(4R,4aR,6S,7S,7aS)-6-Hydroxy-7-hydroxymethyl-4-methylperhydrocyclo-penta[c] pyran-1-one chloroform solvate from Valeriana laxiflora

Acta Crystallographica Section C: Crystal Structure Communications

Volumn 60, Issue 11, 2004, Pages

  Khera, Smriti ^a   Carducci, Michael D ^b   Gu, Jian Qiao ^a   Timmermann, Barbara N ^a  

^a UNIVERSITY OF ARIZONA COLLEGE OF MEDICINE   (United States)

^b University of Arizona   (United States)

Author keywords

[No Author keywords available]

Indexed keywords

APPROXIMATION THEORY; BIODIVERSITY; CONFORMATIONS; CRYSTALS; HYDROGEN BONDS; PROBLEM SOLVING;

BOND DISTANCES; CRYSTAL PACKING; HALF-CHAIR CONFORMATIONS; RING CONFORMATIONS;

DRUG DOSAGE;

(4R,4AR,6S,7S,7AS) 6 HYDROXY 7 HYDROXYMETHYL 4 METHYLPERHYDROCYCLOPENTA(C)PYRAN 1 ONE; (4R,4AR,6S,7S,7AS)-6-HYDROXY-7-HYDROXYMETHYL-4-METHYLPERHYDROCYCLOPENTA(C)PYRAN-1-ONE; CHLOROFORM; CYCLOPENTANE DERIVATIVE; PYRAN DERIVATIVE; SOLVENT; VALERIAN;

ARTICLE; CHEMICAL STRUCTURE; CHEMISTRY; HYDROGEN BOND; PLANT LEAF; PLANT ROOT; PLANT STEM; X RAY CRYSTALLOGRAPHY;

CHLOROFORM; CRYSTALLOGRAPHY, X-RAY; CYCLOPENTANES; HYDROGEN BONDING; MODELS, MOLECULAR; PLANT LEAVES; PLANT ROOTS; PLANT STEMS; PYRANS; SOLVENTS; VALERIAN;

VALERIANA;

EID: 9744276779     PISSN: 01082701     EISSN: None     Source Type: Journal    
DOI: 10.1107/S0108270104021511     Document Type: Article

References (14)

1. Bruker (1997). SAINT, SHELXTL and SMART. Versions 5.0. Bruker AXS Inc., Madison, Wisconsin, USA.
2. Cheung, K. K., Overton, K. H. & Sim, G. A. (1965). Chem. Commun. 24, 634-635.
3. Cohn, D. L., Bustreo, F. & Raviglione, M. C. (1997). Clin. Infect. Dis. 24 (Suppl. 1), S121-130.
4. Corbett, E., Watt, C., Walker, N., Maher, D., Williams, B., Raviglione, M. & Dye C. (2003). Arch. Intern. Med. 163, 1009-1021.
5. Eisenbraun, E. J., Browne, C. E., Eliel, E. L., Harris, D. L., Rahman, A. & van der Helme, D. (1981). J. Org. Chem. 46, 3302-3305.
6. Flack, H. D. (1983). Acta Cryst. A39, 876-881.
7. Flack, H. D. & Bernardinelli, G. (2000). J. Appl. Cryst. 33, 1143-1148.
8. Görbitz, C. H. (1999). Acta Cryst. B55, 1090-1098.
9. Gu, J.-Q., Wang, Y., Franzblau, S. G., Montenegro, G., Yang, D. & Timmermann, B. N. (2004). Planta Med. 70, 509-514.
10. Marini-Bettolo, G. B., Nicoletti, M., Messana, I. & Patamia, M. (1983). Tetrahedron, 39, 323-329.
11. Ohtani, I., Kusumi, T., Kashman, Y. & Kakisawa, H. (1991). J. Am. Chem. Soc. 113, 4092-4096.
12. Sheldrick, G. M. (1997). SHELXL97 and SHELXS97. University of Göttingen, Germany.
13. Sheldrick, G. M. (2003). SADABS. Version 2.03. Bruker AXS Inc., Madison, Wisconsin, USA.
14. World Health Organization (2003). Background Document Prepared for the Second Ad hoc Committee on the TB Epidemic. 18-19 September 2003, Montreux, Switzerland.