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0028880395
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Recently, Imamoto advocated the idea that the cooperative effect of the methoxy group in the (DIPAMP)Rh catalyst is based on purely steric grounds: T. Imamoto, H. Tsuruta, Y. Wada, H. Masuda, K. Yamaguchi, Tetrahedron Lett. 1995, 36, 8271-8274.
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0031802328
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Already one hydroxy group in a chiral (diphosphane)Rh complex is sufficient to achieve in the asymmetric hydrogenation in water in the presence of amphiphiles a dramatic increase of the enantioselectivity: R. Selke, J. Holz, A. Riepe, A. Börner. Chem. Eur. J. 1998, 4, 769-771.
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35
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0031019330
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and ref. cited therein
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D. Heller, J. Holz. S. Borns, A. Spannenberg, R. Kempe, U. Schmidt, A. Börner, Tetrahedron. Asymmetry 1997, 8, 213-222 and ref. cited therein.
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[13a] A. Borner, J. Ward, K. Kortus, H. B. Kagan, Tetrahedron: Asymmetry 1993, 4, 2219-2228.
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Borner, A.1
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37
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85163240894
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The amount of methanesulfonic acid (85 ml) given in the original paper for the cleavage of the acetal is to be corrected to 85 μl
-
[13b] The amount of methanesulfonic acid (85 ml) given in the original paper for the cleavage of the acetal is to be corrected to 85 μl.
-
-
-
-
39
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0001858736
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-
D. Heller, S. Borns, W. Baumann, R. Selke, Chem. Ber 1996, 129, 85-89.
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Heller, D.1
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-
40
-
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85163236302
-
-
The results of the hydrogenation were identical for the COD and the NBD complex
-
The results of the hydrogenation were identical for the COD and the NBD complex.
-
-
-
-
42
-
-
85163236653
-
-
unpublished, structure representation: Schakal-92 E. Keller, Universität Freiburg
-
2 (SHELXL-93: G.M. Sheldrick, unpublished), structure representation: Schakal-92 (E. Keller, Universität Freiburg, 1992).
-
(1992)
-
-
Sheldrick, G.M.1
-
43
-
-
85163236780
-
-
2 (all data) = 0.143, 397 parameters
-
2 (all data) = 0.143, 397 parameters.
-
-
-
-
44
-
-
85163239851
-
-
note
-
2 (all data) = 0.149, 401 parameters. - Crystallographic data (excluding structure factors) for the structures reported have been deposited with the Cambridge Crystallographic Centre as supplementary publication no. CCDC-100869. Copies of the data can be obtained free of charge on application to CCDC, 12 Union Road, Cambridge CB2 1EZ (Fax: int. code + 44-1223/336-033; E-mail: deposit@-ccdc.cam.ac.uk).
-
-
-
-
45
-
-
85163237848
-
-
-1[11]. Therefore, we tentatively attribute the band observed at the longer wavelength to the Rh-coordinated hydroxy group
-
-1[11]. Therefore, we tentatively attribute the band observed at the longer wavelength to the Rh-coordinated hydroxy group.
-
-
-
-
46
-
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0000057204
-
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A. Börner, A. Kless, J. Holz, W. Baumann, A. Tillack, R. Kadyrov, J. Organomet. Chem. 1995, 490, 213-219.
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Börner, A.1
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Holz, J.3
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Tillack, A.5
Kadyrov, R.6
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47
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0030350607
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[20a] K. Tamao, K. Nakamura, S. Yamaguchi, M. Shiro, S. Saito, Chem. Lett. 1996, 1007-1008.
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Tamao, K.1
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48
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0030457105
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[20b] K. Tamao, K. Nakamura, H. Ishii, S. Yamaguchi, M. Shiro, J. Am. Chem. Soc. 1996, 118, 12469-12470.
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Tamao, K.1
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Ishii, H.3
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Shiro, M.5
-
49
-
-
85163237841
-
-
The distance between the oxygen and the rhodium atom is larger than 3.5 Å
-
The distance between the oxygen and the rhodium atom is larger than 3.5 Å.
-
-
-
-
50
-
-
85163239424
-
-
[14] the stablization of the seven-membered chelate is provided by the rigid 1,3-dioxolane ring. Simultaneously, due to this construction both oxygen atoms are not available for the interaction with the metal center
-
[14] the stablization of the seven-membered chelate is provided by the rigid 1,3-dioxolane ring. Simultaneously, due to this construction both oxygen atoms are not available for the interaction with the metal center.
-
-
-
-
51
-
-
85163237091
-
-
In case of the HO-bearing complex attractive interactions between hydroxy and carboxylic group of the substrate may contribute to the improved stereoselection, however, up to now all attempts to obtain spectroscopical evidence for these interactions in methanol failed
-
In case of the HO-bearing complex attractive interactions between hydroxy and carboxylic group of the substrate may contribute to the improved stereoselection, however, up to now all attempts to obtain spectroscopical evidence for these interactions in methanol failed.
-
-
-
-
52
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85163236495
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-
[6a] electrostatic interactions may become more dominant at certain steps
-
[6a] electrostatic interactions may become more dominant at certain steps.
-
-
-
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53
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0026777783
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-
J. Ward, A. Börner, H. B. Kagan, Tetrahedron. Asymmetry 1992, 3, 849-852.
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Tetrahedron. Asymmetry
, vol.3
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Ward, J.1
Börner, A.2
Kagan, H.B.3
|