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Volumn 17, Issue 2, 1998, Pages 173-181

Controlled acidolysis of hexacarbonyltris(μ-alkoxo)dirhenium(I) anions: Facile synthesis of hexacarbonylbis(μ-alkoxo)-[μ-1,1′-bis(diphenylphosphino)ferrocene] dirhenium(I) complexes and nonacarbonyltris(μ-methoxo)(μ3-methoxo)trirhenium(I)

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EID: 0000673203     PISSN: 02767333     EISSN: None     Source Type: Journal    
DOI: 10.1021/om970614l     Document Type: Article
Times cited : (50)

References (36)
  • 8
    • 3743155063 scopus 로고    scopus 로고
    • note
    • Abbreviations used: dppm = bis(diphenylphosphino)methane, dmpm = bis(diphenylphosphino)methane, dppe = 1,2-bis(diphenylphosphino)methane, dmpe = 1,2-bis(diphenylphosphino)methane.
  • 11
    • 3743090379 scopus 로고
    • Translated
    • Ioganson, A. A.; Lokshin, B. V.; Kolobova, E. E.; Anisimov, K. N. J. Gen. Chem. 1974, 20, 20. (Translated from Zh. Obshch. Khim. 1974, 44, 23.)
    • (1974) Zh. Obshch. Khim. , vol.44 , pp. 23
  • 20
    • 85086528228 scopus 로고    scopus 로고
    • note
    • 5.
  • 22
    • 85086527397 scopus 로고    scopus 로고
    • note
    • 1H NMR spectrum of an ethyl group. The methylene signals observed here are not first order, however, as discussed in the subsequent paragraph of the text.
  • 24
    • 0004204702 scopus 로고
    • Clarendon Press: Oxford
    • Emsley, J. The Elements; Clarendon Press: Oxford, 1989; p 46.
    • (1989) The Elements , pp. 46
    • Emsley, J.1
  • 25
  • 27
    • 85086527374 scopus 로고    scopus 로고
    • note
    • 2CO) data, the signals of the methoxo protons occur at δ 3.70 (s, 3H) and 4.23 (s, 9H), respectively. We observed the corresponding signals at δ 4.52 and 4.24, respectively, in the same solvent.
  • 32
    • 3743052432 scopus 로고    scopus 로고
    • note
    • The carbon analysis was consistently lower than the calculated value, despite excellent agreement for the H and N analyses, possibly due to the formation of a small amount of refractory rhenium carbide during combustion analysis.
  • 34
    • 0004150157 scopus 로고
    • Siemens Analytical X-ray Instruments, Inc.: Madison, WI
    • Sheldrick, G. M. SHELXTL PC, Version 5.03; Siemens Analytical X-ray Instruments, Inc.: Madison, WI, 1994.
    • (1994) SHELXTL PC, Version 5.03
    • Sheldrick, G.M.1
  • 36
    • 0039689659 scopus 로고
    • Ahmed, F. R., Ed.; Munksgaard: Copenhagen
    • The refined parameter is the average path length in a mosaic block in μm, see: Larson, A. C. In Crystallographic Computing; Ahmed, F. R., Ed.; Munksgaard: Copenhagen, 1970; p 293.
    • (1970) Crystallographic Computing , pp. 293
    • Larson, A.C.1


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.