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85037506442
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note
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A heating without previous outgazing (laser heating under vacuum with defocused beam - 5 min) produces a white smoke (10 s) containing h-BN platelets, boron oxide, and other impurities, hut no BN nanostructure (TEM and EELS analysis). Commercial h-BN usually contains a large amount of impurities. Also, a little condensed surface of h-BN platelets (abrasive paper polished, etc.) gives poor results. (Here, surface results from a silicon carbide rotating saw.) It was also empirically found that a thermal shock (same procedure than outgazing, but for a few seconds) before heating drastically improves the reproducibility of experiment.
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85037514875
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JCTDS card No. 11-618
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JCTDS card No. 11-618.
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