Characterisation of Halloysite by Spectroscopy

Developments in Clay Science

Volumn 7, Issue , 2016, Pages 115-136

  Kloprogge, J T ^a  

^a UNIVERSITY OF QUEENSLAND   (Australia)

Author keywords

Cathodeluminescence; Electron spin resonance spectroscopy; Halloysite; Infrared spectroscopy; Kaolin; M ssbauer spectroscopy; Raman spectroscopy; Solid state magic angle spinning nuclear magnetic resonance spectroscopy; X ray photoelectron spectroscopy

Indexed keywords

EID: 85012992046     PISSN: 15724352     EISSN: None     Source Type: Book Series    
DOI: 10.1016/B978-0-08-100293-3.00006-6     Document Type: Chapter

References (45)

1. Barron, P.F., Wilson, M.A., Campbell, A.S., Frost, R.L., Detection of imogolite in soils using solid state silicon-29 NMR. Nature 299 (1982), 616–618.
2. Calhoun, F.G., Carlisle, V.W., Infrared spectra of selected colombian Andosols. Proc. Soil Crop Sci. Soc. Florida 31 (1972), 157–161.
3. Chaikum, N., Carr, R.M., Electron spin resonance studies of halloysites. Clay Miner. 22 (1987), 287–296.
4. Cheng, H., Frost, R.L., Yang, J., Liu, Q., He, J., Infrared and infrared emission spectroscopic study of typical Chinese kaolinite and halloysite. Spectrochim. Acta A Mol. Biomol. Spectrosc. 77A (2010), 1014–1020.
5. Cheng, H., Yang, J., Liu, Q., Zhang, J., Frost Ray, L., A spectroscopic comparison of selected Chinese kaolinite, coal bearing kaolinite and halloysite—a mid-infrared and near-infrared study. Spectrochim. Acta A Mol. Biomol. Spectrosc. 77 (2010), 856–861.
6. Coyne, L.M., Costanzo, P.M., Theng, B.K.G., Luminescence and ESR studies of relationships between oxygen(1-)-centers and structural iron in natural and synthetically hydrated kaolinites. Clay Miner. 24 (1989), 671–693.
7. 191. Phys. Rev. Lett., 3, 1959, 221.
8. Crowley, J.K., Vergo, N., Near-infrared reflectance spectra of mixtures of kaolin-group minerals: use in clay mineral studies. Clay Clay Miner. 36 (1988), 310–316.
9. Cruz, M.I., Letellier, M., Fripiat, J.J., NMR study of adsorbed water. II. Molecular motions in the monolayer hydrate of halloysite. J. Chem. Phys. 69 (1978), 2018–2027.
10. De Roy, G., Verhaert, I., Vansant, E.F., Allophane and halloysite minerals. Structural considerations. Recueil des Travaux Chimiques des Pays-Bas 100 (1981), 102–106.
11. Farmer, V.C., The Infrared Spectra of Minerals. 1974, Mineralogical Society, London.
12. Frost, R.L., Fourier transform Raman spectroscopy of kaolinite, dickite and halloysite. Clay Clay Miner. 43 (1995), 191–195.
13. Frost, R.L., The structure of the kaolinite minerals—a FT-Raman study. Clay Miner. 32 (1997), 65–77.
14. Frost, R.L., Hydroxyl deformation in kaolins. Clay Clay Miner. 46 (1998), 280–289.
15. Frost, R.L., Shurvell, H.F., Raman microprobe spectroscopy of halloysite. Clay Clay Miner. 45 (1997), 68–72.
16. Frost, R.L., Vassallo, A.M., The dehydroxylation of the kaolinite clay minerals using infrared emission spectroscopy. Clay Clay Miner. 44 (1996), 635–651.
17. Frost, R.L., Fredericks, P.M., Bartlett, J.R., Fourier transform Raman spectroscopy of kandite clays. SpEectrochIm ACTA A. 49A (1993), 667–674.
18. Goetze, J., Ploetze, M., Goette, T., Neuser, R.D., Richter, D.K., Cathodoluminescence (CL) and electron paramagnetic resonance (EPR) studies of clay minerals. Mineral. Petrol. 76 (2002), 195–212.
19. Johnston, C.T., Sposito, G., Birge, R.R., Raman spectroscopic study of kaolinite in aqueous suspension. Clays Clay Miner. 33 (1985), 483–489.
20. Kinsey, R.A., Kirkpatrick, R.J., Hower, J., Smith, K.A., Oldfield, E., High resolution aluminum-27 and silicon-29 nuclear magnetic resonance spectroscopic study of layer silicates, including clay minerals. Am. Mineral. 70 (1985), 537–548.
21. Kitagawa, Y., An aspect of the water in clay minerals: an application of nuclear magnetic resonance spectrometry to clay mineralogy. Am. Mineral. 57 (1972), 751–764.
22. Kloprogge, J.T., Short introduction to infrared and Raman spectroscopy. Kloprogge, J.T., (eds.) The Application of Vibrational Spectroscopy to Clay Minerals and Layered Double Hydroxides, 2005, The Clay Minerals Society, Aurora, CO, 1–7.
23. Kloprogge, J.T., Comment on “A spectroscopic comparison of selected Chinese kaolinite, coal bearing kaolinite and halloysite—a mid-infrared and near-infrared study” and “Infrared and infrared emission spectroscopic study of typical Chinese kaolinite and halloysite” by Hongfei Cheng et al. (2010). Spectrochim. Acta A Mol. Biomol. Spectrosc. 136 (2015), 175–177.
24. Kloprogge, J.T., Frost, R.L., Raman microprobe spectroscopy of hydrated halloysite from a Neogene cryptokarst from southern Belgium. J. Raman Spectrosc. 30 (1999), 1079–1085.
25. Kloprogge, J.T., Frost, R.L., Infrared emission spectroscopy study of the dehydroxylation of 10 Å halloysite from a Neogene cryptokarst of southern Belgium. Geol. Belg. 2 (2000), 213–220.
26. 4 polymorphs kaolinite, dickite, nacrite and halloysite by X-photoelectron spectroscopy. Clay Science 19 (2015), 39–45.
27. 29Si magic-angle-spinning NMR spectroscopy. Clay Miner. 20 (1985), 327–334.
28. Komusinski, J., Stoch, L., Dubiel, S.M., Application of electron paramagnetic resonance and Mössbauer spectroscopy in the investigation of kaolinite-group minerals. Clays Clay Miner. 29 (1981), 23–30.
29. 19F nuclear magnetic resonance study of natural clays. Clay Clay Miner. 43 (1995), 697–704.
30. Libowitzky, E., Correlation of O-H stretching frequencies and O-H O hydrogen bond lengths in minerals. Schuster, P., Mikenda, W., (eds.) Hydrogen Bond Research, 1999, Springer, Vienna, 103–115.
31. Loh, E., Optical vibrations in sheet silicates. J. Phys. C: Solid State Phys. 6 (1973), 1091–1104.
32. Lyon, R.J.P., Tuddenham, W.M., Infrared determination of the kaolin-group minerals. Nature 185 (1960), 835–836.
33. Madejová, J., Kraus, I., Tunega, D., Samajova, E., Fourier transform infrared spectroscopic characterization of kaolin-group minerals from the main Slovak deposits. Geol. Carpath. Clays 6 (1997), 3–10.
34. Michaelian, K.H., The Raman spectrum of kaolinite #9 at 21°C. Can. J. Chem. 64 (1986), 285–289.
35. 191. Z. Phys. A 151 (1958), 124–143.
36. Nagasawa, K., Noro, H., An electron spin resonance study of halloysites. Clay Sci. 6 (1987), 261–268.
37. 27Al NMR spectroscopy. Clay Miner. 29 (1994), 305–312.
38. Pampuch, R., Infrared study of the thermal transformation of kaolinite and the structure of metakaolin. Pr. Mineral. 6 (1966), 53–70.
39. Petit, S., Madejova, J., Decarreau, A., Martin, F., Characterization of octahedral substitutions in kaolinites using near infrared spectroscopy. Clay Clay Miner. 47 (1999), 103–108.
40. Petit, S., Decarreau, A., Martin, F., Bucher, R., Refined relationship between the position of the fundamental OH stretching and the first overtones for clays. Phys. Chem. Miner. 31 (2004), 585–592.
41. 27Al-NMR and ESR. Geochem. J. 22 (1988), 23–31.
42. Soma, M., Churchman, G.J., Theng, B.K.G., X-ray photoelectron spectroscopic analysis of halloysites with different composition and particle morphology. Clay Miner. 27 (1992), 413–421.
43. Stubičan, V., Roy, R., Proton retention in heated 1:1 clays studied by infrared spectroscopy, weight loss and deuterium uptake. J. Phys. Chem. 65 (1961), 1348–1351.
44. Wiewiora, A., Wieckowski, T., Sokolowska, A., The Raman spectra of kaolinite sub-group minerals and of pyrophyllite. Arch. Mineral. 35 (1979), 5–12.
45. Zhang, Y., Fu, L., Yang, H., Insights into the physicochemical aspects from natural halloysite to silica nanotubes. Colloids Surf. A 414 (2012), 115–119.