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3, 250 MHz; multiplicity, coupling constants in Hz, and relative integration in parentheses): 11.78 (d, 7.3, 1H); 8.90 (dd, 4.3, 1.8, 1H); 8.67 (dd; 7.4, 1.5, 1H); 8.23 (dd, 8.3, 1.8, 1H); 7.90 (dd, 8.1, 1.5, 1H):; 7.62 to 7.2 (m, 7H); 5.23 (d, 4.2, 1H); 4.45 (ddd, 4.2, 4.6, 4.7, 1H); 4.3 (s, 2H); 4.07 (dd, 4.6, 11.2, 1H); 3.92 (dd, 11.2, 4.7, 1H) ppm.
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