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Structure data for CALF-33-Et, H (see SI for details) C, H, Cu, O, P, M, w=1389.45),, T, =173K, triclinic, space group, (2),, a=, 5.08130(10),, b=, 15.1585(3),, c=, 29.3246(7) Å,, =83.8820(10),, =85.7280(10),, =82.705(2)°,, V=, 2223.42(8) Å, Z=, 1,, =1.036 g cm, =0.866 mm, measured reflections, 7376 unique reflections (, R, =0.0939),, R1=, 0.0700 for 3758 observed reflections (, I, >2, I,)) and 379 parameters (after accounting for disordered solvent with the SQUEEZE function in Platon,). CCDC, contains the supplementary crystallographic data for this paper. These data can be obtained free of charge from
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Structure data for CALF-33-Et2H (see SI for details): C56H52Cu3O18P6(Mw=1389.45), T=173(2) K, triclinic, space group P1‾ (No. 2), a=5.08130(10), b=15.1585(3), c=29.3246(7) Å, α=83.8820(10), β=85.7280(10), γ=82.705(2)°, V=2223.42(8) Å3, Z=1, ρcalcd=1.036 g cm−3, μ=0.866 mm−1, measured reflections, 7376 unique reflections (Rint=0.0939), R1=0.0700 for 3758 observed reflections (I>2σ(I)) and 379 parameters (after accounting for disordered solvent with the SQUEEZE function in Platon[21]). CCDC 1496410 contains the supplementary crystallographic data for this paper. These data can be obtained free of charge from TheCambridgeCrystallographicDataCentre.
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