Generation and decomposition of a pentacoordinate spirobis[1,2-oxasiletanide]

Organometallics

Volumn 17, Issue 3, 1998, Pages 367-372

  Kawashima, Takayuki ^a   Naganuma, Kenji ^a   Okazaki, Renji ^a  

^a UNIVERSITY OF TOKYO   (Japan)

Author keywords

[No Author keywords available]

Indexed keywords

EID: 0000177530     PISSN: 02767333     EISSN: None     Source Type: Journal    
DOI: 10.1021/om970459a     Document Type: Article

References (61)

1. For recent reviews, see the following references. For silicon compounds: Corriu, R. J. P.; Guerin, C.; Moreau, L. E. In The Chemistry of Organic Silicon Compounds; Patai, S., Rappoport, Z., Eds.; John Wiley & Sons: Chichester, 1989; Part 1, Chapter 4. Corriu, R. J. P.; Young, J. C. In The Chemistry of Organic Silicon Compounds; Patai, S., Rappoport, Z., Eds.; John Wiley & Sons: Chichester, 1989; Part 2, Chapter 20. Holmes, R. R. Chem. Rev. 1990, 90, 17-31. Chuit, C.; Corriu, R. J. P.; Reye, C.; Young, J. C. Chem. Rev. 1993, 93, 1371-1448. For phosphorus compounds: Holmes, R. R. Chem. Rev. 1996, 96, 927-950. Wong, C. Y.; Kennepohl, Cavell, R. G. Chem. Rev. 1996, 96, 1917-1951. Arduengo, A. J., III; Stewart, C. A. Chem. Rev. 1994, 94, 1215-1237. For sulfur compounds: Hayes, R. A.; Martin, J. C. In Organic Sulfur Chemistry, Theoretical and Experimental Advances; Bernardi, F., Csizimadia, I. G., Mangini, A., Eds.; Elsevier: Amsterdam, 1985; Chapter 8. For selenium and tellurium compounds: Bergman, J.; Engman, L.; Sidén, J. In The Chemistry of Organic Selenium and Tellurium Compounds; Patai, S., Rappoport, Z., Eds.; John Wiley & Sons: New York, 1986; Vol. 1, Chapter 14. For iodine compounds: Stang, P. J.; Zhdankin, V. V. Chem. Rev. 1996, 96, 1123-1178.
2. For recent reviews, see the following references. For silicon compounds: Corriu, R. J. P.; Guerin, C.; Moreau, L. E. In The Chemistry of Organic Silicon Compounds; Patai, S., Rappoport, Z., Eds.; John Wiley & Sons: Chichester, 1989; Part 1, Chapter 4. Corriu, R. J. P.; Young, J. C. In The Chemistry of Organic Silicon Compounds; Patai, S., Rappoport, Z., Eds.; John Wiley & Sons: Chichester, 1989; Part 2, Chapter 20. Holmes, R. R. Chem. Rev. 1990, 90, 17-31. Chuit, C.; Corriu, R. J. P.; Reye, C.; Young, J. C. Chem. Rev. 1993, 93, 1371-1448. For phosphorus compounds: Holmes, R. R. Chem. Rev. 1996, 96, 927-950. Wong, C. Y.; Kennepohl, Cavell, R. G. Chem. Rev. 1996, 96, 1917-1951. Arduengo, A. J., III; Stewart, C. A. Chem. Rev. 1994, 94, 1215-1237. For sulfur compounds: Hayes, R. A.; Martin, J. C. In Organic Sulfur Chemistry, Theoretical and Experimental Advances; Bernardi, F., Csizimadia, I. G., Mangini, A., Eds.; Elsevier: Amsterdam, 1985; Chapter 8. For selenium and tellurium compounds: Bergman, J.; Engman, L.; Sidén, J. In The Chemistry of Organic Selenium and Tellurium Compounds; Patai, S., Rappoport, Z., Eds.; John Wiley & Sons: New York, 1986; Vol. 1, Chapter 14. For iodine compounds: Stang, P. J.; Zhdankin, V. V. Chem. Rev. 1996, 96, 1123-1178.
3. For recent reviews, see the following references. For silicon compounds: Corriu, R. J. P.; Guerin, C.; Moreau, L. E. In The Chemistry of Organic Silicon Compounds; Patai, S., Rappoport, Z., Eds.; John Wiley & Sons: Chichester, 1989; Part 1, Chapter 4. Corriu, R. J. P.; Young, J. C. In The Chemistry of Organic Silicon Compounds; Patai, S., Rappoport, Z., Eds.; John Wiley & Sons: Chichester, 1989; Part 2, Chapter 20. Holmes, R. R. Chem. Rev. 1990, 90, 17-31. Chuit, C.; Corriu, R. J. P.; Reye, C.; Young, J. C. Chem. Rev. 1993, 93, 1371-1448. For phosphorus compounds: Holmes, R. R. Chem. Rev. 1996, 96, 927-950. Wong, C. Y.; Kennepohl, Cavell, R. G. Chem. Rev. 1996, 96, 1917-1951. Arduengo, A. J., III; Stewart, C. A. Chem. Rev. 1994, 94, 1215-1237. For sulfur compounds: Hayes, R. A.; Martin, J. C. In Organic Sulfur Chemistry, Theoretical and Experimental Advances; Bernardi, F., Csizimadia, I. G., Mangini, A., Eds.; Elsevier: Amsterdam, 1985; Chapter 8. For selenium and tellurium compounds: Bergman, J.; Engman, L.; Sidén, J. In The Chemistry of Organic Selenium and Tellurium Compounds; Patai, S., Rappoport, Z., Eds.; John Wiley & Sons: New York, 1986; Vol. 1, Chapter 14. For iodine compounds: Stang, P. J.; Zhdankin, V. V. Chem. Rev. 1996, 96, 1123-1178.
4. For recent reviews, see the following references. For silicon compounds: Corriu, R. J. P.; Guerin, C.; Moreau, L. E. In The Chemistry of Organic Silicon Compounds; Patai, S., Rappoport, Z., Eds.; John Wiley & Sons: Chichester, 1989; Part 1, Chapter 4. Corriu, R. J. P.; Young, J. C. In The Chemistry of Organic Silicon Compounds; Patai, S., Rappoport, Z., Eds.; John Wiley & Sons: Chichester, 1989; Part 2, Chapter 20. Holmes, R. R. Chem. Rev. 1990, 90, 17-31. Chuit, C.; Corriu, R. J. P.; Reye, C.; Young, J. C. Chem. Rev. 1993, 93, 1371-1448. For phosphorus compounds: Holmes, R. R. Chem. Rev. 1996, 96, 927-950. Wong, C. Y.; Kennepohl, Cavell, R. G. Chem. Rev. 1996, 96, 1917-1951. Arduengo, A. J., III; Stewart, C. A. Chem. Rev. 1994, 94, 1215-1237. For sulfur compounds: Hayes, R. A.; Martin, J. C. In Organic Sulfur Chemistry, Theoretical and Experimental Advances; Bernardi, F., Csizimadia, I. G., Mangini, A., Eds.; Elsevier: Amsterdam, 1985; Chapter 8. For selenium and tellurium compounds: Bergman, J.; Engman, L.; Sidén, J. In The Chemistry of Organic Selenium and Tellurium Compounds; Patai, S., Rappoport, Z., Eds.; John Wiley & Sons: New York, 1986; Vol. 1, Chapter 14. For iodine compounds: Stang, P. J.; Zhdankin, V. V. Chem. Rev. 1996, 96, 1123-1178.
5. For recent reviews, see the following references. For silicon compounds: Corriu, R. J. P.; Guerin, C.; Moreau, L. E. In The Chemistry of Organic Silicon Compounds; Patai, S., Rappoport, Z., Eds.; John Wiley & Sons: Chichester, 1989; Part 1, Chapter 4. Corriu, R. J. P.; Young, J. C. In The Chemistry of Organic Silicon Compounds; Patai, S., Rappoport, Z., Eds.; John Wiley & Sons: Chichester, 1989; Part 2, Chapter 20. Holmes, R. R. Chem. Rev. 1990, 90, 17-31. Chuit, C.; Corriu, R. J. P.; Reye, C.; Young, J. C. Chem. Rev. 1993, 93, 1371-1448. For phosphorus compounds: Holmes, R. R. Chem. Rev. 1996, 96, 927-950. Wong, C. Y.; Kennepohl, Cavell, R. G. Chem. Rev. 1996, 96, 1917-1951. Arduengo, A. J., III; Stewart, C. A. Chem. Rev. 1994, 94, 1215-1237. For sulfur compounds: Hayes, R. A.; Martin, J. C. In Organic Sulfur Chemistry, Theoretical and Experimental Advances; Bernardi, F., Csizimadia, I. G., Mangini, A., Eds.; Elsevier: Amsterdam, 1985; Chapter 8. For selenium and tellurium compounds: Bergman, J.; Engman, L.; Sidén, J. In The Chemistry of Organic Selenium and Tellurium Compounds; Patai, S., Rappoport, Z., Eds.; John Wiley & Sons: New York, 1986; Vol. 1, Chapter 14. For iodine compounds: Stang, P. J.; Zhdankin, V. V. Chem. Rev. 1996, 96, 1123-1178.
6. For recent reviews, see the following references. For silicon compounds: Corriu, R. J. P.; Guerin, C.; Moreau, L. E. In The Chemistry of Organic Silicon Compounds; Patai, S., Rappoport, Z., Eds.; John Wiley & Sons: Chichester, 1989; Part 1, Chapter 4. Corriu, R. J. P.; Young, J. C. In The Chemistry of Organic Silicon Compounds; Patai, S., Rappoport, Z., Eds.; John Wiley & Sons: Chichester, 1989; Part 2, Chapter 20. Holmes, R. R. Chem. Rev. 1990, 90, 17-31. Chuit, C.; Corriu, R. J. P.; Reye, C.; Young, J. C. Chem. Rev. 1993, 93, 1371-1448. For phosphorus compounds: Holmes, R. R. Chem. Rev. 1996, 96, 927-950. Wong, C. Y.; Kennepohl, Cavell, R. G. Chem. Rev. 1996, 96, 1917-1951. Arduengo, A. J., III; Stewart, C. A. Chem. Rev. 1994, 94, 1215-1237. For sulfur compounds: Hayes, R. A.; Martin, J. C. In Organic Sulfur Chemistry, Theoretical and Experimental Advances; Bernardi, F., Csizimadia, I. G., Mangini, A., Eds.; Elsevier: Amsterdam, 1985; Chapter 8. For selenium and tellurium compounds: Bergman, J.; Engman, L.; Sidén, J. In The Chemistry of Organic Selenium and Tellurium Compounds; Patai, S., Rappoport, Z., Eds.; John Wiley & Sons: New York, 1986; Vol. 1, Chapter 14. For iodine compounds: Stang, P. J.; Zhdankin, V. V. Chem. Rev. 1996, 96, 1123-1178.
7. For recent reviews, see the following references. For silicon compounds: Corriu, R. J. P.; Guerin, C.; Moreau, L. E. In The Chemistry of Organic Silicon Compounds; Patai, S., Rappoport, Z., Eds.; John Wiley & Sons: Chichester, 1989; Part 1, Chapter 4. Corriu, R. J. P.; Young, J. C. In The Chemistry of Organic Silicon Compounds; Patai, S., Rappoport, Z., Eds.; John Wiley & Sons: Chichester, 1989; Part 2, Chapter 20. Holmes, R. R. Chem. Rev. 1990, 90, 17-31. Chuit, C.; Corriu, R. J. P.; Reye, C.; Young, J. C. Chem. Rev. 1993, 93, 1371-1448. For phosphorus compounds: Holmes, R. R. Chem. Rev. 1996, 96, 927-950. Wong, C. Y.; Kennepohl, Cavell, R. G. Chem. Rev. 1996, 96, 1917-1951. Arduengo, A. J., III; Stewart, C. A. Chem. Rev. 1994, 94, 1215-1237. For sulfur compounds: Hayes, R. A.; Martin, J. C. In Organic Sulfur Chemistry, Theoretical and Experimental Advances; Bernardi, F., Csizimadia, I. G., Mangini, A., Eds.; Elsevier: Amsterdam, 1985; Chapter 8. For selenium and tellurium compounds: Bergman, J.; Engman, L.; Sidén, J. In The Chemistry of Organic Selenium and Tellurium Compounds; Patai, S., Rappoport, Z., Eds.; John Wiley & Sons: New York, 1986; Vol. 1, Chapter 14. For iodine compounds: Stang, P. J.; Zhdankin, V. V. Chem. Rev. 1996, 96, 1123-1178.
8. For recent reviews, see the following references. For silicon compounds: Corriu, R. J. P.; Guerin, C.; Moreau, L. E. In The Chemistry of Organic Silicon Compounds; Patai, S., Rappoport, Z., Eds.; John Wiley & Sons: Chichester, 1989; Part 1, Chapter 4. Corriu, R. J. P.; Young, J. C. In The Chemistry of Organic Silicon Compounds; Patai, S., Rappoport, Z., Eds.; John Wiley & Sons: Chichester, 1989; Part 2, Chapter 20. Holmes, R. R. Chem. Rev. 1990, 90, 17-31. Chuit, C.; Corriu, R. J. P.; Reye, C.; Young, J. C. Chem. Rev. 1993, 93, 1371-1448. For phosphorus compounds: Holmes, R. R. Chem. Rev. 1996, 96, 927-950. Wong, C. Y.; Kennepohl, Cavell, R. G. Chem. Rev. 1996, 96, 1917-1951. Arduengo, A. J., III; Stewart, C. A. Chem. Rev. 1994, 94, 1215-1237. For sulfur compounds: Hayes, R. A.; Martin, J. C. In Organic Sulfur Chemistry, Theoretical and Experimental Advances; Bernardi, F., Csizimadia, I. G., Mangini, A., Eds.; Elsevier: Amsterdam, 1985; Chapter 8. For selenium and tellurium compounds: Bergman, J.; Engman, L.; Sidén, J. In The Chemistry of Organic Selenium and Tellurium Compounds; Patai, S., Rappoport, Z., Eds.; John Wiley & Sons: New York, 1986; Vol. 1, Chapter 14. For iodine compounds: Stang, P. J.; Zhdankin, V. V. Chem. Rev. 1996, 96, 1123-1178.
9. For recent reviews, see the following references. For silicon compounds: Corriu, R. J. P.; Guerin, C.; Moreau, L. E. In The Chemistry of Organic Silicon Compounds; Patai, S., Rappoport, Z., Eds.; John Wiley & Sons: Chichester, 1989; Part 1, Chapter 4. Corriu, R. J. P.; Young, J. C. In The Chemistry of Organic Silicon Compounds; Patai, S., Rappoport, Z., Eds.; John Wiley & Sons: Chichester, 1989; Part 2, Chapter 20. Holmes, R. R. Chem. Rev. 1990, 90, 17-31. Chuit, C.; Corriu, R. J. P.; Reye, C.; Young, J. C. Chem. Rev. 1993, 93, 1371-1448. For phosphorus compounds: Holmes, R. R. Chem. Rev. 1996, 96, 927-950. Wong, C. Y.; Kennepohl, Cavell, R. G. Chem. Rev. 1996, 96, 1917-1951. Arduengo, A. J., III; Stewart, C. A. Chem. Rev. 1994, 94, 1215-1237. For sulfur compounds: Hayes, R. A.; Martin, J. C. In Organic Sulfur Chemistry, Theoretical and Experimental Advances; Bernardi, F., Csizimadia, I. G., Mangini, A., Eds.; Elsevier: Amsterdam, 1985; Chapter 8. For selenium and tellurium compounds: Bergman, J.; Engman, L.; Sidén, J. In The Chemistry of Organic Selenium and Tellurium Compounds; Patai, S., Rappoport, Z., Eds.; John Wiley & Sons: New York, 1986; Vol. 1, Chapter 14. For iodine compounds: Stang, P. J.; Zhdankin, V. V. Chem. Rev. 1996, 96, 1123-1178.
10. For recent reviews, see the following references. For silicon compounds: Corriu, R. J. P.; Guerin, C.; Moreau, L. E. In The Chemistry of Organic Silicon Compounds; Patai, S., Rappoport, Z., Eds.; John Wiley & Sons: Chichester, 1989; Part 1, Chapter 4. Corriu, R. J. P.; Young, J. C. In The Chemistry of Organic Silicon Compounds; Patai, S., Rappoport, Z., Eds.; John Wiley & Sons: Chichester, 1989; Part 2, Chapter 20. Holmes, R. R. Chem. Rev. 1990, 90, 17-31. Chuit, C.; Corriu, R. J. P.; Reye, C.; Young, J. C. Chem. Rev. 1993, 93, 1371-1448. For phosphorus compounds: Holmes, R. R. Chem. Rev. 1996, 96, 927-950. Wong, C. Y.; Kennepohl, Cavell, R. G. Chem. Rev. 1996, 96, 1917-1951. Arduengo, A. J., III; Stewart, C. A. Chem. Rev. 1994, 94, 1215-1237. For sulfur compounds: Hayes, R. A.; Martin, J. C. In Organic Sulfur Chemistry, Theoretical and Experimental Advances; Bernardi, F., Csizimadia, I. G., Mangini, A., Eds.; Elsevier: Amsterdam, 1985; Chapter 8. For selenium and tellurium compounds: Bergman, J.; Engman, L.; Sidén, J. In The Chemistry of Organic Selenium and Tellurium Compounds; Patai, S., Rappoport, Z., Eds.; John Wiley & Sons: New York, 1986; Vol. 1, Chapter 14. For iodine compounds: Stang, P. J.; Zhdankin, V. V. Chem. Rev. 1996, 96, 1123-1178.
11. 2OLi, which can be prepared by directed lithiation of hexafluorocumyl alcohol, is usually used for the introduction of this ligand, see: Perozzi, E. F.; Michalak, R. S.; Figuly, G. D.; Stevenson, W. H., III; Dess, D. B.; Ross, R. M.; Martin, J. C. J. Org. Chem. 1981, 46, 1039-1053. For sulfurane oxides, see: Martin, J. C.; Perozzi, E. F. Science 1976, 191, 154-159. For organo-nonmetallic species, see: Martin, J. C. Science 1983, 221, 509-514. For 10-Te-4, see: Michalak, R. S.; Wilson, S. R.; Martin, J. C. J. Am. Chem. Soc. 1984, 106, 7529-7539. For 10-Br-3, see: Nguyen, T. T.; Wilson, S. R.; Martin, J. C. J. Am. Chem. Soc. 1986, 108, 3803-3811. For 10-Ge-5, see: Denmark, S. E.; Jacobs, R. T.; Dai-Ho, G.; Wilson, S. Organometallics 1990, 9, 3015-3019. For 10-Sb-4, see: Akiba, K.-y.; Nakata, H.; Yamamoto, Y.; Kojima, S. Chem. Lett. 1992, 1559-1562. For 10-Sn-5, see: Akiba, K.-y.; Ito, Y.; Kondo, F.; Ohashi, N.; Sakaguchi, A.; Kojima, S.; Yamamoto, Y. Chem. Lett. 1992, 1563-1566. For 10-I-4, see: Dess, D. B.; Wilson, S. R.; Martin, J. C. J. Am. Chem. Soc. 1993, 115, 2488-2495.
12. 2OLi, which can be prepared by directed lithiation of hexafluorocumyl alcohol, is usually used for the introduction of this ligand, see: Perozzi, E. F.; Michalak, R. S.; Figuly, G. D.; Stevenson, W. H., III; Dess, D. B.; Ross, R. M.; Martin, J. C. J. Org. Chem. 1981, 46, 1039-1053. For sulfurane oxides, see: Martin, J. C.; Perozzi, E. F. Science 1976, 191, 154-159. For organo-nonmetallic species, see: Martin, J. C. Science 1983, 221, 509-514. For 10-Te-4, see: Michalak, R. S.; Wilson, S. R.; Martin, J. C. J. Am. Chem. Soc. 1984, 106, 7529-7539. For 10-Br-3, see: Nguyen, T. T.; Wilson, S. R.; Martin, J. C. J. Am. Chem. Soc. 1986, 108, 3803-3811. For 10-Ge-5, see: Denmark, S. E.; Jacobs, R. T.; Dai-Ho, G.; Wilson, S. Organometallics 1990, 9, 3015-3019. For 10-Sb-4, see: Akiba, K.-y.; Nakata, H.; Yamamoto, Y.; Kojima, S. Chem. Lett. 1992, 1559-1562. For 10-Sn-5, see: Akiba, K.-y.; Ito, Y.; Kondo, F.; Ohashi, N.; Sakaguchi, A.; Kojima, S.; Yamamoto, Y. Chem. Lett. 1992, 1563-1566. For 10-I-4, see: Dess, D. B.; Wilson, S. R.; Martin, J. C. J. Am. Chem. Soc. 1993, 115, 2488-2495.
13. 2OLi, which can be prepared by directed lithiation of hexafluorocumyl alcohol, is usually used for the introduction of this ligand, see: Perozzi, E. F.; Michalak, R. S.; Figuly, G. D.; Stevenson, W. H., III; Dess, D. B.; Ross, R. M.; Martin, J. C. J. Org. Chem. 1981, 46, 1039-1053. For sulfurane oxides, see: Martin, J. C.; Perozzi, E. F. Science 1976, 191, 154-159. For organo-nonmetallic species, see: Martin, J. C. Science 1983, 221, 509-514. For 10-Te-4, see: Michalak, R. S.; Wilson, S. R.; Martin, J. C. J. Am. Chem. Soc. 1984, 106, 7529-7539. For 10-Br-3, see: Nguyen, T. T.; Wilson, S. R.; Martin, J. C. J. Am. Chem. Soc. 1986, 108, 3803-3811. For 10-Ge-5, see: Denmark, S. E.; Jacobs, R. T.; Dai-Ho, G.; Wilson, S. Organometallics 1990, 9, 3015-3019. For 10-Sb-4, see: Akiba, K.-y.; Nakata, H.; Yamamoto, Y.; Kojima, S. Chem. Lett. 1992, 1559-1562. For 10-Sn-5, see: Akiba, K.-y.; Ito, Y.; Kondo, F.; Ohashi, N.; Sakaguchi, A.; Kojima, S.; Yamamoto, Y. Chem. Lett. 1992, 1563-1566. For 10-I-4, see: Dess, D. B.; Wilson, S. R.; Martin, J. C. J. Am. Chem. Soc. 1993, 115, 2488-2495.
14. 2OLi, which can be prepared by directed lithiation of hexafluorocumyl alcohol, is usually used for the introduction of this ligand, see: Perozzi, E. F.; Michalak, R. S.; Figuly, G. D.; Stevenson, W. H., III; Dess, D. B.; Ross, R. M.; Martin, J. C. J. Org. Chem. 1981, 46, 1039-1053. For sulfurane oxides, see: Martin, J. C.; Perozzi, E. F. Science 1976, 191, 154-159. For organo-nonmetallic species, see: Martin, J. C. Science 1983, 221, 509-514. For 10-Te-4, see: Michalak, R. S.; Wilson, S. R.; Martin, J. C. J. Am. Chem. Soc. 1984, 106, 7529-7539. For 10-Br-3, see: Nguyen, T. T.; Wilson, S. R.; Martin, J. C. J. Am. Chem. Soc. 1986, 108, 3803-3811. For 10-Ge-5, see: Denmark, S. E.; Jacobs, R. T.; Dai-Ho, G.; Wilson, S. Organometallics 1990, 9, 3015-3019. For 10-Sb-4, see: Akiba, K.-y.; Nakata, H.; Yamamoto, Y.; Kojima, S. Chem. Lett. 1992, 1559-1562. For 10-Sn-5, see: Akiba, K.-y.; Ito, Y.; Kondo, F.; Ohashi, N.; Sakaguchi, A.; Kojima, S.; Yamamoto, Y. Chem. Lett. 1992, 1563-1566. For 10-I-4, see: Dess, D. B.; Wilson, S. R.; Martin, J. C. J. Am. Chem. Soc. 1993, 115, 2488-2495.
15. 2OLi, which can be prepared by directed lithiation of hexafluorocumyl alcohol, is usually used for the introduction of this ligand, see: Perozzi, E. F.; Michalak, R. S.; Figuly, G. D.; Stevenson, W. H., III; Dess, D. B.; Ross, R. M.; Martin, J. C. J. Org. Chem. 1981, 46, 1039-1053. For sulfurane oxides, see: Martin, J. C.; Perozzi, E. F. Science 1976, 191, 154-159. For organo-nonmetallic species, see: Martin, J. C. Science 1983, 221, 509-514. For 10-Te-4, see: Michalak, R. S.; Wilson, S. R.; Martin, J. C. J. Am. Chem. Soc. 1984, 106, 7529-7539. For 10-Br-3, see: Nguyen, T. T.; Wilson, S. R.; Martin, J. C. J. Am. Chem. Soc. 1986, 108, 3803-3811. For 10-Ge-5, see: Denmark, S. E.; Jacobs, R. T.; Dai-Ho, G.; Wilson, S. Organometallics 1990, 9, 3015-3019. For 10-Sb-4, see: Akiba, K.-y.; Nakata, H.; Yamamoto, Y.; Kojima, S. Chem. Lett. 1992, 1559-1562. For 10-Sn-5, see: Akiba, K.-y.; Ito, Y.; Kondo, F.; Ohashi, N.; Sakaguchi, A.; Kojima, S.; Yamamoto, Y. Chem. Lett. 1992, 1563-1566. For 10-I-4, see: Dess, D. B.; Wilson, S. R.; Martin, J. C. J. Am. Chem. Soc. 1993, 115, 2488-2495.
16. 2OLi, which can be prepared by directed lithiation of hexafluorocumyl alcohol, is usually used for the introduction of this ligand, see: Perozzi, E. F.; Michalak, R. S.; Figuly, G. D.; Stevenson, W. H., III; Dess, D. B.; Ross, R. M.; Martin, J. C. J. Org. Chem. 1981, 46, 1039-1053. For sulfurane oxides, see: Martin, J. C.; Perozzi, E. F. Science 1976, 191, 154-159. For organo-nonmetallic species, see: Martin, J. C. Science 1983, 221, 509-514. For 10-Te-4, see: Michalak, R. S.; Wilson, S. R.; Martin, J. C. J. Am. Chem. Soc. 1984, 106, 7529-7539. For 10-Br-3, see: Nguyen, T. T.; Wilson, S. R.; Martin, J. C. J. Am. Chem. Soc. 1986, 108, 3803-3811. For 10-Ge-5, see: Denmark, S. E.; Jacobs, R. T.; Dai-Ho, G.; Wilson, S. Organometallics 1990, 9, 3015-3019. For 10-Sb-4, see: Akiba, K.-y.; Nakata, H.; Yamamoto, Y.; Kojima, S. Chem. Lett. 1992, 1559-1562. For 10-Sn-5, see: Akiba, K.-y.; Ito, Y.; Kondo, F.; Ohashi, N.; Sakaguchi, A.; Kojima, S.; Yamamoto, Y. Chem. Lett. 1992, 1563-1566. For 10-I-4, see: Dess, D. B.; Wilson, S. R.; Martin, J. C. J. Am. Chem. Soc. 1993, 115, 2488-2495.
17. 2OLi, which can be prepared by directed lithiation of hexafluorocumyl alcohol, is usually used for the introduction of this ligand, see: Perozzi, E. F.; Michalak, R. S.; Figuly, G. D.; Stevenson, W. H., III; Dess, D. B.; Ross, R. M.; Martin, J. C. J. Org. Chem. 1981, 46, 1039-1053. For sulfurane oxides, see: Martin, J. C.; Perozzi, E. F. Science 1976, 191, 154-159. For organo-nonmetallic species, see: Martin, J. C. Science 1983, 221, 509-514. For 10-Te-4, see: Michalak, R. S.; Wilson, S. R.; Martin, J. C. J. Am. Chem. Soc. 1984, 106, 7529-7539. For 10-Br-3, see: Nguyen, T. T.; Wilson, S. R.; Martin, J. C. J. Am. Chem. Soc. 1986, 108, 3803-3811. For 10-Ge-5, see: Denmark, S. E.; Jacobs, R. T.; Dai-Ho, G.; Wilson, S. Organometallics 1990, 9, 3015-3019. For 10-Sb-4, see: Akiba, K.-y.; Nakata, H.; Yamamoto, Y.; Kojima, S. Chem. Lett. 1992, 1559-1562. For 10-Sn-5, see: Akiba, K.-y.; Ito, Y.; Kondo, F.; Ohashi, N.; Sakaguchi, A.; Kojima, S.; Yamamoto, Y. Chem. Lett. 1992, 1563-1566. For 10-I-4, see: Dess, D. B.; Wilson, S. R.; Martin, J. C. J. Am. Chem. Soc. 1993, 115, 2488-2495.
18. 2OLi, which can be prepared by directed lithiation of hexafluorocumyl alcohol, is usually used for the introduction of this ligand, see: Perozzi, E. F.; Michalak, R. S.; Figuly, G. D.; Stevenson, W. H., III; Dess, D. B.; Ross, R. M.; Martin, J. C. J. Org. Chem. 1981, 46, 1039-1053. For sulfurane oxides, see: Martin, J. C.; Perozzi, E. F. Science 1976, 191, 154-159. For organo-nonmetallic species, see: Martin, J. C. Science 1983, 221, 509-514. For 10-Te-4, see: Michalak, R. S.; Wilson, S. R.; Martin, J. C. J. Am. Chem. Soc. 1984, 106, 7529-7539. For 10-Br-3, see: Nguyen, T. T.; Wilson, S. R.; Martin, J. C. J. Am. Chem. Soc. 1986, 108, 3803-3811. For 10-Ge-5, see: Denmark, S. E.; Jacobs, R. T.; Dai-Ho, G.; Wilson, S. Organometallics 1990, 9, 3015-3019. For 10-Sb-4, see: Akiba, K.-y.; Nakata, H.; Yamamoto, Y.; Kojima, S. Chem. Lett. 1992, 1559-1562. For 10-Sn-5, see: Akiba, K.-y.; Ito, Y.; Kondo, F.; Ohashi, N.; Sakaguchi, A.; Kojima, S.; Yamamoto, Y. Chem. Lett. 1992, 1563-1566. For 10-I-4, see: Dess, D. B.; Wilson, S. R.; Martin, J. C. J. Am. Chem. Soc. 1993, 115, 2488-2495.
19. 2OLi, which can be prepared by directed lithiation of hexafluorocumyl alcohol, is usually used for the introduction of this ligand, see: Perozzi, E. F.; Michalak, R. S.; Figuly, G. D.; Stevenson, W. H., III; Dess, D. B.; Ross, R. M.; Martin, J. C. J. Org. Chem. 1981, 46, 1039-1053. For sulfurane oxides, see: Martin, J. C.; Perozzi, E. F. Science 1976, 191, 154-159. For organo-nonmetallic species, see: Martin, J. C. Science 1983, 221, 509-514. For 10-Te-4, see: Michalak, R. S.; Wilson, S. R.; Martin, J. C. J. Am. Chem. Soc. 1984, 106, 7529-7539. For 10-Br-3, see: Nguyen, T. T.; Wilson, S. R.; Martin, J. C. J. Am. Chem. Soc. 1986, 108, 3803-3811. For 10-Ge-5, see: Denmark, S. E.; Jacobs, R. T.; Dai-Ho, G.; Wilson, S. Organometallics 1990, 9, 3015-3019. For 10-Sb-4, see: Akiba, K.-y.; Nakata, H.; Yamamoto, Y.; Kojima, S. Chem. Lett. 1992, 1559-1562. For 10-Sn-5, see: Akiba, K.-y.; Ito, Y.; Kondo, F.; Ohashi, N.; Sakaguchi, A.; Kojima, S.; Yamamoto, Y. Chem. Lett. 1992, 1563-1566. For 10-I-4, see: Dess, D. B.; Wilson, S. R.; Martin, J. C. J. Am. Chem. Soc. 1993, 115, 2488-2495.
20. For 10-Si-5, see: Stevenson, W. H., III; Wilson, S.; Martin, J. C.; Farnham, W. B. J. Am. Chem. Soc. 1985, 107, 6340-6352.
21. 2 can be used for the introduction of this ligand, by which a pentacoordinate tin compound was synthesized for the first time, see: van Koten, G.; Schaap, C. A.; Noltes, J. G. J. Organomet. Chem. 1975, 99, 157-170. For 10-Sn-5, see: van Koten, G.; Noltes, J. G.; Spek, A. L. J. Organomet. Chem. 1976, 118, 183-189. van Koten, G.; Noltes, J. G. J. Am. Chem. Soc. 1976, 98, 5393-5395. van Koten, G.; Jastrzebski, J. T. B. H.; Noltes, J. G.; Pontenagel, W. M. G. F.; Kroon, J.; Spek, A. L. J. Am. Chem. Soc. 1978, 100, 5021-5028. For 10-Ge-5, see: Breliere. C.; Carré, F.; Corriu, R. J. P.; de Saxcé, A.; Poirier, M.; Royo, G. J. Organomet. Chem. 1981, 205, C1-C3. For 10-Si-5, see: Corriu, R. J. P.; Kpoton, A.; Poirier, M.; Royo, G.; de Saxcé, A.; Young, J. C. J. Organomet. Chem. 1990, 395, 1-26. Corriu, R. J. P.; Royo, G.; de Saxcé, A. J. Chem. Soc., Chem. Commun. 1980, 892-894. Boyer, J.; Breière, C.; Carré, F.; Corriu, R. J. P.; Kpoton, A.; Poirier, M. Royo, G.; Young, J. C. J. Chem. Soc., Dalton Trans. 1989, 43-51. For 12-Si-6, see: Brelière, C.; Carré, F.; Corriu, R. J. P.; Douglas, W. E.; Poirier, M.; Royo, G.; Wong Chi Man, M. Organometallics 1992, 11, 1586-1593. For 12-P-6, see: Chuit, C.; Cornu, R. J. P.; Monforte, P.; Reyé, C.; Declereq, J.-P.; Dubourg, A. Angew. Chem., Int. Ed. Engl. 1993, 32, 1430-1432. For 10-Bi-4, see: Yamamoto, Y.; Chen, X.; Akiba, K.-y. J. Am. Chem. Soc. 1992, 114, 7906-7907. Yamamoto, Y.; Chen, X.; Kojima, S.; Ohdoi, K.; Kitano, M.; Doi, Y.; Akiba, K.-y. J. Am. Chem. Soc. 1995, 117, 3922-3932 (a similar 10-Sb-4 compound was also reported).
22. 2 can be used for the introduction of this ligand, by which a pentacoordinate tin compound was synthesized for the first time, see: van Koten, G.; Schaap, C. A.; Noltes, J. G. J. Organomet. Chem. 1975, 99, 157-170. For 10-Sn-5, see: van Koten, G.; Noltes, J. G.; Spek, A. L. J. Organomet. Chem. 1976, 118, 183-189. van Koten, G.; Noltes, J. G. J. Am. Chem. Soc. 1976, 98, 5393-5395. van Koten, G.; Jastrzebski, J. T. B. H.; Noltes, J. G.; Pontenagel, W. M. G. F.; Kroon, J.; Spek, A. L. J. Am. Chem. Soc. 1978, 100, 5021-5028. For 10-Ge-5, see: Breliere. C.; Carré, F.; Corriu, R. J. P.; de Saxcé, A.; Poirier, M.; Royo, G. J. Organomet. Chem. 1981, 205, C1-C3. For 10-Si-5, see: Corriu, R. J. P.; Kpoton, A.; Poirier, M.; Royo, G.; de Saxcé, A.; Young, J. C. J. Organomet. Chem. 1990, 395, 1-26. Corriu, R. J. P.; Royo, G.; de Saxcé, A. J. Chem. Soc., Chem. Commun. 1980, 892-894. Boyer, J.; Breière, C.; Carré, F.; Corriu, R. J. P.; Kpoton, A.; Poirier, M. Royo, G.; Young, J. C. J. Chem. Soc., Dalton Trans. 1989, 43-51. For 12-Si-6, see: Brelière, C.; Carré, F.; Corriu, R. J. P.; Douglas, W. E.; Poirier, M.; Royo, G.; Wong Chi Man, M. Organometallics 1992, 11, 1586-1593. For 12-P-6, see: Chuit, C.; Cornu, R. J. P.; Monforte, P.; Reyé, C.; Declereq, J.-P.; Dubourg, A. Angew. Chem., Int. Ed. Engl. 1993, 32, 1430-1432. For 10-Bi-4, see: Yamamoto, Y.; Chen, X.; Akiba, K.-y. J. Am. Chem. Soc. 1992, 114, 7906-7907. Yamamoto, Y.; Chen, X.; Kojima, S.; Ohdoi, K.; Kitano, M.; Doi, Y.; Akiba, K.-y. J. Am. Chem. Soc. 1995, 117, 3922-3932 (a similar 10-Sb-4 compound was also reported).
23. 2 can be used for the introduction of this ligand, by which a pentacoordinate tin compound was synthesized for the first time, see: van Koten, G.; Schaap, C. A.; Noltes, J. G. J. Organomet. Chem. 1975, 99, 157-170. For 10-Sn-5, see: van Koten, G.; Noltes, J. G.; Spek, A. L. J. Organomet. Chem. 1976, 118, 183-189. van Koten, G.; Noltes, J. G. J. Am. Chem. Soc. 1976, 98, 5393-5395. van Koten, G.; Jastrzebski, J. T. B. H.; Noltes, J. G.; Pontenagel, W. M. G. F.; Kroon, J.; Spek, A. L. J. Am. Chem. Soc. 1978, 100, 5021-5028. For 10-Ge-5, see: Breliere. C.; Carré, F.; Corriu, R. J. P.; de Saxcé, A.; Poirier, M.; Royo, G. J. Organomet. Chem. 1981, 205, C1-C3. For 10-Si-5, see: Corriu, R. J. P.; Kpoton, A.; Poirier, M.; Royo, G.; de Saxcé, A.; Young, J. C. J. Organomet. Chem. 1990, 395, 1-26. Corriu, R. J. P.; Royo, G.; de Saxcé, A. J. Chem. Soc., Chem. Commun. 1980, 892-894. Boyer, J.; Breière, C.; Carré, F.; Corriu, R. J. P.; Kpoton, A.; Poirier, M. Royo, G.; Young, J. C. J. Chem. Soc., Dalton Trans. 1989, 43-51. For 12-Si-6, see: Brelière, C.; Carré, F.; Corriu, R. J. P.; Douglas, W. E.; Poirier, M.; Royo, G.; Wong Chi Man, M. Organometallics 1992, 11, 1586-1593. For 12-P-6, see: Chuit, C.; Cornu, R. J. P.; Monforte, P.; Reyé, C.; Declereq, J.-P.; Dubourg, A. Angew. Chem., Int. Ed. Engl. 1993, 32, 1430-1432. For 10-Bi-4, see: Yamamoto, Y.; Chen, X.; Akiba, K.-y. J. Am. Chem. Soc. 1992, 114, 7906-7907. Yamamoto, Y.; Chen, X.; Kojima, S.; Ohdoi, K.; Kitano, M.; Doi, Y.; Akiba, K.-y. J. Am. Chem. Soc. 1995, 117, 3922-3932 (a similar 10-Sb-4 compound was also reported).
24. 2 can be used for the introduction of this ligand, by which a pentacoordinate tin compound was synthesized for the first time, see: van Koten, G.; Schaap, C. A.; Noltes, J. G. J. Organomet. Chem. 1975, 99, 157-170. For 10-Sn-5, see: van Koten, G.; Noltes, J. G.; Spek, A. L. J. Organomet. Chem. 1976, 118, 183-189. van Koten, G.; Noltes, J. G. J. Am. Chem. Soc. 1976, 98, 5393-5395. van Koten, G.; Jastrzebski, J. T. B. H.; Noltes, J. G.; Pontenagel, W. M. G. F.; Kroon, J.; Spek, A. L. J. Am. Chem. Soc. 1978, 100, 5021-5028. For 10-Ge-5, see: Breliere. C.; Carré, F.; Corriu, R. J. P.; de Saxcé, A.; Poirier, M.; Royo, G. J. Organomet. Chem. 1981, 205, C1-C3. For 10-Si-5, see: Corriu, R. J. P.; Kpoton, A.; Poirier, M.; Royo, G.; de Saxcé, A.; Young, J. C. J. Organomet. Chem. 1990, 395, 1-26. Corriu, R. J. P.; Royo, G.; de Saxcé, A. J. Chem. Soc., Chem. Commun. 1980, 892-894. Boyer, J.; Breière, C.; Carré, F.; Corriu, R. J. P.; Kpoton, A.; Poirier, M. Royo, G.; Young, J. C. J. Chem. Soc., Dalton Trans. 1989, 43-51. For 12-Si-6, see: Brelière, C.; Carré, F.; Corriu, R. J. P.; Douglas, W. E.; Poirier, M.; Royo, G.; Wong Chi Man, M. Organometallics 1992, 11, 1586-1593. For 12-P-6, see: Chuit, C.; Cornu, R. J. P.; Monforte, P.; Reyé, C.; Declereq, J.-P.; Dubourg, A. Angew. Chem., Int. Ed. Engl. 1993, 32, 1430-1432. For 10-Bi-4, see: Yamamoto, Y.; Chen, X.; Akiba, K.-y. J. Am. Chem. Soc. 1992, 114, 7906-7907. Yamamoto, Y.; Chen, X.; Kojima, S.; Ohdoi, K.; Kitano, M.; Doi, Y.; Akiba, K.-y. J. Am. Chem. Soc. 1995, 117, 3922-3932 (a similar 10-Sb-4 compound was also reported).
25. 2 can be used for the introduction of this ligand, by which a pentacoordinate tin compound was synthesized for the first time, see: van Koten, G.; Schaap, C. A.; Noltes, J. G. J. Organomet. Chem. 1975, 99, 157-170. For 10-Sn-5, see: van Koten, G.; Noltes, J. G.; Spek, A. L. J. Organomet. Chem. 1976, 118, 183-189. van Koten, G.; Noltes, J. G. J. Am. Chem. Soc. 1976, 98, 5393-5395. van Koten, G.; Jastrzebski, J. T. B. H.; Noltes, J. G.; Pontenagel, W. M. G. F.; Kroon, J.; Spek, A. L. J. Am. Chem. Soc. 1978, 100, 5021-5028. For 10-Ge-5, see: Breliere. C.; Carré, F.; Corriu, R. J. P.; de Saxcé, A.; Poirier, M.; Royo, G. J. Organomet. Chem. 1981, 205, C1-C3. For 10-Si-5, see: Corriu, R. J. P.; Kpoton, A.; Poirier, M.; Royo, G.; de Saxcé, A.; Young, J. C. J. Organomet. Chem. 1990, 395, 1-26. Corriu, R. J. P.; Royo, G.; de Saxcé, A. J. Chem. Soc., Chem. Commun. 1980, 892-894. Boyer, J.; Breière, C.; Carré, F.; Corriu, R. J. P.; Kpoton, A.; Poirier, M. Royo, G.; Young, J. C. J. Chem. Soc., Dalton Trans. 1989, 43-51. For 12-Si-6, see: Brelière, C.; Carré, F.; Corriu, R. J. P.; Douglas, W. E.; Poirier, M.; Royo, G.; Wong Chi Man, M. Organometallics 1992, 11, 1586-1593. For 12-P-6, see: Chuit, C.; Cornu, R. J. P.; Monforte, P.; Reyé, C.; Declereq, J.-P.; Dubourg, A. Angew. Chem., Int. Ed. Engl. 1993, 32, 1430-1432. For 10-Bi-4, see: Yamamoto, Y.; Chen, X.; Akiba, K.-y. J. Am. Chem. Soc. 1992, 114, 7906-7907. Yamamoto, Y.; Chen, X.; Kojima, S.; Ohdoi, K.; Kitano, M.; Doi, Y.; Akiba, K.-y. J. Am. Chem. Soc. 1995, 117, 3922-3932 (a similar 10-Sb-4 compound was also reported).
26. 2 can be used for the introduction of this ligand, by which a pentacoordinate tin compound was synthesized for the first time, see: van Koten, G.; Schaap, C. A.; Noltes, J. G. J. Organomet. Chem. 1975, 99, 157-170. For 10-Sn-5, see: van Koten, G.; Noltes, J. G.; Spek, A. L. J. Organomet. Chem. 1976, 118, 183-189. van Koten, G.; Noltes, J. G. J. Am. Chem. Soc. 1976, 98, 5393-5395. van Koten, G.; Jastrzebski, J. T. B. H.; Noltes, J. G.; Pontenagel, W. M. G. F.; Kroon, J.; Spek, A. L. J. Am. Chem. Soc. 1978, 100, 5021-5028. For 10-Ge-5, see: Breliere. C.; Carré, F.; Corriu, R. J. P.; de Saxcé, A.; Poirier, M.; Royo, G. J. Organomet. Chem. 1981, 205, C1-C3. For 10-Si-5, see: Corriu, R. J. P.; Kpoton, A.; Poirier, M.; Royo, G.; de Saxcé, A.; Young, J. C. J. Organomet. Chem. 1990, 395, 1-26. Corriu, R. J. P.; Royo, G.; de Saxcé, A. J. Chem. Soc., Chem. Commun. 1980, 892-894. Boyer, J.; Breière, C.; Carré, F.; Corriu, R. J. P.; Kpoton, A.; Poirier, M. Royo, G.; Young, J. C. J. Chem. Soc., Dalton Trans. 1989, 43-51. For 12-Si-6, see: Brelière, C.; Carré, F.; Corriu, R. J. P.; Douglas, W. E.; Poirier, M.; Royo, G.; Wong Chi Man, M. Organometallics 1992, 11, 1586-1593. For 12-P-6, see: Chuit, C.; Cornu, R. J. P.; Monforte, P.; Reyé, C.; Declereq, J.-P.; Dubourg, A. Angew. Chem., Int. Ed. Engl. 1993, 32, 1430-1432. For 10-Bi-4, see: Yamamoto, Y.; Chen, X.; Akiba, K.-y. J. Am. Chem. Soc. 1992, 114, 7906-7907. Yamamoto, Y.; Chen, X.; Kojima, S.; Ohdoi, K.; Kitano, M.; Doi, Y.; Akiba, K.-y. J. Am. Chem. Soc. 1995, 117, 3922-3932 (a similar 10-Sb-4 compound was also reported).
27. 2 can be used for the introduction of this ligand, by which a pentacoordinate tin compound was synthesized for the first time, see: van Koten, G.; Schaap, C. A.; Noltes, J. G. J. Organomet. Chem. 1975, 99, 157-170. For 10-Sn-5, see: van Koten, G.; Noltes, J. G.; Spek, A. L. J. Organomet. Chem. 1976, 118, 183-189. van Koten, G.; Noltes, J. G. J. Am. Chem. Soc. 1976, 98, 5393-5395. van Koten, G.; Jastrzebski, J. T. B. H.; Noltes, J. G.; Pontenagel, W. M. G. F.; Kroon, J.; Spek, A. L. J. Am. Chem. Soc. 1978, 100, 5021-5028. For 10-Ge-5, see: Breliere. C.; Carré, F.; Corriu, R. J. P.; de Saxcé, A.; Poirier, M.; Royo, G. J. Organomet. Chem. 1981, 205, C1-C3. For 10-Si-5, see: Corriu, R. J. P.; Kpoton, A.; Poirier, M.; Royo, G.; de Saxcé, A.; Young, J. C. J. Organomet. Chem. 1990, 395, 1-26. Corriu, R. J. P.; Royo, G.; de Saxcé, A. J. Chem. Soc., Chem. Commun. 1980, 892-894. Boyer, J.; Breière, C.; Carré, F.; Corriu, R. J. P.; Kpoton, A.; Poirier, M. Royo, G.; Young, J. C. J. Chem. Soc., Dalton Trans. 1989, 43-51. For 12-Si-6, see: Brelière, C.; Carré, F.; Corriu, R. J. P.; Douglas, W. E.; Poirier, M.; Royo, G.; Wong Chi Man, M. Organometallics 1992, 11, 1586-1593. For 12-P-6, see: Chuit, C.; Cornu, R. J. P.; Monforte, P.; Reyé, C.; Declereq, J.-P.; Dubourg, A. Angew. Chem., Int. Ed. Engl. 1993, 32, 1430-1432. For 10-Bi-4, see: Yamamoto, Y.; Chen, X.; Akiba, K.-y. J. Am. Chem. Soc. 1992, 114, 7906-7907. Yamamoto, Y.; Chen, X.; Kojima, S.; Ohdoi, K.; Kitano, M.; Doi, Y.; Akiba, K.-y. J. Am. Chem. Soc. 1995, 117, 3922-3932 (a similar 10-Sb-4 compound was also reported).
28. 2 can be used for the introduction of this ligand, by which a pentacoordinate tin compound was synthesized for the first time, see: van Koten, G.; Schaap, C. A.; Noltes, J. G. J. Organomet. Chem. 1975, 99, 157-170. For 10-Sn-5, see: van Koten, G.; Noltes, J. G.; Spek, A. L. J. Organomet. Chem. 1976, 118, 183-189. van Koten, G.; Noltes, J. G. J. Am. Chem. Soc. 1976, 98, 5393-5395. van Koten, G.; Jastrzebski, J. T. B. H.; Noltes, J. G.; Pontenagel, W. M. G. F.; Kroon, J.; Spek, A. L. J. Am. Chem. Soc. 1978, 100, 5021-5028. For 10-Ge-5, see: Breliere. C.; Carré, F.; Corriu, R. J. P.; de Saxcé, A.; Poirier, M.; Royo, G. J. Organomet. Chem. 1981, 205, C1-C3. For 10-Si-5, see: Corriu, R. J. P.; Kpoton, A.; Poirier, M.; Royo, G.; de Saxcé, A.; Young, J. C. J. Organomet. Chem. 1990, 395, 1-26. Corriu, R. J. P.; Royo, G.; de Saxcé, A. J. Chem. Soc., Chem. Commun. 1980, 892-894. Boyer, J.; Breière, C.; Carré, F.; Corriu, R. J. P.; Kpoton, A.; Poirier, M. Royo, G.; Young, J. C. J. Chem. Soc., Dalton Trans. 1989, 43-51. For 12-Si-6, see: Brelière, C.; Carré, F.; Corriu, R. J. P.; Douglas, W. E.; Poirier, M.; Royo, G.; Wong Chi Man, M. Organometallics 1992, 11, 1586-1593. For 12-P-6, see: Chuit, C.; Cornu, R. J. P.; Monforte, P.; Reyé, C.; Declereq, J.-P.; Dubourg, A. Angew. Chem., Int. Ed. Engl. 1993, 32, 1430-1432. For 10-Bi-4, see: Yamamoto, Y.; Chen, X.; Akiba, K.-y. J. Am. Chem. Soc. 1992, 114, 7906-7907. Yamamoto, Y.; Chen, X.; Kojima, S.; Ohdoi, K.; Kitano, M.; Doi, Y.; Akiba, K.-y. J. Am. Chem. Soc. 1995, 117, 3922-3932 (a similar 10-Sb-4 compound was also reported).
29. 2 can be used for the introduction of this ligand, by which a pentacoordinate tin compound was synthesized for the first time, see: van Koten, G.; Schaap, C. A.; Noltes, J. G. J. Organomet. Chem. 1975, 99, 157-170. For 10-Sn-5, see: van Koten, G.; Noltes, J. G.; Spek, A. L. J. Organomet. Chem. 1976, 118, 183-189. van Koten, G.; Noltes, J. G. J. Am. Chem. Soc. 1976, 98, 5393-5395. van Koten, G.; Jastrzebski, J. T. B. H.; Noltes, J. G.; Pontenagel, W. M. G. F.; Kroon, J.; Spek, A. L. J. Am. Chem. Soc. 1978, 100, 5021-5028. For 10-Ge-5, see: Breliere. C.; Carré, F.; Corriu, R. J. P.; de Saxcé, A.; Poirier, M.; Royo, G. J. Organomet. Chem. 1981, 205, C1-C3. For 10-Si-5, see: Corriu, R. J. P.; Kpoton, A.; Poirier, M.; Royo, G.; de Saxcé, A.; Young, J. C. J. Organomet. Chem. 1990, 395, 1-26. Corriu, R. J. P.; Royo, G.; de Saxcé, A. J. Chem. Soc., Chem. Commun. 1980, 892-894. Boyer, J.; Breière, C.; Carré, F.; Corriu, R. J. P.; Kpoton, A.; Poirier, M. Royo, G.; Young, J. C. J. Chem. Soc., Dalton Trans. 1989, 43-51. For 12-Si-6, see: Brelière, C.; Carré, F.; Corriu, R. J. P.; Douglas, W. E.; Poirier, M.; Royo, G.; Wong Chi Man, M. Organometallics 1992, 11, 1586-1593. For 12-P-6, see: Chuit, C.; Cornu, R. J. P.; Monforte, P.; Reyé, C.; Declereq, J.-P.; Dubourg, A. Angew. Chem., Int. Ed. Engl. 1993, 32, 1430-1432. For 10-Bi-4, see: Yamamoto, Y.; Chen, X.; Akiba, K.-y. J. Am. Chem. Soc. 1992, 114, 7906-7907. Yamamoto, Y.; Chen, X.; Kojima, S.; Ohdoi, K.; Kitano, M.; Doi, Y.; Akiba, K.-y. J. Am. Chem. Soc. 1995, 117, 3922-3932 (a similar 10-Sb-4 compound was also reported).
30. 2 can be used for the introduction of this ligand, by which a pentacoordinate tin compound was synthesized for the first time, see: van Koten, G.; Schaap, C. A.; Noltes, J. G. J. Organomet. Chem. 1975, 99, 157-170. For 10-Sn-5, see: van Koten, G.; Noltes, J. G.; Spek, A. L. J. Organomet. Chem. 1976, 118, 183-189. van Koten, G.; Noltes, J. G. J. Am. Chem. Soc. 1976, 98, 5393-5395. van Koten, G.; Jastrzebski, J. T. B. H.; Noltes, J. G.; Pontenagel, W. M. G. F.; Kroon, J.; Spek, A. L. J. Am. Chem. Soc. 1978, 100, 5021-5028. For 10-Ge-5, see: Breliere. C.; Carré, F.; Corriu, R. J. P.; de Saxcé, A.; Poirier, M.; Royo, G. J. Organomet. Chem. 1981, 205, C1-C3. For 10-Si-5, see: Corriu, R. J. P.; Kpoton, A.; Poirier, M.; Royo, G.; de Saxcé, A.; Young, J. C. J. Organomet. Chem. 1990, 395, 1-26. Corriu, R. J. P.; Royo, G.; de Saxcé, A. J. Chem. Soc., Chem. Commun. 1980, 892-894. Boyer, J.; Breière, C.; Carré, F.; Corriu, R. J. P.; Kpoton, A.; Poirier, M. Royo, G.; Young, J. C. J. Chem. Soc., Dalton Trans. 1989, 43-51. For 12-Si-6, see: Brelière, C.; Carré, F.; Corriu, R. J. P.; Douglas, W. E.; Poirier, M.; Royo, G.; Wong Chi Man, M. Organometallics 1992, 11, 1586-1593. For 12-P-6, see: Chuit, C.; Cornu, R. J. P.; Monforte, P.; Reyé, C.; Declereq, J.-P.; Dubourg, A. Angew. Chem., Int. Ed. Engl. 1993, 32, 1430-1432. For 10-Bi-4, see: Yamamoto, Y.; Chen, X.; Akiba, K.-y. J. Am. Chem. Soc. 1992, 114, 7906-7907. Yamamoto, Y.; Chen, X.; Kojima, S.; Ohdoi, K.; Kitano, M.; Doi, Y.; Akiba, K.-y. J. Am. Chem. Soc. 1995, 117, 3922-3932 (a similar 10-Sb-4 compound was also reported).
31. 2 can be used for the introduction of this ligand, by which a pentacoordinate tin compound was synthesized for the first time, see: van Koten, G.; Schaap, C. A.; Noltes, J. G. J. Organomet. Chem. 1975, 99, 157-170. For 10-Sn-5, see: van Koten, G.; Noltes, J. G.; Spek, A. L. J. Organomet. Chem. 1976, 118, 183-189. van Koten, G.; Noltes, J. G. J. Am. Chem. Soc. 1976, 98, 5393-5395. van Koten, G.; Jastrzebski, J. T. B. H.; Noltes, J. G.; Pontenagel, W. M. G. F.; Kroon, J.; Spek, A. L. J. Am. Chem. Soc. 1978, 100, 5021-5028. For 10-Ge-5, see: Breliere. C.; Carré, F.; Corriu, R. J. P.; de Saxcé, A.; Poirier, M.; Royo, G. J. Organomet. Chem. 1981, 205, C1-C3. For 10-Si-5, see: Corriu, R. J. P.; Kpoton, A.; Poirier, M.; Royo, G.; de Saxcé, A.; Young, J. C. J. Organomet. Chem. 1990, 395, 1-26. Corriu, R. J. P.; Royo, G.; de Saxcé, A. J. Chem. Soc., Chem. Commun. 1980, 892-894. Boyer, J.; Breière, C.; Carré, F.; Corriu, R. J. P.; Kpoton, A.; Poirier, M. Royo, G.; Young, J. C. J. Chem. Soc., Dalton Trans. 1989, 43-51. For 12-Si-6, see: Brelière, C.; Carré, F.; Corriu, R. J. P.; Douglas, W. E.; Poirier, M.; Royo, G.; Wong Chi Man, M. Organometallics 1992, 11, 1586-1593. For 12-P-6, see: Chuit, C.; Cornu, R. J. P.; Monforte, P.; Reyé, C.; Declereq, J.-P.; Dubourg, A. Angew. Chem., Int. Ed. Engl. 1993, 32, 1430-1432. For 10-Bi-4, see: Yamamoto, Y.; Chen, X.; Akiba, K.-y. J. Am. Chem. Soc. 1992, 114, 7906-7907. Yamamoto, Y.; Chen, X.; Kojima, S.; Ohdoi, K.; Kitano, M.; Doi, Y.; Akiba, K.-y. J. Am. Chem. Soc. 1995, 117, 3922-3932 (a similar 10-Sb-4 compound was also reported).
32. 2 can be used for the introduction of this ligand, by which a pentacoordinate tin compound was synthesized for the first time, see: van Koten, G.; Schaap, C. A.; Noltes, J. G. J. Organomet. Chem. 1975, 99, 157-170. For 10-Sn-5, see: van Koten, G.; Noltes, J. G.; Spek, A. L. J. Organomet. Chem. 1976, 118, 183-189. van Koten, G.; Noltes, J. G. J. Am. Chem. Soc. 1976, 98, 5393-5395. van Koten, G.; Jastrzebski, J. T. B. H.; Noltes, J. G.; Pontenagel, W. M. G. F.; Kroon, J.; Spek, A. L. J. Am. Chem. Soc. 1978, 100, 5021-5028. For 10-Ge-5, see: Breliere. C.; Carré, F.; Corriu, R. J. P.; de Saxcé, A.; Poirier, M.; Royo, G. J. Organomet. Chem. 1981, 205, C1-C3. For 10-Si-5, see: Corriu, R. J. P.; Kpoton, A.; Poirier, M.; Royo, G.; de Saxcé, A.; Young, J. C. J. Organomet. Chem. 1990, 395, 1-26. Corriu, R. J. P.; Royo, G.; de Saxcé, A. J. Chem. Soc., Chem. Commun. 1980, 892-894. Boyer, J.; Breière, C.; Carré, F.; Corriu, R. J. P.; Kpoton, A.; Poirier, M. Royo, G.; Young, J. C. J. Chem. Soc., Dalton Trans. 1989, 43-51. For 12-Si-6, see: Brelière, C.; Carré, F.; Corriu, R. J. P.; Douglas, W. E.; Poirier, M.; Royo, G.; Wong Chi Man, M. Organometallics 1992, 11, 1586-1593. For 12-P-6, see: Chuit, C.; Cornu, R. J. P.; Monforte, P.; Reyé, C.; Declereq, J.-P.; Dubourg, A. Angew. Chem., Int. Ed. Engl. 1993, 32, 1430-1432. For 10-Bi-4, see: Yamamoto, Y.; Chen, X.; Akiba, K.-y. J. Am. Chem. Soc. 1992, 114, 7906-7907. Yamamoto, Y.; Chen, X.; Kojima, S.; Ohdoi, K.; Kitano, M.; Doi, Y.; Akiba, K.-y. J. Am. Chem. Soc. 1995, 117, 3922-3932 (a similar 10-Sb-4 compound was also reported).
33. Kawashima, T.; Okazaki, R. Synlett 1996, 600-608 and references cited therein. For pentacoordinate 1,2-azaphosphetidines, see: Kawashima, T.; Soda, T.; Okazaki, R. Angew. Chem., Int. Ed. Engl. 1996, 35, 1096-1098. For pentacoordinate 1,2-oxathietanes, see: Ohno, F.; Kawashima, T.; Okazaki, R. J. Am. Chem. Soc. 1996, 118, 697-698. Kawashima, T.; Ohno, F.; Okazaki, R.; Ikeda, H.; Inagaki, S. J. Am. Chem. Soc. 1996, 118, 12455-12456.
34. Kawashima, T.; Okazaki, R. Synlett 1996, 600-608 and references cited therein. For pentacoordinate 1,2-azaphosphetidines, see: Kawashima, T.; Soda, T.; Okazaki, R. Angew. Chem., Int. Ed. Engl. 1996, 35, 1096-1098. For pentacoordinate 1,2-oxathietanes, see: Ohno, F.; Kawashima, T.; Okazaki, R. J. Am. Chem. Soc. 1996, 118, 697-698. Kawashima, T.; Ohno, F.; Okazaki, R.; Ikeda, H.; Inagaki, S. J. Am. Chem. Soc. 1996, 118, 12455-12456.
35. Kawashima, T.; Okazaki, R. Synlett 1996, 600-608 and references cited therein. For pentacoordinate 1,2-azaphosphetidines, see: Kawashima, T.; Soda, T.; Okazaki, R. Angew. Chem., Int. Ed. Engl. 1996, 35, 1096-1098. For pentacoordinate 1,2-oxathietanes, see: Ohno, F.; Kawashima, T.; Okazaki, R. J. Am. Chem. Soc. 1996, 118, 697-698. Kawashima, T.; Ohno, F.; Okazaki, R.; Ikeda, H.; Inagaki, S. J. Am. Chem. Soc. 1996, 118, 12455-12456.
36. Kawashima, T.; Okazaki, R. Synlett 1996, 600-608 and references cited therein. For pentacoordinate 1,2-azaphosphetidines, see: Kawashima, T.; Soda, T.; Okazaki, R. Angew. Chem., Int. Ed. Engl. 1996, 35, 1096-1098. For pentacoordinate 1,2-oxathietanes, see: Ohno, F.; Kawashima, T.; Okazaki, R. J. Am. Chem. Soc. 1996, 118, 697-698. Kawashima, T.; Ohno, F.; Okazaki, R.; Ikeda, H.; Inagaki, S. J. Am. Chem. Soc. 1996, 118, 12455-12456.
37. Kawashima, T.; Iwama, N.; Okazaki, R. J. Am. Chem. Soc. 1992, 114, 7598-7599.
38. Kawashima, T.; Nishiwaki, Y.; Okazaki, R. J. Organomet. Chem. 1995, 499, 143-146.
39. Kawashima, T.; Iwama, N.; Okazaki, R. J. Am. Chem. Soc. 1993, 115, 2507-2508.
40. For Peterson reaction, see: Colvin, E. W. Silicon in Organic Synthesis; Butterworths: London, 1981; pp 141-152. Weber, W. P. Silicon Reagents for Organic Synthesis; Springer-Verlag: New York, 1983; pp 58-73. Ager, D. J. Synthesis 1984, 384-398. Ager, D. J. Org. React. (NY) 1990, 38, 1-223. For Peterson-type reactions, see: Kauffmann, T. Top. Curr. Chem. 1980, 92, 109-147. Kauffmann, T. Angew. Chem., Int. Ed. Engl. 1982, 21, 410-429. Pereyre, M.; Quintard, J.-P.; Rahm, A. Tin in Organic Synthesis; Butterworths: London, 1987; pp 176-177.
41. For Peterson reaction, see: Colvin, E. W. Silicon in Organic Synthesis; Butterworths: London, 1981; pp 141-152. Weber, W. P. Silicon Reagents for Organic Synthesis; Springer-Verlag: New York, 1983; pp 58-73. Ager, D. J. Synthesis 1984, 384-398. Ager, D. J. Org. React. (NY) 1990, 38, 1-223. For Peterson-type reactions, see: Kauffmann, T. Top. Curr. Chem. 1980, 92, 109-147. Kauffmann, T. Angew. Chem., Int. Ed. Engl. 1982, 21, 410-429. Pereyre, M.; Quintard, J.-P.; Rahm, A. Tin in Organic Synthesis; Butterworths: London, 1987; pp 176-177.
42. For Peterson reaction, see: Colvin, E. W. Silicon in Organic Synthesis; Butterworths: London, 1981; pp 141-152. Weber, W. P. Silicon Reagents for Organic Synthesis; Springer-Verlag: New York, 1983; pp 58-73. Ager, D. J. Synthesis 1984, 384-398. Ager, D. J. Org. React. (NY) 1990, 38, 1-223. For Peterson-type reactions, see: Kauffmann, T. Top. Curr. Chem. 1980, 92, 109-147. Kauffmann, T. Angew. Chem., Int. Ed. Engl. 1982, 21, 410-429. Pereyre, M.; Quintard, J.-P.; Rahm, A. Tin in Organic Synthesis; Butterworths: London, 1987; pp 176-177.
43. For Peterson reaction, see: Colvin, E. W. Silicon in Organic Synthesis; Butterworths: London, 1981; pp 141-152. Weber, W. P. Silicon Reagents for Organic Synthesis; Springer-Verlag: New York, 1983; pp 58-73. Ager, D. J. Synthesis 1984, 384-398. Ager, D. J. Org. React. (NY) 1990, 38, 1-223. For Peterson-type reactions, see: Kauffmann, T. Top. Curr. Chem. 1980, 92, 109-147. Kauffmann, T. Angew. Chem., Int. Ed. Engl. 1982, 21, 410-429. Pereyre, M.; Quintard, J.-P.; Rahm, A. Tin in Organic Synthesis; Butterworths: London, 1987; pp 176-177.
44. For Peterson reaction, see: Colvin, E. W. Silicon in Organic Synthesis; Butterworths: London, 1981; pp 141-152. Weber, W. P. Silicon Reagents for Organic Synthesis; Springer-Verlag: New York, 1983; pp 58-73. Ager, D. J. Synthesis 1984, 384-398. Ager, D. J. Org. React. (NY) 1990, 38, 1-223. For Peterson-type reactions, see: Kauffmann, T. Top. Curr. Chem. 1980, 92, 109-147. Kauffmann, T. Angew. Chem., Int. Ed. Engl. 1982, 21, 410-429. Pereyre, M.; Quintard, J.-P.; Rahm, A. Tin in Organic Synthesis; Butterworths: London, 1987; pp 176-177.
45. For Peterson reaction, see: Colvin, E. W. Silicon in Organic Synthesis; Butterworths: London, 1981; pp 141-152. Weber, W. P. Silicon Reagents for Organic Synthesis; Springer-Verlag: New York, 1983; pp 58-73. Ager, D. J. Synthesis 1984, 384-398. Ager, D. J. Org. React. (NY) 1990, 38, 1-223. For Peterson-type reactions, see: Kauffmann, T. Top. Curr. Chem. 1980, 92, 109-147. Kauffmann, T. Angew. Chem., Int. Ed. Engl. 1982, 21, 410-429. Pereyre, M.; Quintard, J.-P.; Rahm, A. Tin in Organic Synthesis; Butterworths: London, 1987; pp 176-177.
46. For Peterson reaction, see: Colvin, E. W. Silicon in Organic Synthesis; Butterworths: London, 1981; pp 141-152. Weber, W. P. Silicon Reagents for Organic Synthesis; Springer-Verlag: New York, 1983; pp 58-73. Ager, D. J. Synthesis 1984, 384-398. Ager, D. J. Org. React. (NY) 1990, 38, 1-223. For Peterson-type reactions, see: Kauffmann, T. Top. Curr. Chem. 1980, 92, 109-147. Kauffmann, T. Angew. Chem., Int. Ed. Engl. 1982, 21, 410-429. Pereyre, M.; Quintard, J.-P.; Rahm, A. Tin in Organic Synthesis; Butterworths: London, 1987; pp 176-177.
47. Kawashima, T.; Takami, H.; Okazaki, R. J. Am. Chem. Soc. 1994, 116, 4509-4510.
48. Ager, D. J. J. Org. Chem. 1984, 49, 168-170.
49. Generation of the dianion by reduction of bis(phenylthiomethyl)silanes with LiNaph followed by reaction with electrophiles was independently reported by Strohmann, see: Strohmann, C.; Lüdtke, S.; Wack, E. Chem. Ber. 1996, 129, 799-805.
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52. For silyl group migration from carbon to oxygen, see: Yamamoto, K.; Tomo, Y. Tetrahedron Lett. 1983, 24, 1997-2000. Sato, F.; Tanaka, Y.; Sato, M. J. Chem. Soc., Chem. Commun. 1983, 160-166. Wilson, S. R.; Georgiadis, G. M. J. Org. Chem. 1983, 48, 4143-4144. Yamamoto, K.; Kimura, T.; Tomo, Y. Tetrahedron Lett. 1985, 26, 4505-4508. Shinokubo, H.; Miura, K.; Oshima, K.; Utimoto, K. Tetrahedron Lett. 1993, 34, 1951-1954. Shinokubo, H.; Oshima, K.; Utimoto, K. Chem. Lett. 1995, 461-462.
53. For silyl group migration from carbon to oxygen, see: Yamamoto, K.; Tomo, Y. Tetrahedron Lett. 1983, 24, 1997-2000. Sato, F.; Tanaka, Y.; Sato, M. J. Chem. Soc., Chem. Commun. 1983, 160-166. Wilson, S. R.; Georgiadis, G. M. J. Org. Chem. 1983, 48, 4143-4144. Yamamoto, K.; Kimura, T.; Tomo, Y. Tetrahedron Lett. 1985, 26, 4505-4508. Shinokubo, H.; Miura, K.; Oshima, K.; Utimoto, K. Tetrahedron Lett. 1993, 34, 1951-1954. Shinokubo, H.; Oshima, K.; Utimoto, K. Chem. Lett. 1995, 461-462.
54. For silyl group migration from carbon to oxygen, see: Yamamoto, K.; Tomo, Y. Tetrahedron Lett. 1983, 24, 1997-2000. Sato, F.; Tanaka, Y.; Sato, M. J. Chem. Soc., Chem. Commun. 1983, 160-166. Wilson, S. R.; Georgiadis, G. M. J. Org. Chem. 1983, 48, 4143-4144. Yamamoto, K.; Kimura, T.; Tomo, Y. Tetrahedron Lett. 1985, 26, 4505-4508. Shinokubo, H.; Miura, K.; Oshima, K.; Utimoto, K. Tetrahedron Lett. 1993, 34, 1951-1954. Shinokubo, H.; Oshima, K.; Utimoto, K. Chem. Lett. 1995, 461-462.
55. For silyl group migration from carbon to oxygen, see: Yamamoto, K.; Tomo, Y. Tetrahedron Lett. 1983, 24, 1997-2000. Sato, F.; Tanaka, Y.; Sato, M. J. Chem. Soc., Chem. Commun. 1983, 160-166. Wilson, S. R.; Georgiadis, G. M. J. Org. Chem. 1983, 48, 4143-4144. Yamamoto, K.; Kimura, T.; Tomo, Y. Tetrahedron Lett. 1985, 26, 4505-4508. Shinokubo, H.; Miura, K.; Oshima, K.; Utimoto, K. Tetrahedron Lett. 1993, 34, 1951-1954. Shinokubo, H.; Oshima, K.; Utimoto, K. Chem. Lett. 1995, 461-462.
56. For silyl group migration from carbon to oxygen, see: Yamamoto, K.; Tomo, Y. Tetrahedron Lett. 1983, 24, 1997-2000. Sato, F.; Tanaka, Y.; Sato, M. J. Chem. Soc., Chem. Commun. 1983, 160-166. Wilson, S. R.; Georgiadis, G. M. J. Org. Chem. 1983, 48, 4143-4144. Yamamoto, K.; Kimura, T.; Tomo, Y. Tetrahedron Lett. 1985, 26, 4505-4508. Shinokubo, H.; Miura, K.; Oshima, K.; Utimoto, K. Tetrahedron Lett. 1993, 34, 1951-1954. Shinokubo, H.; Oshima, K.; Utimoto, K. Chem. Lett. 1995, 461-462.
57. Hudrlik, P. F.; Nagendrappa, G.; Kulkarni, A. K.; Hudrlik, A. M. Tetrahedron Lett. 1979, 2237-2240. Hudrlik, P. F.; Hudrlik, A. M.; Kulkarni, A. K. J. Am. Chem. Soc. 1982, 104, 6809-6811.
58. Hudrlik, P. F.; Nagendrappa, G.; Kulkarni, A. K.; Hudrlik, A. M. Tetrahedron Lett. 1979, 2237-2240. Hudrlik, P. F.; Hudrlik, A. M.; Kulkarni, A. K. J. Am. Chem. Soc. 1982, 104, 6809-6811.
59. Corey, E. J.; Seebach, D. J. Org. Chem. 1966, 31, 4097-4099.
60. Reich, H. J.; Dykstra, R. R. J. Am. Chem. Soc. 1993, 115, 7041-7042.
61. The parent peak of this alcohol was not observed, see: McCarthy, E. R. J. Org. Chem. 1966, 31, 2042-2045.