Synthesis and molecular structures of the base-stabilized arylboron dichlorides BCl2(2,6-(NEt2CH2)2C6H3) and BCl2(2-(NMe2CH2)C6H4)

Main Group Chemistry

Volumn 2, Issue 2, 1997, Pages 141-148

  Schlengermann, Robert ^a   Sieler, Joachim ^a   Hey Hawkins, Evamarie ^a  

^a UNIVERSITY OF LEIPZIG   (Germany)

Author keywords

[No Author keywords available]

Indexed keywords

EID: 85013593329     PISSN: 10241221     EISSN: 17451167     Source Type: Journal    
DOI: 10.1080/10241229712331341274     Document Type: Article

References (42)

1. Manzer, L. E. J. Am. Chem. Soc. 1978, 200, 8068.
2. Cope, A. C; Gourley, R. N. J. Orgcmomet. Chem. 1967, 8, 527.
3. Coggin, D. K.; Fanwick, P. E.; Green, M. A. J. Chem. Soc., Chem. Commun. 1993, 1127.
4. Khan, M; Steevensz, R. C; Tuck, D. G.; Noltes, J. G.; Corfield, P. W. R. Inorg. Chem. 1980, 19, 3407.
5. Grove, D. M; van Koten, G.; Louwen, J. N.; Noltes, J. G.; Spek, A. L.; Ubbels, H. J. C. J. Am. Chem. Soc. 1982, 204, 6609.
6. de Koster, A.; Kanters, J. A.; Spek, A. L.; van der Zeijden, A. A. H.; van Koten, G.; Vrieze, K. Acta Crystallogr. 1985, 42C, 893.
7. van der Zeijden, A. A. H.; van Koten, G. Inorg. Chem. 1986, 25, 4723.
8. Wayda, A. L.; Rogers, R. D. Organometallics 1985, 4, 1440.
9. Cotton, F. A.; Mott, G. N. Organometallics 1982, 2, 38.
10. Manzer, L. E. J. Am. Chem. Soc. 1978, 200, 8068.
11. van Koten, G. Pure Appl. Chem. 1989, 62, 1681.
12. van Koten, G. Pure Appl. Chem. 1990, 62, 1155.
13. Jastrzebski, J. T. B. H.; van Koten, G. Adv. Organomet. Chem. 1993, 35, 241.
14. Hogerheide, M. P.; Boersma, J.; Spek, A. L.; van Koten, G. Organometallics 1996, 25, 1505.
15. Schumann, H.; Hartmann, U.; Wassermann, W.; Dietrich, A.; Görlitz, F. H.; Pohl, L.; Hostalek, M. Chem. Ber. 1990, 223, 1093.
16. Müller, J.; Englert, U. Chem. Ber. 1995, 128, 493.
17. Isom, H. S.; Cowley, A. H.; Decken, A.; Sissingh, F.; Corbelin, S.; Lagow, R. J. Organometallics 1995, 24, 2400.
18. Contreras, L.; Cowley, A. H.; Gabbai, F. P.; Jones, R. A.; Carrano, C. J.; Bond, M. R. J. Organomet. Chem. 1995, 489, CL.
19. Schumann, H.; Hartmann, U.; Wassermann, W. Chem. Ber. 1991, 224, 1567.
20. Schumann, H.; Wassermann, W.; Dietrich, A. J. Organomet. Chem. 1989, 365, 11.
21. Lauer, M.; Böhnke, H.; Grotstollen, R.; Salehnia, M.; Wulff, G. Chem. Ber. 1985, 118, 246.
22. Toyota, S.; Oki, M. Bull. Chem. Soc. jpn. 1992, 65, 1832.
23. Toyota, S.; Futawaka, T.; Ikeda, H.; Oki, M. J. Chem. Soc, Chem. Commun. 1995, 2499.
24. Lauer, M.; Wulff, G. J. Organomet. Chem. 1983, 256, 1.
25. 2(/i-BX), with X = NMe2, R = H, Me; X = Bu’, R = Me (Braunschweiger, H.; Wagner, T. Angew. Chem. 1995, 207, 904.
26. Schlengermann, R.; Jelonek, S.; Sieler, J.; Hey-Hawkins, E. J. Chem. Soc, Chem. Commun. 1997, 197.
27. 3) was characterized by comparison with the NMR data of BrjNEt.CHQHJ: van Beek, J. A. M.; van Koten, G.; Dekker, G. P. C. M.; Wissing, E. J. Organomet. Chem. 1990, 394, 659.
28. Nöth, H.; Vahrenkamp, H. Chem. Ber. 1966, 99, 1049.
29. Gmelin, Handbuch der Anorganischen Chemie, Ergänzungswerk zur 8. Auflage, Bd. 37, Teil 10, Springer Verlag, Berlin, 1976.
30. Kalbarczyk-Bidelska, E.; Pasynkiewicz, S. J. Organomet. Chem. 1991, 407, 143 and 427, 1.
31. Kalbarczyk-Bidelska, E.; Pasynkiewicz, S. Main Group Met. Chem. 1991, 24, 123.
32. Kalbarczyk, E.; Pasynkiewicz, S. J. Organomet. Chem. 1985, 292, 119.
33. Kalbarczyk, E.; Pasynkiewicz, S. J. Organomet. Chem. 1984, 273, C23.
34. Nöth, H.; Wrackmeyer, B. NMR Spectroscopy of Boron Compounds, in Diehl, P.; Fluck, E.; Kosfeld, R. (Eds); Springer Verlag, Berlin, Vol. 14, 1978.
35. Contreras, R.; Garcia, C; Mancilla, T.; Wrackmeyer, B. J. Organomet. Chem. 1983, 246, 213.
36. Weidlein, J.; Müller, U.; Dehnicke, K. Schwingungsfrequenzen I, Hauptgruppenelemente, G. Thieme Verlag, Stuttgart, 1981.
37. Hess, H. Acta Crystallogr. 1969, 25B, 2338.
38. Swanson, B.; Shriver, D. F.; Ibers, J. A. Inorg. Chem. 1969, 8, 2182.
39. Gerrard, W.; Läppert, M. F. J. Chem. Soc. 1951, 1020.
40. SHELXTL-PLUS, Siemens Analyt. X-ray Inst. Inc., 1990, XS: Program for Crystal Structure Solution, XL: Program for Crystal Structure Determination, XP: Interactive Molecular Graphics.
41. Blessing, R. H. Acta Crystallogr. 1995, 51A, 33.
42. Further details of the structure determination may be obtained upon request from the Fachinformationszentrum Karlsruhe, D-76344 Eggenstein-Leopoldshafen, Germany, giving reference to the depository number CSD 406261 (for 2) and CSD 406260 (for 3), and citing the authors and this paper.