Microwave assisted synthesis of the fragrant compound Calone 1951®

Tetrahedron Letters

Volumn 46, Issue 1, 2005, Pages 39-41

  Drevermann, Britta ^a   Lingham, Anthony ^a   Hügel, Helmut ^a   Marriott, Philip ^a  

^a RMIT UNIVERSITY   (Australia)

Author keywords

Calone 1951 ; Fragrant compound; Microwave irradiation

Indexed keywords

BENZENE DERIVATIVE; OZONE;

ARTICLE; CHEMICAL REACTION; MICROWAVE IRRADIATION; REACTION TIME; SYNTHESIS;

EID: 9944244578     PISSN: 00404039     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.tetlet.2004.11.045     Document Type: Article

References (18)

1. Gaudin, J. U.S. Patent 5, 990, 076, Nov 23, 1999; Chem. Abstr. 1999, 130, 227560
2. P. Lidström, J. Tierney, B. Wathey, and J. Westman Tetrahedron 57 2001 9225 9283
3. C.R. Strauss, and R.W. Trainor Aust. J. Chem. 48 1995 1665 1692
4. L. Perreux, and A. Loupy Tetrahedron 44 2001 9199 9223
5. G.V. Thanh, and A. Loupy Tetrahedron Lett. 44 2003 9091 9094
6. K.D. Raner, C.R. Strauss, R.W. Trainor, and J.S. Thorn J. Org. Chem. 60 1995 2456 2460
7. Microwave experiments were performed in a prototype microwave applicator 'MDV2.4' and 0-700 W variable power microwave source (2m172) provided on trial by Warlock Engineering: www.warlock.com.au/chemreactor.htm
8. D. Bogdal, J. Pielichowski, and K. Jascot Org. Prep. Proced. Int. 30 1998 427 432
9. Bogdal, D.; Pielichowski, J.; Boron, A. First International Electronic Conference on Synthetic Organic Chemistry (ECSOC-1) September 1-30, 1997
10. F. Li, Q. Wang, Z. Ding, and F. Tao Org. Lett. 5 2003 2169 2171
11. 3): δ (in ppm): 169.4, 169.2, 147.5, 145.5, 132.2, 122.5, 116.0, 115.5, 66.6, 66.2, 51.8, 51.8, 20.6; EIMS parent ion 268 m/z
12. A. Loupy, D. Monteux, A. Petit, J.M. Aizpurua, E. Dominguez, and C. Palomo Tetrahedron Lett. 37 1996 8177 8180
13. B. Rechsteiner, F. Texier-Boullet, and J. Hamelin Tetrahedron Lett. 34 1993 5071 5074
14. R.S. Varma, and D. Kumar Org. Lett. 1 1999 697 700
15. Beereboom, J. J.; Lyme, O.; Cameron, D. P.; Stephens, C. R. U.S. Patent 3, 517, 031, June 23, 1970; Chem. Abstr. 1970, 73, 56143
16. 3): δ (in ppm): 199.7, 199.6, 165.5, 165.5, 147.0, 146.6, 145.0, 144.8, 135.1, 133.7, 125.6, 124.2, 121.7, 121.2, 120.7, 120.3, 82.1, 81.8, 77.0, 76.6, 52.9, 52.9, 20.7, 20.6; EIMS parent ion 236 m/z
17. L.A. Paquette, and H. Wang J. Org. Chem. 61 1996 5352 5356
18. 3): (in ppm): 204.9, 147.9, 145.9, 133.7, 124.3, 121.1, 120.6, 75.7, 75.4, 20.5; EIMS parent ion 178 m/z