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Volumn 27, Issue 12, 1988, Pages 1725-1727

Reductive Oligomerization of 1,2‐Di‐tert‐butyl‐1,1,2,2‐tetrachlorodisilane: The Tricyclo[2.2.0.02,5]hexasilane and Tetracyclo[3.3.0.02,7.03,6]octasilane Systems

Author keywords

[No Author keywords available]

Indexed keywords


EID: 84989507666     PISSN: 05700833     EISSN: 15213773     Source Type: Journal    
DOI: 10.1002/anie.198817251     Document Type: Article
Times cited : (34)

References (32)
  • 18
    • 84990117897 scopus 로고    scopus 로고
    • 3‐mediated Ph/Cl exchange reaction of 1,2‐di‐tert‐butyl‐1,1,2,2‐tetraphenyldisilane, which was in turn obtained by reductive coupling of commercially available tert‐butylchlorodiphenylsilane. We were informed that Prof. R. West also obtained 1 and 2 (private communication).
  • 19
    • 84990107132 scopus 로고    scopus 로고
    • 3,6]octane system is apparently unknown.
  • 22
    • 84990128132 scopus 로고    scopus 로고
    • κα radiation (λ = 1.5418 Å). The structure was solved by direct methods (MULTAN 80) [7]. Strong diffractions of heavy atoms (Si, Cl) produced the satisfactory solution of the Si‐framework, but severe disordering of tert‐butyl groups resulted in a moderate quality of the refinement.
  • 24
    • 84990146074 scopus 로고    scopus 로고
    • Further details of the crystal structure investigations are available on request from the Fachinformationszentrum Energie, Physik, Mathematik GmbH, D‐7514 Eggenstein‐Leopoldshafen 2 (FRG), on quoting the depository · number CSD‐53324, the names of the authors, and the journal citation.
  • 26
    • 84990077318 scopus 로고    scopus 로고
    • 3, Z = 4, 10771 collected reflections, R = 0.0741.


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.