Thin-layer chromatography in clinical chemistry

Practical Thin-Layer Chromatography: A Multidisciplinary Approach

Volumn , Issue , 2017, Pages 131-152

  Jain, Raka ^a  

^a ALL INDIA INSTITUTE OF MEDICAL SCIENCES   (India)

Author keywords

[No Author keywords available]

Indexed keywords

BIOCHEMISTRY; CHROMATOGRAPHIC ANALYSIS; LABORATORIES;

CHROMATOGRAPHIC SYSTEMS; CLINICAL CHEMISTRY; COST OF OPERATIONS; LABORATORY EQUIPMENTS; SAMPLE APPLICATIONS; STATIONARY PHASIS; TECHNOLOGICAL ADVANCES;

THIN LAYER CHROMATOGRAPHY;

EID: 85052481886     PISSN: None     EISSN: None     Source Type: Book    
DOI: 10.1201/9780203742365     Document Type: Chapter

References (120)

1. Randerath, K., Thin Layer Chromatography, 2nd ed., Verlag Chemie, Weinheim, and Academic Press, New York, 1966.
2. Stahl, E., Thin Layer Chromatography, A Laboratory Handbook, 2nd ed., Springer-Verlag, New York, 1969.
3. Niederwieser, A. and Patakl, G., Eds., Progress in Thin Layer Chromatography and Related Methods, Vol. I, Ann Arbor-Humphrey Science Publishers, Ann Arbor and London, 1970.
4. Kaiser, R. E., in HPTLC - High Performance Thin Layer Chromatography, Zlatkis, A., and Kaiser, R. E., Eds., Elsevier/North Holland Biomedical Press, Amsterdam, 1977, p. 73.
5. Bertsch, W., Hara, S., Kaiser, R. E., and Zlatkis, A., Eds., Instrumental HPTLC, Dr. Alfred Heuthig Verlag, Heidelberg, 1980.
6. Dallas, F. A. A., Read, H., Ruane, R. J., and Wilson, I.D., Eds., Recent Advances in Thin Layer Chromatography, Plenum Press, New York, 1988.
7. Siouffi, A. M., Mincsovics, E., and Tyihak, E., Planar chromatographic techniques in biomedicine: current status, J. Chromatogr., 492, 471, 1981.
8. Wilson, I. D., Contemporary thin-layer chromatography: an introduction, in Recent Advances in Thin-Layer Chromatography, Dallas, F. A. A., Read, H., Ruane, R. J., and Wilson, I. D., Eds., Plenum Press, New York, 1988, Chap. 1.
9. McMurray, J. R., Collection of specimens, in Varley’s Practical Clinical Biochemistry, Gowenlock, A. H., Mc-Murray, J. R., and McLauchlan, D. M., Eds., Heinemann Medical Books, London, 1988, Chap. 14.
10. Pickard, M. A., Collection and handling of patient specimens, in Clinical Chemistry, Theory Analysis and Correlation, Kaplan, L. A., and Pesce, A. J., Eds., Mosby, St. Louis, 1989, Chap. 2.
11. Report of the Substance-Abuse Testing Committee, Critical Issues in Urinalysis of Abused Substances, Clin. Chem., 34, 605, 1988.
12. Jain, R., Interference of adulterants in thin layer chromatography method for drugs of abuse, Ind. J. Pharmacol., 25, 240, 1993.
13. Jain, R., Laboratory services for drug abuse screening in a clinical setting, J. Forensic, Med. Toxicol., x, 26, 1994.
14. Jain, R. and Ray, K., Detection of drugs of abuse and its relevance to clinical practice, Ind. J. Pharmacol., 21, 1995 (in press).
15. Harkey, M. R. and Stalowitz, M. L., Solid phase extraction techniques for biological specimens, in Advances in Analytical Toxicology, Baselt, R. C, Ed., Biomedical Publications, Foster City, CA, 1984, Chap. 9.
16. Mcdowall, R. D., Pearce, J. C, and Murkitt, G. S., Liquid-solid sample preparation in drug analysis, J. Pharm. Biomed. Anal., 4, 3, 1986.
17. Mcdowall, R. D., Sample preparation for biomedical analysis, J. Chromatogr., 492, 3, 1989.
18. Li, F., Lira, C. K., and Peters, T. J., A high performance liquid chromatographic method for the assay of coproporphyrinogen oxidase activity in rat liver, Biochem. J., 239, 481, 1986.
19. Kaiser, R. E., J. Planar Chromatogr.-Mod. TLC, 1, 182, 1988.
20. Quoted in Siouffi, A. M., Mincsovics, E., and Tyihak, E., Planar chromatographic techniques in biomedicine: current status, J. Chromatogr., 492, 471, 1989.
21. Johnson, E. K. and Nurok, D., Computer simulation as an aid to optimizing continuous development two-dimensional thin layer chromatography, J. Chromatogr., 302, 135, 1984.
22. Treiber, L. R., Quantitative Thin Layer Chromatography and Its Industrial Applications, Marcel Dekker, New York, 1987.
23. Poole, C. F., Poole., S. K., and Dean, T. A., Quantitative methods in thin-layer chromatography, in Recent Advances in Thin Layer Chromatography, Dallas, F. A. A., Read, H., Ruane, R. J. and Wilson, I. D., Eds., Plenum Press, New York, 1988, Chap. 2.
24. Baeyens, W. R. G. and Lin Ling, B., Thin layer chromatography application with fluorodensitometric detection, J. Planar Chromatogr.-Mod. TLC, 1, 198, 1988.
25. Poole, C. F., Poole, S. K., Dean, T. A., and Chirco, N. M., Sample requirements for quantitation in thin layer chromatography, J. Planar Chromatogr.-Mod. TLC, 2, 180, 1989.
26. Poole, C. F. and Poole, S. K., Progress in densitometry for quantitation in planar chromatography, J. Chromatogr., 492, 539, 1989.
27. Jork, H., in Proceedings IV Intl. Symp. Instrumental HPTLC, Traitler, H., Studer, R., Kaiser R. E., Eds., Institute for Chromatography, Bad Durkheim, F. R. G., 1987, p. 193.
28. Jaenchen, D. E., Instrument thin layer chromatography, state of the art and future trends, Internal. Analyst, 3, 36, 1987.
29. Wu, J. T., Screening for inborn errors of amino acid metabolism., Ann. Clin. Lab. Sci, 21, 123, 1991.
30. Edwards, M. A., Grant, S., and Green, A., A practical approach to the investigation of amino acid disorders, Ann. Clin. Biochem., 25, 129, 1988.
31. Silverman, L. M. and Christenson, R. H., Amino acids and proteins, in Tietz Textbook of Clinical Chemistry, Burtis, C. A., and Ashwood, E. R., Eds., W. B. Saunders, Philadelphia, 1994, Chap. 19.
32. Varley, H., Amino acids, in Varley’s Practical Clinical Biochemistry, Gowenlocks, A. H., McMurray, J. R., and McLauchlan, D. M., Eds., Heinemann Medical Books, London, 1988, Chap. 18.
33. Street, J. M., Trafford. D. J. H., and Makin, H. L. J., The quantitative estimation of bile acids and their conjugates in human biological fluids, J. Lipid Res., 24, 491, 1983.
34. Kindel, M., Ludwig-Koehn, H., and Lembcke, M., New and versatile method for the determination of faecal bile acids by thin layer chromatography with direct scanning fluorimetry, J. Chromatogr., 497, 139, 1989.
35. Ferreira, H. C. S. and Elliott, W. H., Pre-column derivatization of free bile acids for high performance liquid chromatographic and gas chromatographic-mass spectrometric analysis, J. Chromatogr., 562, 697, 1991.
36. Iida, T., Moinose, T., Shinohara, T., Goto, J., Nambara, T., and Chang, F. C., Separation of alio bile acid stereoisomers by thin layer and high performance liquid chromatography, J. Chromatogr., 366, 396, 1986.
37. Vaden Ende, A., Radecker, C. E., and Mairuhu, W. M., Microanalysis of free and conjugated bile acids by thin-layer chromatography and in situ spectrofluorimetry, Anal. Biochem., 134, 153, 1983.
38. Klaus, R., Procedures for quantitative high pressure liquid chromatographic analysis of nonfluorescing compounds with bile acids as an example, J. Chromatogr., 333, 276, 1985.
39. Roberts, K. and Whitelaw, M., Chromatography of monosaccharides and disaccharides, J. Chromatogr., 373, 81, 1986.
40. Flick, J. A., Schnaar, R. L., and Perman, J. A., Thin layer chromatographic determination of urinary excretion of lectulose, simplified and applied to cystic fibrosis patients, Clin. Chem., 3317, 1211, 1987.
41. Menzies, I. S., Mount, J. N., and Wheeler, J. N., Quantitative estimation of clinically important monosaccharides in plasma by rapid thin layer chromatography, Ann. Clin. Biochem., 15, 65, 1978.
42. Blom, W., Luteyn, J. C, Hkelholt-Dijkman, H., Huismans, J. B., and Loonen, M. C. B., Thin layer chromatography of oligosaccharides in urine as a rapid indication for the diagnosis of lysosomal and maltose deficiency (Pompes’ disease), Clin. Chim. Acta., 134, 221, 1983.
43. Humbel, R. and Collart, M., Oligasaccharides in urine of patients with glycoprotein storage diseases. I. Rapid detection by thin-layer chromatography, Clin. Chim. Acta, 60, 143, 1975.
44. Sewell, A. C., An improved thin layer chromatographic method for urinary oligosaccharide screening, Clin. Chim. Acta, 92, 411, 1979.
45. Friedman, R. B., Williams, M. A., Moser, H. W., and Kolodny, E. H., Improved thin layer chromatography method in the diagnosis of mannosidosis, Clin. Chem., 24, 1576, 1978.
46. Midland, J. D. and Jones, D. W., Thin layer chromatographic screening procedure for broad spectrum drug detection, Am. Lab., 12, 104, 1980.
47. Lillsunde, P. and Korte, J., Comprehensive drug screen in urine using solid-phase extraction and combined TLC and GC/MS identification, J. Anal. Toxicol., 15, 71, 1991.
48. Singh, A. K., Granley, K., Ashraf, M., and Mishra, U., Drug screening and confirmation by thin layer chromatography, J. Planar Chromatogr.-Mod. TLC, 3411, 1989.
49. Jain, N. C., Forensic toxicology: general unknown, in Developments in Analytical Methods in Pharmaceutical, Biomedical and Forensic Sciences, Piemonte, G., Tagliaro, F., Marigo, M., and Frigerio, A., Eds., Plenum Press, New York, 1987, p. 51.
50. Maickel, R. P., Procedures for the isolation of organic compounds from biological materials, in Guidelines for Analytical Toxicology Programs, Vol. I, Thoma, J. J., Bando, P. B., and Sunshine, I., Eds., CRC Press, Cleveland, Ohio, 1977, p. 189.
51. Gorodetzky, C. H. W., Detection of drugs of abuse in biological fluids, in Handbook of Experimental Pharmacology, Drug Addiction, Vol. II, Martin, W. R., Ed., Springer-Verlag, New York, 1977, Chap. 6.
52. Davidow, B., Petri, L. N., Quame, B., Searle, B., Fastlich, E., and Sovitzky, J., A thin layer chromatographic screening test for the detection of users of morphine or heroin, Am. J. Clin. Path., 46, 5a8, 1966.
53. Nishigami, J., Okshima, T., Takayasu, T., Kondo, T., Lin, Z., and Nagaro, T., Forensic toxicological application of Toxi-lab screening for biological specimens in autopsy and emergency cases., Nippon-Hoigaku-Zasshi, 47, 372, 1993.
54. Wolf, k., Sanderson, M. J., Hay, A. W., and Barnes, I., An evaluation of the measurement of drugs of abuse by commercial and in-house horizontal layer chromatography, Ann. Clin. Biochem., 30, 163, 1993.
55. Vinson, J. A. and Patel, A. M., Detection and quantitation of tetrahydrocannabinol in serum using thin-layer chromatography and fluorometry, J. Chromatogr., 307, 493, 1984.
56. Vinson, J. A. and Lofatofsky, D. J., A semi-automated extraction and spotting system for drug analysis by TLC: procedure for analysis of the major metabolite of 9-tetrahydrocannabinol in urine, J. Anal. Toxicol., 9, 6, 1985.
57. Jain, R., Determination of buprenorphine and its N-dealkylated metabolite in urine by TLC densitometry, Ind. J. Pharmacol., 26, 288, 1994.
58. Jain, R., Simultaneous determination of diazepam and its metabolites in urine by thin-layer chromatography and direct densitometry, J. Chromatogr., 615, 365, 1993.
59. Inouc. T. and Ni Waguchi, T., Determination of nitrazepam and its main metabolites in urine by thin-layer chromatography and direct densitometry, J. Chromatogr., 339, 163, 1985.
60. Delia Lasa, E. and Martone, G., A quantitative determination of heroin and cocaine samples by high performance thin layer chromatography, Forensic Sci. Int., 32, 117, 1986.
61. Fenimore, D. C, Meyer, C. J., Davis, C. M., Hsu, F., and Zlatkes, A., High performance thin layer chromatographic determination of psychopharmacologic agents in blood serum, J. Chromatogr., 142, 399, 1977.
62. Fenimore, D. C, Davis, C. M., and Meyer, C. J., Determination of drugs in plasma by high performance thin layer chromatography, Clin. Chem., 24, 1386, 1978.
63. Reimer, G. J. and Suraz, A., Development of a screening method for five sulfonamides in salmon muscle tissue using thin-layer chromatography, J. Chromatogr., 555. 315, 1991.
64. Chiong, D. M., Consegrao-Rodriguez, E., and Aimirall, J. R., The analysis and identification of steroids, J. Forensic Sci., 37, 488, 1992.
65. Oka, A., Ikai, V., Hayakawa, J., Masudo, K., Harada, K., and Suzaki, M., Improvement of chemical analysis of antibiotics. Part XIX: Determination of tetracycline antibiotics in milk by liquid chromatography and thin-layer chromatography/fast atom mass spectrometry, J. AOAC. Int., 11, 891, 1994.
66. Kuksis, A., Chromatography in Biomedical Research and Clinical Diagnostics, Journal of Chromatography Library, Vol. 37, Elsevier, Amsterdam, 1987.
67. Kuksis, A. and Myher, J. J., Lipids and their constituents, J. Chromatogr., 379, 57. 1986.
68. Folch, J. M., Lees, M., and Sloane-Stanley, C. H., A simple method for the isolation and purification of total lipids from animal tissues, J. Biol. Chem., 226, 497, 1957.
69. Nelson, G. J., in Nelson, G. J., Ed., Blood and Lipoproteins-Quantitation, Composition and Metabolism. Wiley, New York, 1972, p. 3.
70. Mitchell, R. H., Hawthorne, J. N., Coleman, R., and Karnosky, M. L., Extraction of polyphosphoinositides with neutral and acidified solvents - a comparison of guinea-pig brain and liver and measurement of rat liver inositol compounds which are resistant to extraction, Biochem. Biophys. Acta, 210, 86, 1970.
71. Christie, W. W., Extraction and hydrolysis of lipids and some reactions of their fatty acid components, in CRC Handbook of Chromatography, Lipids, Vol. 1., Mangold, H. K., Zweig. G., and Sherma, J., Eds., CRC Press, Boca Raton, 1984, Chap. 2.
72. Bounias, M., Analyse Biochimique Quantitiative par Nanochromatograplue en Couches Minces, Masson, Paris, 1983, p. 83.
73. Bhat, H. K. and Ansari, G. A. S., Improved separation of lipid esters by thin-layer chromatography, J. Chromatogr., 483, 369, 1989.
74. Yao, J. K. and Rasteller, G. M., Microanalysis of complex tissue lipids by high-performance thin layer chromatography, Anal. Biochem. 150, 111, 1985.
75. Schmitz, G., Assmann, G., and Bowyer, D. E., A quantitative densitometric method for the rapid separation and quantitation of the major tissue and lipoprotein lipids by high performance thin layer chromatography. I. Sample preparation, chromatography and densitometry, J. Chromatrogr., 307, 65, 1984.
76. Peters, T. J. and Cairns, S. K., Analysis and subcellular localization of lipid in alcoholic liver disease, Alcohol, 2, 447, 1985.
77. Edouard, L., Doucel, F., Buxtof, J. C, and Beaumont, J. L., Quantitative determination of free cholesterol and cholesteryl esters in skin biopsies, Clin. Physiol. Biochem., 3, 323, 1981.
78. Saint Leger, D. and Bague, A., A simple and accurate rapid procedure for qualitative analysis of skin surface lipids (SSL) in man, Arch. Dermatol. Res., 271, 215, 1981.
79. Jacobsen, E., Stewart, M. E., and Dowing, D. T., Age related changes in sebaceous wax ester secretion rates in men and women, J. Invest. Dermatol., 85, 483.
80. Ohta, A., Mayo, M. C, Kramer, N., and Lands, W. E., Rapid analysis of fatty acids in plasma lipids, Lipids, 25, 742, 1990.
81. Spillman, T. and Cotton, D. B., Current perspectives in assessment of fetal pulmonary surfactant status with amniotic fluid, Crit. Rev. Clin. Lab. Sci, 27, 345, 1989.
82. Serranto, de la., Cruz, D., Santillana, E., Mingo, A., Fuenmayor, G., Pantoja, A., and Fernandez, K., Improved thin layer chromatographic determination of phospholipids in gastric aspirate from newborns, for assessment of lung maturity, Clin. Chem., 34, 736, 1988.
83. Toso F. H. and Zachman, R. D., Use of quantitative amniotic fluid phosphatidyl glycerol as a criterion for fetal lung maturation, Am. J. Perinatal., 9, 34, 1992.
84. Gluck, L. and Kulovich, M. V., Lecithin-sphingomyelin ratio in amniotic fluid in normal and abnormal pregnancy, Am. J. Obstet. Gynecol, 115, 539, 1973.
85. Gluck, L., Kulovich, M. V., and Borer, R. C., Jr., The diagnosis of the respiratory distress syndrome by amniocentesis, Am. J. Obstet. Gynecol, 109, 440, 1972.
86. Kolins, M. D., Epstein, E., Civin, W. H., and Weiner, S., Amniotic fluid phospholipids measured by continuous development thin layer chromatography, Clin. Chem., 26, 403, 1980.
87. Touchstone, J. C. and Alvarez, J. G., Separation of acidic and neutral glycolipids by diphasic thin-layer chromatography, J. Chromatogr., 436, 515, 1988.
88. Freer, D. E. and Statland, B. E., Measurement of amniotic fluid surfactant, Clin. Chem., 27, 1629, 1981.
89. Blass, K. G. and Ho, C. S., Sensitive and highly reproducible qualitative fluorescent thin layer chromatographic visualization technique for lecithin and sphingomyelin, J. Chromatogr., 208, 170, 1981.
90. Colarow, L., Quantitation of phospholipid classes on thin layer plates with a fluorescence reagent in the mobile phase, J. Planar Chromatogr.-Mod. TLC, 2, 19, 1989.
91. Ojima-Uchiyama, A., Masuzawa, V., Sugiura, T., Waka, K., Saito, H., Yui, Y., and Tomioka, H., Phospholipid analysis of human eosinophils: high levels of alkyl acyl glycerophosphocholine (PAF precursor), Lipids, 23, 815, 1988.
92. Narayan, P. and Dahiya, R., Alteration in sphingomyelin and fatty acids in human benign prostatic hyperplasia and prostatic cancer, Biomed. Biochim. Acta, 50, 1099, 1991.
93. Dembitsky, V. M., Quantification of plasmalogens, alkylacyl and diacyl glycerophospholipids by micro thin layer chromatography, J. Chromatogr., 436, 467, 1988.
94. Cartwright, I. J., Separation and analysis of phospholipids by thin layer chromatography, Methods Mol. Biol, 19, 153, 1993.
95. Gregson, N. A., The extraction and analysis of glycosphingolipids, Methods. Mol. Biol, 19, 287, 1993.
96. Raajmakers, J. G. A. M., System for the identification for novel prostaglandins, J. Chromatogr., 138, 355, 1977.
97. Tsunamoto, K., Todo, S., and Ismashuku, S., Separation of prostaglandins and thromboxane by two-dimensional thin layer chromatography, J. Chromatogr., 417, 414, 1987.
98. Beneytout, J., Grenrt, D., and Tixer, M., J. High Resolut. Chromatogr. Chromatogr. Commun., 7, 211, 1984.
99. quoted in Siouffi, A.M., Mincsovics, E., and Tyihak, E., Planar chromatographic techniques in biomedicine: current status, J. Chromatogr., 492, 471, 1989.
100. Herman, C. A., Hamberg, M., and Granstram, L., Quantitative determination of prostaglandins El, E2, and E3 in frog tissue, J. Chromatogr., 394, 353, 1987.
101. Goswami, S. K. and Kinsellas J. E., A nondestructive spray reagent for the detection of prostaglandins and other lipids on thin layer chromatography, Lipids, 16, 759, 1981.
102. Riutta, A., Seppala, E., and Vapaatalo, H., A rapid, sensitive method for detecting different arachidonic acid metabolites by thin layer chromatography: the use of autoradiography, J. Chromatogr., 307, 185, 1985.
103. Jacob, K. and Lappa, P., Application of ion pair high performance liquid chromatography to the analysis of porphyrins in clinical samples, Biomed. Chromatogr., 5, 122, 1991.
104. Petryka, Z. J., Porphyrins in densitometry, in Thin Layer Chromatography, Practice and Application. Touchstone, J. C. and Sherma, J., Eds., Wiley-Interscience, New York, 1979, Chap. 24.
105. Heftman, E., Chromatography of Steroids, Elsevier, Amsterdam, 1976.
106. Touchstone, J. C., CRC Handbook of Chromatography-Steroids, Zweig, G. and Sherma, J., Eds., CRC Press, Boca Raton, FL, 1986.
107. Lamparczyk, H., in Handbook of Chromatography, Analysis and Characterization of Steroids, Sherma, J., Ed., CRC Press, Boca Raton, FL, 1992.
108. Sherma, J. and Fried, B., Eds., Handbook of Thin Layer Chromatography, Marcel Dekker, New York, 1991, p. 1047.
109. Lamparczyk, H., Chromatographic techniques used in steroid analysis, in Handbook of Chromatography-Analysis and Characterization of Steroids, Sherma, J., Ed., CRC Press, Boca Raton, FL, 1992, Chap. 3.
110. Vanlook, L., Deschuytere, Ph., and Van Peteghem, C., Thin layer chromatographic method for the detection of anabolics in fatty tissues, J. Chromatogr., 489, 213, 1989.
111. Brown, J. W., Carballeria, A., and Fishman, L. M., Rapid two-dimensional thin layer chromatographic system for the separation of multiple steroids of secretary and neuroendocrine interest, J. Chromatogr., 439, 441, 1988.
112. Watkins, T. R., Smith, A., and Touchstone, J. C., Reversed-phase thin layer chromatography of estrogen glucu-ronides, J. Chromatogr., 374, 221, 1986.
113. Curtius, H. C. and Muller, M., Combination of gas chromatography and thin layer chromatography in steroid investigations, J. Chromatogr., 32, 222, 1968.
114. Kraft, R., Otto, A., Makower, A., and Etzold, G., Combined thin-layer chromatography/mass spectrometry without substance elution: use for direct identification of phenols, steroids, nucleosides, biogenic amines and amino acids, Anal. Biochem., 113, 193, 1981.
115. Kono, K., Tschida, T., Kern, D. H., and Irie, R., Ganglioside composition of human melanoma and response to anti-tumor treatment, Cancer Invest., 8, 161, 1990.
116. Merritt, W. D., Der-Minassian, V., and Reaman, G. H., Increased GD3 gangliosides in plasma with children with T-cell and lyphoplastic leukemia, Leukemia, 85, 816, 1994.
117. Nakakuma, H., Horikawa, H., Kawaguchi, T., Hidaka, M., Nagakura, S., Hirari, S., Kageshita, I., Ono, I., Kageshita, I., and Iwamori, M., Common phenotypic expression of gangliosides GH3 and GD3 in normal human tissues and neoplastic skin lesion, Jpn. J. Clin. Oncol., 22, 308, 1992.
118. 2Cer, J. Chromatogr., 426, 183, 1988.
119. Alemany, G., Nicolav, M. C, Gamundi. A., and Rial, R., Thin layer chromatographic determination of brain catecholamine and 5-hydroxy tryptamine, Biomed. Chromatogr., 7, 315, 1993.
120. Lee, B. Y. and Thurmon, T. F., Compact gas chromatography used with thin layer chromatography for assessment of abnormalities of organic acids, Clin. Chim. Acta, 218, 215, 1993.