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Volumn 56, Issue 21, 2000, Pages 3425-3437

Synthesis of thiabicyclic heterocycles through free radical cyclization of β-thioacrylates

Author keywords

Cyclization; Radicals and radical reactions; Sulfoxides; Sulfur heterocycles

Indexed keywords

ACRYLIC ACID DERIVATIVE; FREE RADICAL; HETEROCYCLIC COMPOUND; SULFOXIDE; SULFUR DERIVATIVE;

EID: 85034349502     PISSN: 00404020     EISSN: None     Source Type: Journal    
DOI: 10.1016/S0040-4020(00)00247-7     Document Type: Article
Times cited : (17)

References (57)
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    • (1987) Usp. Khim. , vol.56 , pp. 938-974
    • Karaulova, E.N.1
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    • Reviews on synthesis and chemistry of cyclic sulfides: (a) Vedejs, E.; Krafft, G. A. Tetrahedron 1982, 38, 2857-2881. (b) Klimenko, S. K.; Stolbova, T. V. Usp. Khim. 1985, 54, 803-836; Russ. Chem. Rev. (Engl. Transl.) 1985, 54, 476-494. (c) Karaulova, E. N. Usp. Khim. 1987, 56, 938-974; Russ. Chem. Rev. (Engl. Transl.) 1987, 56, 546-563. (d) Karaulova, E. N. Usp. Khim. 1988, 57, 1131-1169; Russ. Chem. Rev. (Engl. Transl.) 1988, 57, 648-667. (e) Vedejs, E. In Total Synthesis Mediated by Cyclic Sulfides; Block, E., Ed.; Advances in Sulfur Chemistry; Jai Press: Greenwich, 1994; Vol. 1, pp 1-40; (f) Capozzi, G.; Menichetti, S.; Nativi, C. In Cyclic Sulfides; Patai, S.; Rappoport, Z., Eds.; Syntheses of Sulphones, Sulphoxides and Cyclic Sulphides; Wiley: Chichester, 1994; pp 529-648.
    • (1988) Usp. Khim. , vol.57 , pp. 1131-1169
    • Karaulova, E.N.1
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    • Reviews on synthesis and chemistry of cyclic sulfides: (a) Vedejs, E.; Krafft, G. A. Tetrahedron 1982, 38, 2857-2881. (b) Klimenko, S. K.; Stolbova, T. V. Usp. Khim. 1985, 54, 803-836; Russ. Chem. Rev. (Engl. Transl.) 1985, 54, 476-494. (c) Karaulova, E. N. Usp. Khim. 1987, 56, 938-974; Russ. Chem. Rev. (Engl. Transl.) 1987, 56, 546-563. (d) Karaulova, E. N. Usp. Khim. 1988, 57, 1131-1169; Russ. Chem. Rev. (Engl. Transl.) 1988, 57, 648-667. (e) Vedejs, E. In Total Synthesis Mediated by Cyclic Sulfides; Block, E., Ed.; Advances in Sulfur Chemistry; Jai Press: Greenwich, 1994; Vol. 1, pp 1-40; (f) Capozzi, G.; Menichetti, S.; Nativi, C. In Cyclic Sulfides; Patai, S.; Rappoport, Z., Eds.; Syntheses of Sulphones, Sulphoxides and Cyclic Sulphides; Wiley: Chichester, 1994; pp 529-648.
    • (1988) Russ. Chem. Rev. (Engl. Transl.) , vol.57 , pp. 648-667
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    • Reviews on synthesis and chemistry of cyclic sulfides: (a) Vedejs, E.; Krafft, G. A. Tetrahedron 1982, 38, 2857-2881. (b) Klimenko, S. K.; Stolbova, T. V. Usp. Khim. 1985, 54, 803-836; Russ. Chem. Rev. (Engl. Transl.) 1985, 54, 476-494. (c) Karaulova, E. N. Usp. Khim. 1987, 56, 938-974; Russ. Chem. Rev. (Engl. Transl.) 1987, 56, 546-563. (d) Karaulova, E. N. Usp. Khim. 1988, 57, 1131-1169; Russ. Chem. Rev. (Engl. Transl.) 1988, 57, 648-667. (e) Vedejs, E. In Total Synthesis Mediated by Cyclic Sulfides; Block, E., Ed.; Advances in Sulfur Chemistry; Jai Press: Greenwich, 1994; Vol. 1, pp 1-40; (f) Capozzi, G.; Menichetti, S.; Nativi, C. In Cyclic Sulfides; Patai, S.; Rappoport, Z., Eds.; Syntheses of Sulphones, Sulphoxides and Cyclic Sulphides; Wiley: Chichester, 1994; pp 529-648.
    • (1994) In Total Synthesis Mediated by Cyclic Sulfides , vol.1 , pp. 1-40
    • Vedejs, E.1
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    • (f) Patai, S.; Rappoport, Z., Eds.; Syntheses of Sulphones, Sulphoxides and Cyclic Sulphides; Wiley: Chichester
    • Reviews on synthesis and chemistry of cyclic sulfides: (a) Vedejs, E.; Krafft, G. A. Tetrahedron 1982, 38, 2857-2881. (b) Klimenko, S. K.; Stolbova, T. V. Usp. Khim. 1985, 54, 803-836; Russ. Chem. Rev. (Engl. Transl.) 1985, 54, 476-494. (c) Karaulova, E. N. Usp. Khim. 1987, 56, 938-974; Russ. Chem. Rev. (Engl. Transl.) 1987, 56, 546-563. (d) Karaulova, E. N. Usp. Khim. 1988, 57, 1131-1169; Russ. Chem. Rev. (Engl. Transl.) 1988, 57, 648-667. (e) Vedejs, E. In Total Synthesis Mediated by Cyclic Sulfides; Block, E., Ed.; Advances in Sulfur Chemistry; Jai Press: Greenwich, 1994; Vol. 1, pp 1-40; (f) Capozzi, G.; Menichetti, S.; Nativi, C. In Cyclic Sulfides; Patai, S.; Rappoport, Z., Eds.; Syntheses of Sulphones, Sulphoxides and Cyclic Sulphides; Wiley: Chichester, 1994; pp 529-648.
    • (1994) In Cyclic Sulfides , pp. 529-648
    • Capozzi, G.1    Menichetti, S.2    Nativi, C.3
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    • For synthesis and structure elucidation of some thiabicyclo[4.4.0]decanes and thiabicyclo[4.3.0]nonanes, see: (a)
    • For synthesis and structure elucidation of some thiabicyclo[4.4.0]decanes and thiabicyclo[4.3.0]nonanes, see: (a) Volynskii, N. P.; Alikhanova, O. L. Izv. Akad. Nauk USSR, Ser. Khim. 1991, 1877-1884; Bull. Acad. Sci. USSR, Div. Chem. Sci. 1991, 40, 1664-1671. (b) Volynskii, N. P.; Smirnov, M. B. Izv. Akad. Nauk SSR, Ser. Khim. 1991, 2045-2048; Bull. Acad. Sci. USSR, Div. Chem. Sci. 1991, 40, 1808-1811. (c) Pettett, M. G.; Holmes, A. B. J. Chem. Soc., Perkin Trans. 1 1985, 1161-1166. (d) Pettett, M. G.; Holmes, A. B. J. Chem. Soc., Perkin Trans. 1 1983, 1243-1248. (e) Benedetti, F.; Fabrissin, S.; Risaliti, A. Tetrahedron 1983, 39, 3887-3894. (f) Fabrissin, S.; Fatutta, S.; Risaliti, A. J. Chem. Soc., Perkin Trans. 1 1981, 109-112. (g) Takaki, K.; Nakagawa, K.; Negoro, K. J. Org. Chem. 1980, 45, 4789-4791. (h) Fabrissin, S.; Fatutta, S.; Risaliti, A. J. Chem. Soc., Perkin Trans. 1 1978, 1321-1325.
    • (1991) Izv. Akad. Nauk USSR, Ser. Khim. , pp. 1877-1884
    • Volynskii, N.P.1    Alikhanova, O.L.2
  • 16
    • 0343381504 scopus 로고
    • For synthesis and structure elucidation of some thiabicyclo[4.4.0]decanes and thiabicyclo[4.3.0]nonanes, see: (a) Volynskii, N. P.; Alikhanova, O. L. Izv. Akad. Nauk USSR, Ser. Khim. 1991, 1877-1884; Bull. Acad. Sci. USSR, Div. Chem. Sci. 1991, 40, 1664-1671. (b) Volynskii, N. P.; Smirnov, M. B. Izv. Akad. Nauk SSR, Ser. Khim. 1991, 2045-2048; Bull. Acad. Sci. USSR, Div. Chem. Sci. 1991, 40, 1808-1811. (c) Pettett, M. G.; Holmes, A. B. J. Chem. Soc., Perkin Trans. 1 1985, 1161-1166. (d) Pettett, M. G.; Holmes, A. B. J. Chem. Soc., Perkin Trans. 1 1983, 1243-1248. (e) Benedetti, F.; Fabrissin, S.; Risaliti, A. Tetrahedron 1983, 39, 3887-3894. (f) Fabrissin, S.; Fatutta, S.; Risaliti, A. J. Chem. Soc., Perkin Trans. 1 1981, 109-112. (g) Takaki, K.; Nakagawa, K.; Negoro, K. J. Org. Chem. 1980, 45, 4789-4791. (h) Fabrissin, S.; Fatutta, S.; Risaliti, A. J. Chem. Soc., Perkin Trans. 1 1978, 1321-1325.
    • (1991) Bull. Acad. Sci. USSR, Div. Chem. Sci. , vol.40 , pp. 1664-1671
  • 17
    • 0342946013 scopus 로고
    • (b)
    • For synthesis and structure elucidation of some thiabicyclo[4.4.0]decanes and thiabicyclo[4.3.0]nonanes, see: (a) Volynskii, N. P.; Alikhanova, O. L. Izv. Akad. Nauk USSR, Ser. Khim. 1991, 1877-1884; Bull. Acad. Sci. USSR, Div. Chem. Sci. 1991, 40, 1664-1671. (b) Volynskii, N. P.; Smirnov, M. B. Izv. Akad. Nauk SSR, Ser. Khim. 1991, 2045-2048; Bull. Acad. Sci. USSR, Div. Chem. Sci. 1991, 40, 1808-1811. (c) Pettett, M. G.; Holmes, A. B. J. Chem. Soc., Perkin Trans. 1 1985, 1161-1166. (d) Pettett, M. G.; Holmes, A. B. J. Chem. Soc., Perkin Trans. 1 1983, 1243-1248. (e) Benedetti, F.; Fabrissin, S.; Risaliti, A. Tetrahedron 1983, 39, 3887-3894. (f) Fabrissin, S.; Fatutta, S.; Risaliti, A. J. Chem. Soc., Perkin Trans. 1 1981, 109-112. (g) Takaki, K.; Nakagawa, K.; Negoro, K. J. Org. Chem. 1980, 45, 4789-4791. (h) Fabrissin, S.; Fatutta, S.; Risaliti, A. J. Chem. Soc., Perkin Trans. 1 1978, 1321-1325.
    • (1991) Izv. Akad. Nauk SSR, Ser. Khim. , pp. 2045-2048
    • Volynskii, N.P.1    Smirnov, M.B.2
  • 18
    • 0342946019 scopus 로고
    • For synthesis and structure elucidation of some thiabicyclo[4.4.0]decanes and thiabicyclo[4.3.0]nonanes, see: (a) Volynskii, N. P.; Alikhanova, O. L. Izv. Akad. Nauk USSR, Ser. Khim. 1991, 1877-1884; Bull. Acad. Sci. USSR, Div. Chem. Sci. 1991, 40, 1664-1671. (b) Volynskii, N. P.; Smirnov, M. B. Izv. Akad. Nauk SSR, Ser. Khim. 1991, 2045-2048; Bull. Acad. Sci. USSR, Div. Chem. Sci. 1991, 40, 1808-1811. (c) Pettett, M. G.; Holmes, A. B. J. Chem. Soc., Perkin Trans. 1 1985, 1161-1166. (d) Pettett, M. G.; Holmes, A. B. J. Chem. Soc., Perkin Trans. 1 1983, 1243-1248. (e) Benedetti, F.; Fabrissin, S.; Risaliti, A. Tetrahedron 1983, 39, 3887-3894. (f) Fabrissin, S.; Fatutta, S.; Risaliti, A. J. Chem. Soc., Perkin Trans. 1 1981, 109-112. (g) Takaki, K.; Nakagawa, K.; Negoro, K. J. Org. Chem. 1980, 45, 4789-4791. (h) Fabrissin, S.; Fatutta, S.; Risaliti, A. J. Chem. Soc., Perkin Trans. 1 1978, 1321-1325.
    • (1991) Bull. Acad. Sci. USSR, Div. Chem. Sci. , vol.40 , pp. 1808-1811
  • 19
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    • (c)
    • For synthesis and structure elucidation of some thiabicyclo[4.4.0]decanes and thiabicyclo[4.3.0]nonanes, see: (a) Volynskii, N. P.; Alikhanova, O. L. Izv. Akad. Nauk USSR, Ser. Khim. 1991, 1877-1884; Bull. Acad. Sci. USSR, Div. Chem. Sci. 1991, 40, 1664-1671. (b) Volynskii, N. P.; Smirnov, M. B. Izv. Akad. Nauk SSR, Ser. Khim. 1991, 2045-2048; Bull. Acad. Sci. USSR, Div. Chem. Sci. 1991, 40, 1808-1811. (c) Pettett, M. G.; Holmes, A. B. J. Chem. Soc., Perkin Trans. 1 1985, 1161-1166. (d) Pettett, M. G.; Holmes, A. B. J. Chem. Soc., Perkin Trans. 1 1983, 1243-1248. (e) Benedetti, F.; Fabrissin, S.; Risaliti, A. Tetrahedron 1983, 39, 3887-3894. (f) Fabrissin, S.; Fatutta, S.; Risaliti, A. J. Chem. Soc., Perkin Trans. 1 1981, 109-112. (g) Takaki, K.; Nakagawa, K.; Negoro, K. J. Org. Chem. 1980, 45, 4789-4791. (h) Fabrissin, S.; Fatutta, S.; Risaliti, A. J. Chem. Soc., Perkin Trans. 1 1978, 1321-1325.
    • (1985) J. Chem. Soc., Perkin Trans. , vol.1 , pp. 1161-1166
    • Pettett, M.G.1    Holmes, A.B.2
  • 20
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    • (d)
    • For synthesis and structure elucidation of some thiabicyclo[4.4.0]decanes and thiabicyclo[4.3.0]nonanes, see: (a) Volynskii, N. P.; Alikhanova, O. L. Izv. Akad. Nauk USSR, Ser. Khim. 1991, 1877-1884; Bull. Acad. Sci. USSR, Div. Chem. Sci. 1991, 40, 1664-1671. (b) Volynskii, N. P.; Smirnov, M. B. Izv. Akad. Nauk SSR, Ser. Khim. 1991, 2045-2048; Bull. Acad. Sci. USSR, Div. Chem. Sci. 1991, 40, 1808-1811. (c) Pettett, M. G.; Holmes, A. B. J. Chem. Soc., Perkin Trans. 1 1985, 1161-1166. (d) Pettett, M. G.; Holmes, A. B. J. Chem. Soc., Perkin Trans. 1 1983, 1243-1248. (e) Benedetti, F.; Fabrissin, S.; Risaliti, A. Tetrahedron 1983, 39, 3887-3894. (f) Fabrissin, S.; Fatutta, S.; Risaliti, A. J. Chem. Soc., Perkin Trans. 1 1981, 109-112. (g) Takaki, K.; Nakagawa, K.; Negoro, K. J. Org. Chem. 1980, 45, 4789-4791. (h) Fabrissin, S.; Fatutta, S.; Risaliti, A. J. Chem. Soc., Perkin Trans. 1 1978, 1321-1325.
    • (1983) J. Chem. Soc., Perkin Trans. , vol.1 , pp. 1243-1248
    • Pettett, M.G.1    Holmes, A.B.2
  • 21
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    • (e)
    • For synthesis and structure elucidation of some thiabicyclo[4.4.0]decanes and thiabicyclo[4.3.0]nonanes, see: (a) Volynskii, N. P.; Alikhanova, O. L. Izv. Akad. Nauk USSR, Ser. Khim. 1991, 1877-1884; Bull. Acad. Sci. USSR, Div. Chem. Sci. 1991, 40, 1664-1671. (b) Volynskii, N. P.; Smirnov, M. B. Izv. Akad. Nauk SSR, Ser. Khim. 1991, 2045-2048; Bull. Acad. Sci. USSR, Div. Chem. Sci. 1991, 40, 1808-1811. (c) Pettett, M. G.; Holmes, A. B. J. Chem. Soc., Perkin Trans. 1 1985, 1161-1166. (d) Pettett, M. G.; Holmes, A. B. J. Chem. Soc., Perkin Trans. 1 1983, 1243-1248. (e) Benedetti, F.; Fabrissin, S.; Risaliti, A. Tetrahedron 1983, 39, 3887-3894. (f) Fabrissin, S.; Fatutta, S.; Risaliti, A. J. Chem. Soc., Perkin Trans. 1 1981, 109-112. (g) Takaki, K.; Nakagawa, K.; Negoro, K. J. Org. Chem. 1980, 45, 4789-4791. (h) Fabrissin, S.; Fatutta, S.; Risaliti, A. J. Chem. Soc., Perkin Trans. 1 1978, 1321-1325.
    • (1983) Tetrahedron , vol.39 , pp. 3887-3894
    • Benedetti, F.1    Fabrissin, S.2    Risaliti, A.3
  • 22
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    • (f)
    • For synthesis and structure elucidation of some thiabicyclo[4.4.0]decanes and thiabicyclo[4.3.0]nonanes, see: (a) Volynskii, N. P.; Alikhanova, O. L. Izv. Akad. Nauk USSR, Ser. Khim. 1991, 1877-1884; Bull. Acad. Sci. USSR, Div. Chem. Sci. 1991, 40, 1664-1671. (b) Volynskii, N. P.; Smirnov, M. B. Izv. Akad. Nauk SSR, Ser. Khim. 1991, 2045-2048; Bull. Acad. Sci. USSR, Div. Chem. Sci. 1991, 40, 1808-1811. (c) Pettett, M. G.; Holmes, A. B. J. Chem. Soc., Perkin Trans. 1 1985, 1161-1166. (d) Pettett, M. G.; Holmes, A. B. J. Chem. Soc., Perkin Trans. 1 1983, 1243-1248. (e) Benedetti, F.; Fabrissin, S.; Risaliti, A. Tetrahedron 1983, 39, 3887-3894. (f) Fabrissin, S.; Fatutta, S.; Risaliti, A. J. Chem. Soc., Perkin Trans. 1 1981, 109-112. (g) Takaki, K.; Nakagawa, K.; Negoro, K. J. Org. Chem. 1980, 45, 4789-4791. (h) Fabrissin, S.; Fatutta, S.; Risaliti, A. J. Chem. Soc., Perkin Trans. 1 1978, 1321-1325.
    • (1981) J. Chem. Soc., Perkin Trans. , vol.1 , pp. 109-112
    • Fabrissin, S.1    Fatutta, S.2    Risaliti, A.3
  • 23
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    • (g)
    • For synthesis and structure elucidation of some thiabicyclo[4.4.0]decanes and thiabicyclo[4.3.0]nonanes, see: (a) Volynskii, N. P.; Alikhanova, O. L. Izv. Akad. Nauk USSR, Ser. Khim. 1991, 1877-1884; Bull. Acad. Sci. USSR, Div. Chem. Sci. 1991, 40, 1664-1671. (b) Volynskii, N. P.; Smirnov, M. B. Izv. Akad. Nauk SSR, Ser. Khim. 1991, 2045-2048; Bull. Acad. Sci. USSR, Div. Chem. Sci. 1991, 40, 1808-1811. (c) Pettett, M. G.; Holmes, A. B. J. Chem. Soc., Perkin Trans. 1 1985, 1161-1166. (d) Pettett, M. G.; Holmes, A. B. J. Chem. Soc., Perkin Trans. 1 1983, 1243-1248. (e) Benedetti, F.; Fabrissin, S.; Risaliti, A. Tetrahedron 1983, 39, 3887-3894. (f) Fabrissin, S.; Fatutta, S.; Risaliti, A. J. Chem. Soc., Perkin Trans. 1 1981, 109-112. (g) Takaki, K.; Nakagawa, K.; Negoro, K. J. Org. Chem. 1980, 45, 4789-4791. (h) Fabrissin, S.; Fatutta, S.; Risaliti, A. J. Chem. Soc., Perkin Trans. 1 1978, 1321-1325.
    • (1980) J. Org. Chem. , vol.45 , pp. 4789-4791
    • Takaki, K.1    Nakagawa, K.2    Negoro, K.3
  • 24
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    • For synthesis and structure elucidation of some thiabicyclo[4.4.0]decanes and thiabicyclo[4.3.0]nonanes, see: (a) Volynskii, N. P.; Alikhanova, O. L. Izv. Akad. Nauk USSR, Ser. Khim. 1991, 1877-1884; Bull. Acad. Sci. USSR, Div. Chem. Sci. 1991, 40, 1664-1671. (b) Volynskii, N. P.; Smirnov, M. B. Izv. Akad. Nauk SSR, Ser. Khim. 1991, 2045-2048; Bull. Acad. Sci. USSR, Div. Chem. Sci. 1991, 40, 1808-1811. (c) Pettett, M. G.; Holmes, A. B. J. Chem. Soc., Perkin Trans. 1 1985, 1161-1166. (d) Pettett, M. G.; Holmes, A. B. J. Chem. Soc., Perkin Trans. 1 1983, 1243-1248. (e) Benedetti, F.; Fabrissin, S.; Risaliti, A. Tetrahedron 1983, 39, 3887-3894. (f) Fabrissin, S.; Fatutta, S.; Risaliti, A. J. Chem. Soc., Perkin Trans. 1 1981, 109-112. (g) Takaki, K.; Nakagawa, K.; Negoro, K. J. Org. Chem. 1980, 45, 4789-4791. (h) Fabrissin, S.; Fatutta, S.; Risaliti, A. J. Chem. Soc., Perkin Trans. 1 1978, 1321-1325.
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  • 25
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    • (a) The amino acid obtained by deprotection of thiabicyclic compound 7 (Scheme 1) as well as a variety of other heterocycles comprising a restricted glutamic acid structure were synthesized in this laboratory. These compounds were tested by Professor Vivian Teichberg (Department of Neurobiology, Weizmann Institute of Science) and found to exhibit neuroactivity. Details will be published elsewhere. For recent reviews on excitatory amino acids, see
    • (a) The amino acid obtained by deprotection of thiabicyclic compound 7 (Scheme 1) as well as a variety of other heterocycles comprising a restricted glutamic acid structure were synthesized in this laboratory. These compounds were tested by Professor Vivian Teichberg (Department of Neurobiology, Weizmann Institute of Science) and found to exhibit neuroactivity. Details will be published elsewhere. For recent reviews on excitatory amino acids, see
  • 27
  • 28
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    • Reviews on synthesis of heterocycles by radical cyclization: (a)
    • Reviews on synthesis of heterocycles by radical cyclization: (a) Bowman, W. R.; Bridge, C. F.; Brookes, P. J. Chem. Soc., Perkin Trans. 1 2000, 1-14. (b) Easton, C. J. Chem. Rev. 1997, 97, 53-82. (c) Aldabbagh, F.; Bowman, W. R. Contemp. Org. Synth. 1997, 4, 261-280. (d) Giese, B.; Kopping, B.; Göbel, T.; Dickhaut, J.; Thoma, G.; Kulicke, K. J.; Trach, F. Org. React. (N.Y.) 1996, 48, 301-856. (e) Zlotsky, S. S.; Kochinashvili, M. V.; Rakhmankulov, D. L. Khim. Geterotsikl. Soedin. 1993, 1011-1034; Chem. Heterocycl. Compd. (Engl. Transl.) 1993, 29, 857-877.
    • (2000) J. Chem. Soc., Perkin Trans. , vol.1 , pp. 1-14
    • Bowman, W.R.1    Bridge, C.F.2    Brookes, P.3
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    • (b)
    • Reviews on synthesis of heterocycles by radical cyclization: (a) Bowman, W. R.; Bridge, C. F.; Brookes, P. J. Chem. Soc., Perkin Trans. 1 2000, 1-14. (b) Easton, C. J. Chem. Rev. 1997, 97, 53-82. (c) Aldabbagh, F.; Bowman, W. R. Contemp. Org. Synth. 1997, 4, 261-280. (d) Giese, B.; Kopping, B.; Göbel, T.; Dickhaut, J.; Thoma, G.; Kulicke, K. J.; Trach, F. Org. React. (N.Y.) 1996, 48, 301-856. (e) Zlotsky, S. S.; Kochinashvili, M. V.; Rakhmankulov, D. L. Khim. Geterotsikl. Soedin. 1993, 1011-1034; Chem. Heterocycl. Compd. (Engl. Transl.) 1993, 29, 857-877.
    • (1997) J. Chem. Rev. , vol.97 , pp. 53-82
    • Easton, C.1
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    • Reviews on synthesis of heterocycles by radical cyclization: (a) Bowman, W. R.; Bridge, C. F.; Brookes, P. J. Chem. Soc., Perkin Trans. 1 2000, 1-14. (b) Easton, C. J. Chem. Rev. 1997, 97, 53-82. (c) Aldabbagh, F.; Bowman, W. R. Contemp. Org. Synth. 1997, 4, 261-280. (d) Giese, B.; Kopping, B.; Göbel, T.; Dickhaut, J.; Thoma, G.; Kulicke, K. J.; Trach, F. Org. React. (N.Y.) 1996, 48, 301-856. (e) Zlotsky, S. S.; Kochinashvili, M. V.; Rakhmankulov, D. L. Khim. Geterotsikl. Soedin. 1993, 1011-1034; Chem. Heterocycl. Compd. (Engl. Transl.) 1993, 29, 857-877.
    • (1997) Contemp. Org. Synth. , vol.4 , pp. 261-280
    • Aldabbagh, F.1    Bowman, W.R.2
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    • (d)
    • Reviews on synthesis of heterocycles by radical cyclization: (a) Bowman, W. R.; Bridge, C. F.; Brookes, P. J. Chem. Soc., Perkin Trans. 1 2000, 1-14. (b) Easton, C. J. Chem. Rev. 1997, 97, 53-82. (c) Aldabbagh, F.; Bowman, W. R. Contemp. Org. Synth. 1997, 4, 261-280. (d) Giese, B.; Kopping, B.; Göbel, T.; Dickhaut, J.; Thoma, G.; Kulicke, K. J.; Trach, F. Org. React. (N.Y.) 1996, 48, 301-856. (e) Zlotsky, S. S.; Kochinashvili, M. V.; Rakhmankulov, D. L. Khim. Geterotsikl. Soedin. 1993, 1011-1034; Chem. Heterocycl. Compd. (Engl. Transl.) 1993, 29, 857-877.
    • (1996) Org. React. (N.Y.) , vol.48 , pp. 301-856
    • Giese, B.1    Kopping, B.2    Göbel, T.3    Dickhaut, J.4    Thoma, G.5    Kulicke, K.J.6    Trach, F.7
  • 32
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    • (e)
    • Reviews on synthesis of heterocycles by radical cyclization: (a) Bowman, W. R.; Bridge, C. F.; Brookes, P. J. Chem. Soc., Perkin Trans. 1 2000, 1-14. (b) Easton, C. J. Chem. Rev. 1997, 97, 53-82. (c) Aldabbagh, F.; Bowman, W. R. Contemp. Org. Synth. 1997, 4, 261-280. (d) Giese, B.; Kopping, B.; Göbel, T.; Dickhaut, J.; Thoma, G.; Kulicke, K. J.; Trach, F. Org. React. (N.Y.) 1996, 48, 301-856. (e) Zlotsky, S. S.; Kochinashvili, M. V.; Rakhmankulov, D. L. Khim. Geterotsikl. Soedin. 1993, 1011-1034; Chem. Heterocycl. Compd. (Engl. Transl.) 1993, 29, 857-877.
    • (1993) Khim. Geterotsikl. Soedin. , pp. 1011-1034
    • Zlotsky, S.S.1    Kochinashvili, M.V.2    Rakhmankulov, D.L.3
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    • Reviews on synthesis of heterocycles by radical cyclization: (a) Bowman, W. R.; Bridge, C. F.; Brookes, P. J. Chem. Soc., Perkin Trans. 1 2000, 1-14. (b) Easton, C. J. Chem. Rev. 1997, 97, 53-82. (c) Aldabbagh, F.; Bowman, W. R. Contemp. Org. Synth. 1997, 4, 261-280. (d) Giese, B.; Kopping, B.; Göbel, T.; Dickhaut, J.; Thoma, G.; Kulicke, K. J.; Trach, F. Org. React. (N.Y.) 1996, 48, 301-856. (e) Zlotsky, S. S.; Kochinashvili, M. V.; Rakhmankulov, D. L. Khim. Geterotsikl. Soedin. 1993, 1011-1034; Chem. Heterocycl. Compd. (Engl. Transl.) 1993, 29, 857-877.
    • (1993) Chem. Heterocycl. Compd. (Engl. Transl.) , vol.29 , pp. 857-877
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    • (n) Block, E. J. Am. Chem. Soc. 1972, 94, 644-645; and references therein.
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    • For a review on applications of perfluoroalkanesulfonic esters, see
    • For a review on applications of perfluoroalkanesulfonic esters, see: Stang, P. J.; Hanack, M.; Subramanian, L. R. Synthesis 1982, 85-126.
    • (1982) Synthesis , pp. 85-126
    • Stang, P.J.1    Hanack, M.2    Subramanian, L.R.3


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