New face-to-face metallocene triads

Organometallics

Volumn 19, Issue 4, 2000, Pages 469-474

  Hudson, Richard D A ^a   Foxman, Bruce M ^a   Rosenblum, Myron ^a  

^a BRANDEIS UNIVERSITY   (United States)

Author keywords

[No Author keywords available]

Indexed keywords

EID: 0000128184     PISSN: 02767333     EISSN: None     Source Type: Journal    
DOI: 10.1021/om990750l     Document Type: Article

References (31)

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4. Rosenblum, M.; Nugent, H. M.; Jang, K.-S.; Labes, M. M.; Cahalane, W.; Klemarczyk, P.; Reiff, W. M. Macromolecules 1995, 28, 6330-6342. Hudson, R. D. A.; Foxman, B. M.; Rosenblum, M. Organometallics 1999, 18, 4098-4106.
5. The use of zinc reagent represents a significant improvement in these cyclopentadienyl coupling reactions, which have previously been carried out with less satisfactory copper reagents. Foxman, B. M.; Gronbeck, D. A.; Khruschova, N.; Rosenblum, M. J. Org. Chem. 1993, 58, 4078-4082.
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9. 8 under the best of conditions, yields mixtures of ferrocene and of mono- and dilithioferrocene, which complicates the purification procedure for 5. To obtain pure monolithioferrocene, using the Kagan procedure, it is necessary to transform the lithio salt to the trimethylstannyl derivative, purify it, and reconvert this to the lithio salt.
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