A solid-state NMR study of tungsten methyl group dynamics in [W(η 5-C 5Me 5)Me 4][PF 6]

Journal of the American Chemical Society

Volumn 118, Issue 24, 1996, Pages 5665-5671

  Maus, Douglas C ^a   Copié, Valérie ^a,c   Sun, Boqin ^a   Griffiths, Janet M ^a,b   Griffin, Robert G ^a   Luo, Shifang ^a,d   Schrock, Richard R ^a   Liu, Andrew H ^a,f   Seidel, Scott W ^a   Davis, William M ^a   Grohmann, Andreas ^a,e  

^a MASSACHUSETTS INSTITUTE OF TECHNOLOGY   (United States)

^b USA   (United States)

^c NATIONAL INSTITUTE OF DENTAL AND CRANIOFACIAL RESEARCH   (United States)

^d EXXONMOBIL UPSTREAM RESEARCH COMPANY   (United States)

^e UNIVERSITY OF ERLANGEN NUREMBERG   (Germany)

^f DUPONT COMPANY   (United States)

Author keywords

[No Author keywords available]

Indexed keywords

METAL COMPLEX; TUNGSTEN DERIVATIVE;

ARTICLE; DRUG STRUCTURE; NUCLEAR MAGNETIC RESONANCE;

EID: 8944223032     PISSN: 00027863     EISSN: None     Source Type: Journal    
DOI: 10.1021/ja960248h     Document Type: Article

References (34)

1. Smith, S. O.; Palings, I.; Copié, V.; Raleigh, D. P.; Courtin, J.; Pardoen, J. A.; Lugtenburg, J.; Mathies, R. A.; Griffin, R. G. Biochemistry 1987, 26, 1606.
2. Sefcik, M. D.; Schaefer, J.; Stejskal, E. O.; MacKay, R. A.; Ellena, J. F.; Dodd, S. W.; Brown, M. F. Biochem. Biophys. Res. Commun. 1983, 114, 1048.
3. Lewis, B. A.; Harbison, G. S.; Herzfeld, J.; Griffin, R. G. Biochemistry 1985, 24, 4671.
4. Lee, C. W. B. Ph.D. Thesis, Massachusetts Institute of Technology, 1990.
5. Griffiths, J. G.; Sun, B.; Lansbury, P. A.; Griffin, R. G. In preparation.
6. Liu, A. H.; Murray, R. C.; Dewan, J. C.; Santarsiero, B. D.; Schrock, R. R. J. Am. Chem. Soc. 1987, 109, 4282.
7. Kubácek, P.; Hoffmann, R.; Havlas, Z. Organometallics 1982, 1, 180.
8. Lerke, S. A.; Evans, D. H. J. Am. Chem. Soc. 1995, 117, 11768.
9. Brookhart, M.; Green, M. L. H.; Wong, L.-L. Prog. Inorg. Chem. 1988, 36, 1.
10. Schrock, R. R. In Reactions of Coordinated Ligands; Braterman, P. R., Ed.; Plenum: New York, 1986.
11. Green, M. L. H.; Hughes, A. K.; Popham, N. A.; Stephens, A. H. H.; Wong, L.-L. J. Chem. Soc., Dalton Trans. 1992, 3077.
12. Bielecki, A.; Burum, D. P. J. Magn. Reson. Ser. A 1995, 116, 215.
13. Wittebort, R. J.; Olejniczak, E. T.; Griffin, R. G. J. Chem. Phys. 1987, 86, 5411.
14. Long, J. R.; Sun, B. Q.; Bowen, A.; Griffin, R. G. J. Am. Chem. Soc. 1994, 116, 11950.
15. See, for example: Okuda, J.; Herdtweck, E.; Hermann, W. A. Inorg. Chem. 1988, 27, 1254.
16. Liu, A. H.; O'Regan, M. B.; Finch, W. C.; Payack, J. F.; Schrock, R. R. Inorg. Chem. 1988, 27, 3574.
17. O'Regan, M. B.; Liu, A. H.; Finch, W. C.; Schrock, R. R.; Davis, W. M. J. Am. Chem. Soc. 1990, 112, 4331.
18. Schrock, R. R.; Kolodziej, R. M.; Liu, A. H.; Davis, W. M.; Vale, M. G. J. Am. Chem. Soc. 1990, 112, 4338.
19. Glassman, T. E.; Liu, A. H.; Schrock, R. R. Inorg. Chem. 1991, 30, 4723.
20. Glassman, T. E.; Vale, M. G.; Schrock, R. R.; Kol, M. J. Am. Chem. Soc. 1993, 115, 1760.
21. Rothwell, W. P.; Waugh, J. S. J. Chem. Phys. 1981, 74, 2721.
22. Herzfeld, J.; Berger, A. E. J. Chem. Phys. 1980, 73, 6021.
23. Torchia, D. A.; Szabo, A. J. Magn. Reson. 1985, 64, 135.
24. Vold, R. R.; Vold, R. L. In Advances in Magnetic and Optical Resonance, Warren, W. S., Ed.; Academic Press, Inc.: New York, 1991; Vol. 16, p 85.
25. Hiyama, Y.; Roy, S.; Guo, K.; Butler, L. G.; Torchia, D. J. Am. Chem. Soc. 1987, 109, 2525.
26. Hoatson, G. L.; Vold, R. L.; Tse, T. Y. J. Chem. Phys. 1994, 100, 4756.
27. Wann, M.-H.; Harbison, G. S. J. Chem. Phys. 1994, 101, 231.
28. Dawoodi, Z.; Green, M. L. H.; Mtetwa, V. S. B.; Prout, K.; Schultz, A. J.; Williams, J. M.; Koetzle, T. F. J. Chem. Soc., Dalton Trans. 1986, 1629.
29. Calvert, R. B.; Shapley, J. R. J. Am. Chem. Soc. 1978, 100, 7726.
30. Beshah, K.; Olejniczak, E. T.; Griffin, R. G. J. Chem. Phys. 1987, 86, 4730.
31. Beshah, K.; Griffin, R. G. J. Magn. Reson. 1989, 84, 268.
32. Jordan, R. F.; Norton, J. R. J. Am. Chem. Soc. 1979, 101, 4853.
33. Lafleur, D.; Huang, Y.; Gilson, D. F. R.; Butler, I. S. J. Solid State Chem. 1994, 108, 99.
34. Schrock, R. R.; Sharp, P. R. J. Am. Chem. Soc. 1978, 100, 2389.