The Solution Structure of a Copper(II) Compound of a New Cyclic Octapeptide by EPR Spectroscopy and Force Field Calculations

Inorganic Chemistry

Volumn 37, Issue 26, 1998, Pages 6721-6727

  Comba, Peter ^a   Cusack, Rodney ^b   Fairlie, David P ^b   Gahan, Lawrence R ^b   Hanson, Graeme R ^b   Kazmaier, Uli ^a   Ramlow, Anne ^a  

^a UNIVERSITY OF HEIDELBERG   (Germany)

^b UNIVERSITY OF QUEENSLAND   (Australia)

Author keywords

[No Author keywords available]

Indexed keywords

EID: 0000845438     PISSN: 00201669     EISSN: None     Source Type: Journal    
DOI: None     Document Type: Article

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52. 1H NMR spectra. Unambiguous reasons for these differences have not been identified so far, but all experiments reported here (spectroscopic analyses of the peptide, complexation with copper(II), and spectroscopic analyses of the mono-and dinuclear copper(II) compounds) have been done on a pure fraction of 22 mg of PatN that was combined from three independent cyclization/purification procedures.