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11
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0030747009
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Polymeric silver(I) diaminocarbenes were also previously prepared by treatment of triazolium salts with silver(I) acetate in refluxing thf, see:
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Polymeric silver(I) diaminocarbenes were also previously prepared by treatment of triazolium salts with silver(I) acetate in refluxing thf, see: Guerret O., Solé S., Gornitzka H., Teichert M., Trinquier G., Bertrand G. J. Am. Chem. Soc. 119:1997;6668.
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Bertrand, G.6
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13
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0001474120
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Magill A.M., McGuinness D.S., Cavell K.J., Britovsek G.J.P., Gibson V.C., White A.J.P., Williams D.J., White A.H., Skelton B.W. J. Organomet. Chem. 617-618:2001;546.
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Gibson, V.C.5
White, A.J.P.6
Williams, D.J.7
White, A.H.8
Skelton, B.W.9
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14
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15
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0042771951
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See in reviews Refs. [1a] and [1b] and:
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See in reviews Refs. [1a] and [1b] and: Lappert M.F. J. Organomet. Chem. 358:1988;185.
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19
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0034742983
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The classical methods to obtained directly the salt 3e from the chiral diamine used to prepare the aminal 1 (Ref. [8]), using ethylformate or chloral, were not tested since we early noticed that this diamine is unreactive towards most of the aldehydes, except formaldehyde
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A. Alexakis, I. Aujard, J. Pytkowicz, S. Roland, P. Mangeney, J. Chem. Soc. Perkin Trans. I (2001) 949. The classical methods to obtained directly the salt 3e from the chiral diamine used to prepare the aminal 1 (Ref. [8]), using ethylformate or chloral, were not tested since we early noticed that this diamine is unreactive towards most of the aldehydes, except formaldehyde.
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21
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0041751022
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13C-NMR spectra with enough resolution and to measure its optical rotation. Moreover, elemental analysis of 3e performed on the same sample gave unreproductible results.
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13C-NMR spectra with enough resolution and to measure its optical rotation. Moreover, elemental analysis of 3e performed on the same sample gave unreproductible results.
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