First quaternary A-Pb-Bi-Q (A = K, Rb, Cs; Q = S, Se) compounds: Synthesis, structure, and properties of α-and β-CsPbBi3Se6, APbBi3Se6, (A = K, Rb), and APbBi3S6 (A = Rb, Cs)

Chemistry of Materials

Volumn 11, Issue 5, 1999, Pages 1352-1362

  Chung, Duck Young ^a   Iordanidis, Lykourgos ^a   Rangan, Krishnaswamy Kasthuri ^a   Brazis, Paul W ^b   Kannewurf, Carl R ^b   Kanatzidis, Mercouri G ^a  

^a MICHIGAN STATE UNIVERSITY   (United States)

^b Northwestern University   (United States)

Author keywords

[No Author keywords available]

Indexed keywords

EID: 0000834536     PISSN: 08974756     EISSN: None     Source Type: Journal    
DOI: 10.1021/cm9811388     Document Type: Article

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64. 6. The results from both programs are also consistent with our assignment of the M(4) site as Pb atom. The results are as follows: from EUTAX, valence sums at Bi(1) ) 3.168, Bi(2) ) 3.139, Bi(3) ) 3.242, Bi(4) ) 2.721, Se(1) ) 2.288, Se(2) ) 2.205, Se(3) ) 1.662, Se(4) ) 1.812, Se(5) ) 2.058, Se(6) ) 2.245; from VALENCE, valence sums at Bi(1) ) 2.929, Pb(1) ) 2.882, Bi(2) ) 2.999, Bi(3) ) 2.898, Bi(4) ) 2.514, Pb(4) ) 2.474.
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