Crystal and molecular structure of the solventfree hexamethyldisilazides of rubidium and cesium and the crystal structure of a toluene solvate;Kristall- und molekülstruktur der solvatfreien hexamethyldisilazide des rubidiums und caesiums und die kristallstruktur eines toluolsolvates

Zeitschrift fur Anorganische und Allgemeine Chemie

Volumn 625, Issue 9, 1999, Pages 1429-1434

  Neander, Swen ^a   Behrens, Ulrich ^a  

^a UNIVERSITY OF HAMBURG   (Germany)

Author keywords

Alkali metals; Cesium; Crystal Structure; Hexamethyldisilazide; Rubidium

Indexed keywords

EID: 0000813538     PISSN: 00442313     EISSN: None     Source Type: Journal    
DOI: 10.1002/(SICI)1521-3749(199909)625:9<1429::AID-ZAAC1429>3.0.CO;2-E     Document Type: Article

References (32)

1. Viele Beispiele in: L. F. Fieser, M. Fieser (Hrsg.), Reagents for Organic Synthesis, Bände 1-17, Wiley, New York, 1967-1994.
2. U. Wannagat, Pure Appl. Chem. 1969, 19, 329.
3. R. A. Andersen, K. Faegri, Jr., J. C. Green, A. Haaland, M. F. Lappert, W.-P. Leung, K. Rypdal, Inorg. Chem. 1988, 27, 1782.
4. S. Neander, Dissertation, Univ. Hamburg 1999.
5. a) D. Mootz, A. Zinnius, B. Böttcher, Angew. Chem. 1969, 81, 398; Angew. Chem. Int. Ed. Engl. 1969, 8, 378;
6. a) D. Mootz, A. Zinnius, B. Böttcher, Angew. Chem. 1969, 81, 398; Angew. Chem. Int. Ed. Engl. 1969, 8, 378;
7. b) R. D. Rogers, J. L. Atwood, R. Grüning, J. Organomet. Chem. 1978, 157, 229.
8. J. Knizek, I. Krossing, H. Nöth, H. Schwenk, T. Seifert, Chem. Ber. 1997, 130, 1053.
9. R. Grüning, J. L. Atwood, J. Organomet. Chem. 1977, 137, 101.
10. K. F. Tesh, T. P. Hanusa, J. C. Huffman, Inorg. Chem. 1990, 29, 1584.
11. P. G. Williard, Acta Crystallogr. 1988, C 44, 270.
12. T. Fjeldberg, P. B. Hitchcock, M. F. Lappert, A. J. Thorne, J. Chem. Soc., Chem. Commun. 1984, 822.
13. J. C. Green, M. Payne, E. A. Seddon, R. A. Andersen, J. Chem. Soc., Dalton Trans. 1982, 887.
14. H. Bürger, H. Seyffert, Angew. Chem. 1964, 76, 577; Angew. Chem. Int. Ed. Engl. 1964, 3, 646.
15. H. Bürger, H. Seyffert, Angew. Chem. 1964, 76, 577; Angew. Chem. Int. Ed. Engl. 1964, 3, 646.
16. K. W. Henderson, A. E. Dorigo, Qi-Y. Liu, P. G. Williard, J. Am. Chem. Soc. 1997, 119, 11855.
17. P. P. Power, X. Xiaojie, J. Chem. Soc., Chem. Commun. 1984, 358.
18. A. M. Domingos, G. M. Sheldrick, Acta Crystallogr. 1974, B 30, 517.
19. F. T. Edelmann, F. Pauer, M. Wedler, D. Stalke, Inorg. Chem. 1992, 31, 4143.
20. G. M. Sheldrick, SHELXS-97, Program for Crystal Structure Solution, Göttingen 1997.
21. G. M. Sheldrick, SHELXL-97, Program for the Refinement of Crystal Structures, Göttingen 1997.
22. R. D. Shannon, Acta Crystallogr. 1976, A 32, 751.
23. L. Pauling, The Nature of Chemical Bond, Cornell University Press, Ithaca, New York 1960.
24. M. Westerhausen, Coord. Chem. Rev. 1998, 176, 157.
25. P. G. Eller, D. C. Bradley, M. B. Hursthouse, D. W. Meek, Coord. Chem. Rev. 1977, 24, 1.
26. C. Eaborn, K. Izod, J. D. Smith, J. Organomet. Chem. 1995, 500, 89.
27. M. R. Kopp, B. Neumüller, Organometallics 1997, 16, 5623.
28. M. R. Kopp, B. Neumüller, Z. Anorg. Allg. Chem. 1998, 624, 361.
29. D. A. Dougherty, Science 1996, 271, 163.
30. A. L. Spek, DIFABS: Part of the program PLATON-95, Acta Crystallogr. 1990, A 46, C34; N. Walker, D. Stuart, DIFABS: An Empirical Method for Correcting Diffractometer Data for Absorption Effects, Acta Crystallogr. 1983, A 39, 158.
31. A. L. Spek, DIFABS: Part of the program PLATON-95, Acta Crystallogr. 1990, A 46, C34; N. Walker, D. Stuart, DIFABS: An Empirical Method for Correcting Diffractometer Data for Absorption Effects, Acta Crystallogr. 1983, A 39, 158.
32. G. M. Sheldrick, SADABS, Empirical Absorption Correction Program, Göttingen 1996.