Microwave assisted high yielding preparation of N-protected 2′-deoxyribonucleosides useful for oligonucleotide synthesis

Nucleosides, Nucleotides and Nucleic Acids

Volumn 21, Issue 4-5, 2002, Pages 393-400

  Rao, N S ^a   Kumar, P ^a   Chauhan, V K ^a   Garg, B S ^b   Gupta, K C ^a  

^a CSIR INSTITUTE OF GENOMICS AND INTEGRATIVE BIOLOGY   (India)

^b UNIVERSITY OF DELHI   (India)

Author keywords

[No Author keywords available]

Indexed keywords

DEOXYRIBONUCLEOSIDE; OLIGONUCLEOTIDE; DEOXYCYTIDINE;

ARTICLE; DNA SYNTHESIS; MATRIX ASSISTED LASER DESORPTION IONIZATION TIME OF FLIGHT MASS SPECTROMETRY; MICROWAVE RADIATION; PRECURSOR; PROTON NUCLEAR MAGNETIC RESONANCE; SYNTHESIS; CHEMICAL MODEL; HYDROLYSIS; KINETICS; MASS SPECTROMETRY; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY;

DEOXYCYTIDINE; DEOXYRIBONUCLEOSIDES; HYDROLYSIS; KINETICS; MAGNETIC RESONANCE SPECTROSCOPY; MICROWAVES; MODELS, CHEMICAL; SPECTROMETRY, MASS, MATRIX-ASSISTED LASER DESORPTION-IONIZATION;

EID: 85047684288     PISSN: 15257770     EISSN: None     Source Type: Journal    
DOI: 10.1081/NCN-120006833     Document Type: Article

References (15)

1. The Stepwise Synthesis of Specific Deoxyribopolynucleotides. Protected Derivatives of Deoxyribonucleosides and New Syntheses of Deoxyribonucleoside-3′ Phosphates
2. Total Synthesis of the Structural Gene foe an Alanine Transfer Ribonucleic Acid from Yeast. Chemical Synthesis of an Icosadeoxyribonucleotide Corresponding to the Nucleotide Sequence 21 to 40
3. Transient Protection: Efficient One Flask Synthesis of Protected Deoxynucleosides
4. 2-(2-methylpropanol)-2′-deoxyguanosine
5. Alumina-mediated Microwave Thermolysis: A New Approach to Deprotection of Benzyl Esters
6. Alumina-mediated Deacetylation of Benzaldehyde Diacetates-A Simple Deprotection Method
7. Microwave-assisted Synthesis of S-trityl and S-acylmercapothexanol and Their Deprotection
8. Microwave Assisted Rapid and Clean Deprotection of Oligodeoxynucleotides
9. Hydrolysis of Adenosine Triphosphate by Conventional or Microwave Heating
10. Synthesis in Dry Media Coupled with Microwave Irradiation: Application to the Preparation of β-amino Esters and β-lactams via Silyl Keten Acetals and Aldimines
11. New Solvent-free Organic Synthesis Using Focused Microwaves
12. Microwave Assisted Organic Reactions
13. Liquid Crystalline 5,6-O-acetals of L-galactono-1,4-lactone Prepared by Microwave Irradiation on Montmorillonite
14. Solid-liquid Phase Transfer Catalysis Without Solvent Coupled with Microwave Irradiation: A Quick and Efficient Method for Saponification of Esters