Diffuse reflectance FTIR spectroscopic study of base desorption from thermally treated silica

Colloidal Silica: Fundamentals and Applications

Volumn , Issue , 2005, Pages 385-396

  Proctor, Kristina G ^a   Markway, Sally J ^b   Garcia, Miguel ^b   Armstrong, Cheryl A ^b   Gonzales, Chad P ^b  

^a Veterinary Dentistry and Oral Surgery   (United States)

^b Malik and Seeme Hasan School of Business   (United States)

Author keywords

[No Author keywords available]

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EID: 85017078022     PISSN: None     EISSN: None     Source Type: Book    
DOI: None     Document Type: Chapter

References (32)

1. K.K. Unger, ed., Packings and Stationary Phases in Chromatographic Techniques, Marcel-Dekker, New York, 1990.
2. R.K. Iler, The Chemistry of Silica. Solubility, Polymerization, Colloid and Surface Properties, and Biochemistry, Wiley-Interscience, New York, 1979.
3. K.K. Unger, Porous Silica, Its Properties and Use as a Support in Column Liquid Chromatography, J. Chromatography Library, Vol 16, Elsevier, Amsterdam, 1979.
4. J. Nawrocki, The Silanol Group and Its Role in Liquid Chromatography, J. Chromtograph. A, 779, pp. 29-71, 1997.
5. M. Peussa, S. Härkönen, J. Puputti, and L. Niinistö, Application of PLS Multivariate Calibration for the Determination of the Hydroxyl Group Content in Calcined Silica by DRIFTS, J. Chemometrics, 14, pp. 501-512, 2000.
6. M.J. Wirth, M.D. Ludes, and D.J. Swinton, Spectroscopic Observation of Adsorption to Active Silanols, Anal. Chem., 71, pp. 3911-3917, 1999.
7. S. Ashtekar, J.J. Hatings, P.J. Barrie, and L.F. Gladden, Quantification of the Number of Silanol Groups in Silicalite and Mesoporous MCM-41: Use of FT-Raman spectroscopy, Spectroscopy Lett., 33(4), pp. 569-584, 2000.
8. 29 Si Solid State NMR Chemical Shifts of Silane and Silanol Groups in Silica, Chem. Phys. Lett., 326, pp. 523-529, 2000.
9. B.A. Morrow and I.D. Gay, Infrared and NMR Characterization of the Silica Surface, Adsorption on Silica Surfaces (Series: Surfactant Science Series 90), E. Papirer, ed., Marcel Dekker Inc., New York, pp. 9-33, 2000.
10. G.E. Maciel and P.D. Ellis, NMR Characterization of Silica and Alumina Surfaces, NMR Techniques in Catalysis, Chemical Industries, 55, pp. 231-309, 1994.
11. I.S. Chuang, and G.E. Maciel, Probing Hydrogen Bonding and the Local Environment of Silanols on Silica Surfaces via Nuclear Spin Cross Polarization Dynamics, J. Am. Chem. Soc., 118, pp. 401-406, 1996.
12. G.E. Maciel, C.E. Bronnimann, R.C. Zeigler, I-Ssuer Chuang, D.R. Kinney, and E.A. Keiter, Multinuclear NMR Spectroscopy Studies of Silica Surface, in The Colloid Chemistry of Silica, ACS Advances in Chemistry Series no. 239, pp. 269-282, 1994.
13. M.L. Hair, Infrared Spectroscopy in Surface Chemistry, Marcel Dekker, New York, 1967.
14. M.L. Hair and W. Hertl, Adsorption on Hydroxylated Silica Surfaces, J. Phys. Chem., 73(12), pp.4269-4276, 1969.
15. P.R. Griffiths, Chemical Infrared Fourier Transform Infrared Spectroscopy, Vol. 3, Academic Press, New York, 1982.
16. J.P. Blitz, R.S.S. Murthy, and D.E. Leyden, Comparison of Transmission and Diffuse Reflectance Sampling Techniques for FT-IR Spectrometry of Silane Modified Silica Gel, Appl. Spectrosc., 40(6), pp. 829-831, 1986.
17. J.P. Blitz, Diffuse Reflectance Spectroscopy, in Modern Techniques in Applied Molecular Spectroscopy, Francis M. Mirabella (ed.), Wiley-Interscience, New York, pp. 185-219, 1998.
18. F.H. Hambleton, J.A. Hockey, and J.A.G. Taylor, An Infra-red Investigation of the Effect of Pressure on Silica Powders, as Revealed by Deuterium Oxide Exchange, Nature, 208, pp. 138-139, 1965.
19. P.W. Yang and H.L. Casal, In-Situ Monitoring of Solid-State Photochemical Reactions by Diffuse Reflectance Infrared Spectroscopy, Appl. Spectrosc., 40(7), pp. 1070-1073, 1986.
20. V.A. Bell, V.R. Citro, and G.D. Hodge, Effect of Pellet Pressing on the Infrared Spectrum of Kaolinite, Clays and Clay Minerals, 39(3), pp. 290-292, 1991.
21. R.S.S. Murthy and D.E. Leyden, Quantitative Determination of 3-Aminopropyl Triethoxysilane on Silica Gel Surface Using Diffuse Reflectance Infrared Fourier Transform Spectrometry, Anal. Chem., 58, pp. 1228-1234, 1986.
22. J. Kohler, J.J. Kirkland, J. Chromatogr., 385, p. 125, 1987.
23. J. Kohler, D.B. Chase, R.D. Farlee, A.J. Vega, J.J. Kirkland, J. Chromatogr., 352, p. 275, 1986.
24. 2, Surface Science, 188, pp. 181-198, 1988.
25. A.J. McFarlan and B.A. Morrow, Infrared Evidence for Two Isolated Silanol Species on Activated Silicas, J. Phys. Chem., 95, pp. 5388-5390, 1991.
26. K.G. Proctor, S.K. Ramirez, K.L. McWilliams, J.L. Huerta, and J.J. Kirkland, The Progressive Effect of Surface Silylation on the Silanol Population of Silica, Chemically Modified Surfaces, J.J. Pesek, M.T. Matyska and R.R. Abuelafiya, Eds., Royal Society of Chemistry, Cambridge, UK, pp. 45-60, 1996.
27. E.P. Parry, An Infrared Study of Pyridine Adsorbed on Acidic Solids. Characterization of Surface Acidity, J. Catal., 2, pp. 371-379, 1963.
28. I. Gillis-D’Hamers, I. Cornelissens, K.C. Vrancken, P. Van Der Voort, and E.F. Vansant, Modeling of the Hydroxyl Group Population Using an Energetic Analysis of the Temperature-Programmed Desorption of Pyridine from Silica, J. Chem. Soc. Faraday Trans., 88(5), pp. 723-727, 1992.
29. K.G. Proctor and D.E. Leyden, Surface Acidity Characterization of Siliceous Materials by Variable Temperature Diffuse Reflectance FTIR, Chemically Modified Oxide Surfaces, Vol. 3, D.E. Leyden and W.T. Collins Eds., Gordon and Breach Science Publishers, New York, pp. 137-149, 1990.
30. D.E. Leyden and K.G. Proctor, Variable-Temperature Diffuse Reflectance Fourier Transform Infrared Spectroscopic Studies of Amine Desorption from a Siliceous Surface, The Colloid Chemistry of Silica, ACS Advances in Chemistry Series No. 234, H. Bergna Ed., pp. 257-267, 1994.
31. K.G. Proctor, K.M. Murphy, C.B. France, S.K. Ramirez, and A.R. Gennuso, DRIFTS Study of Silica Selection in Preparation of Substrates for HPLC, 7th International Conference on Chemically Modified Surfaces, Evanston, IL, June 1999.
32. H.A.M. Velhurst, L.J.M. van de Ven, J.W. deHaan, H.A. Claessens, F. Eisenbeiss, and C.A. Cramers, J. Chromatogr. A., 687, p. 213, 1994.