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Volumn 28, Issue 1, 1989, Pages 64-66

A trans‐Dimethyl Derivative of Octahedral TiIV: Alkylation and Arylation of TiIV‐Schiff Base Complexes

Author keywords

[No Author keywords available]

Indexed keywords

EID: 84990101212 PISSN: 05700833 EISSN: 15213773 Source Type: Journal
DOI: 10.1002/anie.198900641 Document Type: Article

Times cited : (47)

References (20)

2
- 0002291128
- Organometallverbindungen von Titan und Zirconium als selektive nucleophile Reagentien für die Organische Synthese
- (1983) Angewandte Chemie , vol.95 , pp. 12
- Weidmann, B.¹ Seebach, D.²

4
- 0000099879
- R. Scheffold, Wiley, New York
- (1983) Modern Synthetic Methods , vol.3
- Seebach, D.¹ Weidmann, B.² Widler, L.³

13
- 34547449181
- (a) Very easy synthesis of 1
- J. Chem. Soc. Dalton Trans. , vol.1982 , pp. 2197
- Dell'Amico, G.¹ Marchetti, F.² Floriani, C.³

14
- 0001690674
- The crystal and molecular structure of dichloro-N,N'-ethylenebis(salicylideneiminato)titanium(IV)–tetrahydrofuran
- (b) structure of 1:, B 28
- (1972) Acta Crystallographica Section B Structural Crystallography and Crystal Chemistry , pp. 1889
- Gilli, G.¹ Cruickshank, D.W.J.² Beddocs, R.C.³ Mills, O.S.⁴

15
- 84990168343
- 2): δ = −0.25 (s, 6·H), 4.31 (s, 4 H), 7.02 (m, 4 H), 7.35 (s, 4 H), 8.37 (s, 2 H).

16
- 84990146584
- 2). 882 unique observed reflections [I > 2 σ(I)] collected at room temperature (6° < 2θ < 46°) were used, R = 0.038 [13].

17
- 84990146633
- eff = 1.77 BM at 294 K. The solid state structure shows a pseu‐dooctahedral coordination for titanium with the Ph group trans to the THF molecule; the salen ligand forms the equatorial plane.

18
- 84990119052
- 6): δ = 1.60 (s, 3 H), 2.03 (s, 3 H), 2.12 (s, 3 H), 2.43 (s, 3 H), 2.49 (s, 6 H), 2.70 (m, 1 H), 3.17 (m, 1 H), 3.39 (m, 1 H), 4.29 (m, 1 H), 6.30–7.25 (a series of multiplets, 12 H), 7.28 (s, 1 H).

19
- 84990136750
- 2). 3625 unique observed reflections [I > 2σ(I)] collected at room temperature (6° <2θ<130°) were used, R = 0.057. The intensities were corrected for absorption [13].

20
- 84990136749
- Further details of the crystal structure investigation are available from the Director of the Cambridge Crystallographic Data Centre, University Chemical Laboratory, Lensfield Road, Cambridge CB2 1EW (England) on quoting the full literature citation.

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