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48
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2742579223
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note
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Four out of five geometric fac-isomers are chiral octahedrons thus forming pairs of diastereomers.
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0001005022
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Titanium tetrafluoride is insoluble in common aprotic solvents; however, its solubility is moderate in acetonitrile, see: D. R. Gauthier, E. M. Carreira, Angew. Chem. 1996, 108, 2521-2522; Angew. Chem. Int. Ed. Engl. 1996, 35, 2363-2365.
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0030472831
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Titanium tetrafluoride is insoluble in common aprotic solvents; however, its solubility is moderate in acetonitrile, see: D. R. Gauthier, E. M. Carreira, Angew. Chem. 1996, 108, 2521-2522; Angew. Chem. Int. Ed. Engl. 1996, 35, 2363-2365.
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55
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note
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Crystallographic data (excluding structure factors) for the structure reported in this paper have been deposited with the Cambridge Crystallographic Data Centre as supplementary publication no. CCDC-100872. Copies of the data can be obtained free of charge on application to CCDC, 12 Union Road, Cambridge CB2 1EZ, UK [fax: (internat.) + 44(1223)/336-033, e-mail: deposit@ccdc.cam.ac.uk].
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University of Göttingen, Germany
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G. M. Sheldrick, SHELXL-93, University of Göttingen, Germany, 1993
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Sheldrick, G.M.1
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