Determination of Fumonisins in Rodent Feed Using HPLC with Electrospray Mass Spectrometric Detection

Journal of Agricultural and Food Chemistry

Volumn 45, Issue 7, 1997, Pages 2573-2578

  Churchwell, Mona I ^a   Cooper, Willie Mae ^a   Howard, Paul C ^a   Doerge, Daniel R ^a  

^a NATIONAL CENTER FOR TOXICOLOGICAL RESEARCH   (United States)

Author keywords

Electrospray; Fumonisin; HPLC; Mass spectrometry; Rodent feed

Indexed keywords

RODENTIA;

EID: 0001075379     PISSN: 00218561     EISSN: None     Source Type: Journal    
DOI: 10.1021/jf970021l     Document Type: Article

References (21)

1. Bucci, T. J.; Howard, P. C. Effect of fumonisin mycotoxins in animals. J. Toxicol., Toxin Rev. 1996, 15, 293-302.
2. 1, a mycotoxin produced on corn by Fusarium moniliforme. Contemp. Top. 1993, 32, 26-28.
3. Doerge, D. R.; Bajic, S.; Analysis of Pesticides Using Atmospheric Pressure Chemical Ionization Mass Spectrometry. Rapid Commun. Mass Spectrom. 1992, 6, 663-666.
4. Doerge, D. R.; Howard, P. C.; Bajic, S.; Preece, S. W. Determination of fumonisins using on-line liquid chromatography coupled to electrospray mass spectrometry. Rapid Commun. Mass Spectrom. 1994, 8, 603-606.
5. Doerge, D. R.; Churchwell, M. I.; Rushing, L. G.; Bajic, S. Confirmation of gentian violet and its metabolite leucogentian violet in catfish muscle using LC-APCI/MS. Rapid Commun. Mass Spectrom. 1996a, 10, 1479-1484.
6. Doerge, D. R.; Churchwell, M. I.; Holder, C. L.; Rowe, L.; Bajic, S. Detection and confirmation of β-agonists in bovine retina using LC-APCI/MS. Anal. Chem. 1996b, 68, 1918-1923.
7. 1, in rats. Carcinogenesis 1991, 12, 1247-1251.
8. Haschek, W. M.; Motelin, G.; Ness, D. K.; Harlin, K. S.; Hall, W. F.; Vesonder, R. F.; Peterson, R. E.; Beasley, V. R. Characterization of fumonisin toxicity in orally and intravenously dosed swine. Mycopathologia 1992, 117, 83-96.
9. 1 in rodent feed by gradient elution HPLC using precolumn derivatization with and fluorescence detection. J. Agric. Food Chem. 1993, 41, 764-767.
10. 1 in corn-containing foods. J. Agric. Food Chem. 1993, 41, 1655-1658.
11. 1. Proc. Am. Assoc. Cancer Res. 1996, 37, 791.
12. 1. Onderstepoort J. Vet. Res. 1990, 57, 269-275.
13. 2 in corn and corn products by high-performance liquid chromatography-electrospray-ionization tandem mass spectrometry. Chromatographia 1996, 43, 124-128.
14. 1 containing stable isotopes. J. Assoc. Off. Anal. Chem. Int. 1994, 77, 525-532.
15. Rheeder, J. P.; Marasas, W. F. O.; Thiel, P. G.; Sydenham, E. W.; Shephard, G. S.; van Schalkwyk, D. J. Fusarium moniliforme and fumonisins in corn in relation to human esophageal cancer in Transkei. Phytopathology 1992, 82, 353-357.
16. Riley, R. T.; An, N.-H.; Showker, J. L.; Yoo, H.-S.; Norred, W. P.; Chamberlain, W. J.; Wang, E.; Merrill, Jr., A. H.; Montelin, G.; Beasley, V. R.; Haschek, W. M. Alteration of tissue and serum sphinganine to sphingosine ratio: An early biomarker of exposure to fumonisin-containing feeds in pigs. Toxicol. Appl. Pharmacol. 1993, 118, 105-112.
17. Shephard, G. S.; Thiel, P. G.; Stockenstrom, S.; Sydenham, E. W. Worldwide survey of fumonisin contamination of corn and corn-based products. J. Assoc. Off. Anal. Chem. Int. 1996, 79, 671-687.
18. Sydenham, E. W.; Shephard, G. S.; Thiel, P. G.; Marasas, W. F. O.; Stockenstrom, S. Fumonisin contamination of commercial corn-based human foodstuffs. J. Agric. Food Chem. 1991, 39, 2014-2018.
19. 3 in corn: AOAC-IUPAC collaborative study. J. Assoc. Off. Anal. Chem. Int. 1996, 79, 688-696.
20. Tolleson, W. H.; Sheldon, W. G.; Thurman, J. D.; Bucci, T. J.; Howard, P. C. The mycotoxin fumonisin induces apoptosis in cultured human cells and in livers and kidneys of rats. In Fumonisins in Foods; Jackson, L., DeVries, J. W., Bullerman, L. B., Eds.; Plenum Press: New York, 1996; pp 237-250.
21. Ware, G. M.; Umrigar, P. P.; Carman, A. S.; Kuan, S. S. Evaluation of Fumonitest immunoaffinity columns. Anal. Lett. 1994, 27, 693-715.