.
5. Gray, G. M. Comments Inorg. Chem. 1995, 17, 95.
6. Constable, E. C. Progress in Inorganic Chemistry; K. D. Karlin, K. D., Ed.; John Wiley & Sons, Inc.: New York, 1994: Vol. 42, pp 67-137.
7. Barrow, H.; Brown, D.A.; Alcock, N. W.; Clase, H. J.; Wallbridge, M. G. H. J. Chem. Soc. Chem. Commun. 1995, 1231.
8. Chandler, C. D.; Roger, C.; Hampden-Smith, M. J. Chem. Rev. 1993, 93, 1205.
9. Bradley, D. C. Chem. Rev. 1989, 89, 1317.
10. Caneschi, A.; Cornia, A.; Lippard, S. J. Angew. Chem., Int. Ed. Engl. 1995, 34, 467.
11. Creaser, I.; Heckel, M. C.; Neitz, R. J.; Pope, M. T. Inorg. Chem. 1993, 32, 1573.
12. Fischer, J.; Ricard, L.; Weiss, R. J. Am. Chem. Soc. 1976, 98, 3050.
13. Pecoraro, V. L.; Stemmler, A. J.; Gibney, B. R.; Bodwin, J. J.; Wang, H.; Kampf, J. W.; Barwinski, A. Progress in Inorganic Chemistry, Karlin, K. D., Eds.;); John Wiley & Sons, Inc.; New York. Vol. 45, 1997; pp 83-177.
14. Stemmler, A. J.; Kampf, J. W.; Pecoraro, V. L. Inorg. Chem. 1995, 34, 2271.
15. Lah, M. S.; Pecoraro, V. L. J. Am. Chem. Soc. 1989, 111, 7258.
16. Lah, M. S.; Pecoraro, V. L. Inorg. Chem. 1991, 30, 878.
17. Kessissoglou, D. P.; Kampf, J.; Pecoraro, V. L. Polyhedron 1994, 13, 1379.
18. Gibney, B. R.; Kessissoglou, D. P.; Kampf, J. W.; Pecoraro, V. L. Inorg. Chem. 1994, 33, 4849.
19. Saalfrank, R. W.; Burak, R.; Reihs, S.; Löw, N.; Hampel, F.; Stachel, H.-D.; Lentmaier, J.; Peters, K.; Peters, E.-M.; von Schering, H. G. Angew. Chem., Int. Ed. Engl. 1995, 34, 993.
20. Saalfrank, R. W.; Bernt, I.; Uller, E.; Hampel, F. Angew. Chem., Int. Ed. Engl. 1997, 36, 2482.
21. Saalfrank, R. W.; Löw, N.; Kareth, S.; Seitz, V.; Hampel, F.; Stalke, D.; Teichert, M. Angew. Chem., Int. Ed. 1998, 37, 172.
22. -1, dmf solution): 460 (2217), 345 (18 614), 310 (18 556).
23. 3; Z = 2; GOF = 1.074, R1 = 0.0640; wR2 = 0.1700 for 7956 refs with I > 2σ(I). Symmetry equivalent data were averaged with R = 0.0444 to give 14 759 independent reflections from a total 15 177 collected.
24. (b) Sheldrick, G. M. SHELXS-86: Structure Solving Program; University of Gottingen: Germany. 1986.
25. (c) Sheldrick, G. M. SHELXL-93: Crystal Structure Refinement; University of Gottingen: Germany, 1993.
26. M(ox)N(ligand)-4] cores: 12 indicates the total ring size, 4 indicates the number of oxygen donor atoms, MC specifies the metallacrown, M and ox specify the ring metal and its oxidation state [Ni(II], N specifies the remaining nitrogen bridge, and in parenthesis are the abbreviations for the organic ligands that provide the oxygen donor atoms.