Self-Assembly of Infinite Double Helical and Tubular Coordination Polymers from Ag(CF3SO3) and 1,3-Bis(4-pyridyl)propane

Inorganic Chemistry

Volumn 36, Issue 18, 1997, Pages 3812-3813

  Carlucci, Lucia ^a   Ciani, Gianfranco ^a   V Gudenberg, Dorothea W ^a   Proserpio, Davide M ^a  

^a CNR   (Italy)

Author keywords

[No Author keywords available]

Indexed keywords

EID: 0000668149     PISSN: 00201669     EISSN: None     Source Type: Journal    
DOI: 10.1021/ic970803w     Document Type: Article

References (27)

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18. -3, final A value 0.0965 for 2940 independent reflections [F 2, The data collections were performed at 293 K no a Siemens SMART CCD area-detector diffractometer for 1 and 2 and an Enrat Nonius CAD4 for 3 (Mo Ka. = 0.71073 Å the method within the limits 2 < H < 27° 11). 1 < 26°= (2), and < 0 < 25 (3). An empirical absorption correction was applied (SARABS for 1 and 2. -scan for 3). The structures were solved by direct method (SIR92) and refined by full-matrix least-squares (SHEL,X93.), Aniso, tropic thermal parameters were assigned to all the non-hydrogen atoms but in 3 where the statistically disordered bpp was refined isotropically All the diagrams were obtained using SCHAKAL programme.
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