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3), to prevent base-catalyzed desilylation leading to explosive unprotected tetraethynylethene derivatives. But addition of HCl aq. to 1 caused its deterioration.
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2) for 3493 data (I > 2σ(I)) and 329 parameters. The disordered olefinic part was refined taking into account a minor component [C(01,02):C(01a, 02a) = 0.753 : 0.247].
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20
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