Identification of anthraquinone dye colourants in red fibres from an Ohio Hopewell mound site by direct analysis in real time mass spectrometry

Science and Technology of Archaeological Research

Volumn 1, Issue 2, 2015, Pages 1-10

  Armitage, Ruth Ann ^a   Day, Calvin ^a   Jakes, Kathryn A ^b  

^a EASTERN MICHIGAN UNIVERSITY   (United States)

^b OHIO STATE UNIVERSITY   (United States)

Author keywords

Anthraquinone; DART MS; Dyes; Galium; Hopewell; Textile

Indexed keywords

EID: 84987901174     PISSN: None     EISSN: 20548923     Source Type: Journal    
DOI: 10.1179/2054892315Y.0000000010     Document Type: Article

References (49)

1. Baldia, Christel M., and Kathryn A. Jakes. 2007. “Photographic Methods to Detect Colourants in Archaeological Textiles.” Journal of Archaeological Science 34 (4): 519–525.
2. Baldia, Christel M., Kathryn A. Jakes, and Maximillian O. Baldia. 2008. “Colorations and Fabric Structure of Selected Polychrome Textiles from the Seip Mound Group.” Midcontinental Journal of Archaeology 33 (2): 197–222.
3. Brose, David, James A. Brown, and David W. Penney. 1985. Ancient Art of the American Woodland Indians. New York: Harry Abrams.
4. Cardon, Dominique. 2007. Natural Dyes: Sources, Tradition, Technology and Science. London: Archetype.
5. Carr, Christopher, and D. Troy Case. 2006. Gathering Hopewell: Society, Ritual and Ritual Interaction. New York: Springer.
6. Church, Flora. 1983. “An Analysis of Textile Fragments from Three Ohio Hopewell Sites.” Ohio Archaeologist 33 (1): 10–15.
7. Church, Flora. 1984. “Textiles as Markers of Ohio Hopewell Social Identities.” Midcontinental Journal of Archaeology 9: 1–25.
8. Cody, Robert B., James A. Laramee, and H. Dupont Durst. 2005. “Versatile New Ion Source for the Analysis of Materials in Open Air Under Ambient Conditions.” Analytical Chemistry 77 (8): 2297–2302.
9. Day, Calvin J., Cathy Selvius DeRoo, and Ruth Ann Armitage. 2013. “Developing Direct Analysis in Real Time Time-of-Flight Mass Spectrometric Methods for Identification of Organic Dyes in Historic Wool Textiles.” In Archaeological Chemistry VIII, edited by R. A. Armitage and J. H. Burton, 69–85. Washington, DC: ACS.
10. Degano, Illaria, Erika Ribechini, Francesca Modugno, and Maria Perla Colombini. 2009. “Analytical Methods for the Characterization of Organic Dyes in Artworks and in Historical Textiles.” Applied Spectroscopy Reviews 44: 363–410.
11. Densmore, Frances. 1974. How Indians Use Wild Plants for Food, Medicine and Crafts. Original Edition, First published as Uses of plants by the Chippewa Indians in 44th Annual Report of the Bureau of American Ethnology to the Secretary of the Smithsonian Institution 1926–27, 275–397. Washington, DC: U.S. Government Printing Office New York: Dover.
12. Du Pratz, Le Page. 1972 [1758]. Histoire de la Lousiane. Translated from the French by T. Becket. Baton Rouge: Claitor's Publishing Division Paris: De Bure.
13. Geiger, Jordyn, Ruth Ann Armitage, and Cathy Selvius DeRoo. 2012. “Identification of Organic Dyes by Direct Analysis in Real Time-Time of Flight Mass Spectrometry.” In Collaborative Endeavors in the Chemical Analysis of Art and Cultural Heritage Materials, edited by P. L. Lang and R. A. Armitage, 123–129. American Chemical Society, Washington D.C.
14. Green, F. M., T. L. Salter, P. Stokes, I. S. Gilmore, and G. O'Connor. 2010. “Ambient Mass Spectrometry: Advances and Applications in Forensics.” Surface and Interface Analysis 42 (5): 347–357.
15. Hamilton, Henry W., B. Griffin James, and Charles C. Willoughby. 1952. “The Spiro Mound.” The Missouri Archaeologist 14 (1): 1–5.
16. Hariot, Thomas. 1966 [1590]. A Brief and True Report of the New Found Land of Virginia. Facsimile Edition of the 1588 Quarto. New York: History Book Club.
17. Hinkle, K. 1984. Ohio Hopewell Textiles: A Medium for the Exchange of Social and Stylistic Information, Unpublished M.S. thesis, Department of Anthropology, University of Arkansas, Fayetteville.
18. Hofenk de Graaff, Judith H. 2004. The Colourful Past: Origins, Chemistry and Identification of Natural Syestuffs. London: Archetype.
19. Jakes, Kathryn A., and Annette G. Ericksen. 2001. “Prehistoric Use of Sumac and Bedstraw as Dye Plants in Eastern North America.” Southeastern Archaeology 20 (1): 56–66.
20. Jakes, Kathryn A., Jack E. Katon, and Pamela A. Martoglio. 1991. “Identification of Dyes and Characterization of Fibers by Infrared and Visible Microspectroscopy: Application to Paracas Textiles.” In Archaeometry ’90, edited by G. A. Wagner and E. Pernicka. Basel: Birkhäuser: 305–315.
21. Jakes, Kathryn A., Lucy R. Sibley, and Richard W. Yerkes. 1994. “A Comparative Collection for the Study of Fibres Used in Prehistoric Textiles from Eastern North America.” Journal of Archaeological Science 21 (5): 641–650.
22. Jones, Roger W., Robert B. Cody, and John F. McClelland. 2006. “Differentiating Writing Inks Using Direct Analysis in Real Time Mass Spectrometry.” Journal of Forensic Sciences 51 (4): 915–918.
23. Karapanagiotis, Ioannis, and Yannis Chryssoulakis. 2005. “Investigation of Red Natural Dyes in Historical Objects by HPLC-DAD-MS.” Annali Di Chimica 96 (1-2): 75–84.
24. King, Mary Elizabeth, and Jane S. Gardner. 1981. “The Analysis of Textiles from Spiro Mound, Oklahoma.” In The Research Potential of Anthropological Museum Collections, edited by Anne-Marie E. Cantwell, James B. Griffin, and Nan A. Rothschild, 123–139. New York: New York Academy of Sciences.
25. Lech, Katarzyna, Katarzyna Połeć-Pawlak, and Maciej Jarosz. 2009. “Characterization of Organic Natural Dyes by Electrospray Mass Spectrometry Coupled with HPLC and/or Capillary Electrophoresis.” In Organic Mass Spectrometry in Art and Archaeology, edited by Maria Perla Colombini and Francesca Modugno, 365–388. Wiley, Chichester.
26. Lewis, Theodore H. 1907. “The Narrative of the Expedition of Hernando de Soto, by the Gentleman of Elvas.” In Spanish Explorers in the Southern United States, edited by J. F. Jameson, 133–272. New York: Charles Scribner's Sons.
27. Manhita, Ana, Teresa Ferreira, António Candeias, and Cristina Barrocas Dias. 2011. “Extracting Natural Dyes from Wool – An Evaluation of Extraction Methods.” Analytical and Bioanalytical Chemistry 400: 1501–1514.
28. Mantzouris, Dimitrios, Ioannis Karapanagiotis, Lemonia Valianou, and Costas Panayiotou. 2011. “HPLC-DAD-MS Analysis of Dyes Identified in Textiles from Mount Athos.” Analytical and Bioanalytical Chemistry 399 (9): 3665–3679.
29. Martoglio, Pamela A., Steven P. Bouffard, André J. Sommer, Jack E. Katon, and Kathryn A. Jakes. 1990. “Unlocking the Secrets of the Past: The Analysis of Archaeological Textiles and Dyes.” Analytical Chemistry 62 (21): 1123A–1128A.
30. Martoglio, Pamela A., Kathryn A. Jakes, and Jack E. Katon. 1992. “The Use of Infrared Microspectroscopy in the Analysis of Etowah Textiles: Evidence of Dye Use and Pseudomorph Formation.” In Proceedings of the 50th Annual Meeting of the Electron Microscopy Society of America, edited by W. Bailey, J. Bentley, and J. A. Small, 1534–1535, San Francisco: Microbeam Analysis Society.
31. Mills, William C. 1909. “Exploration of Seip Mound.” Ohio Archaeological and Historical Quarterly 18: 269–313.
32. Moerman, Dan. 2014. “Native American Ethnobotany: A Database of Foods, Drugs, Dyes and Fibers of Native American Peoples, Derived from Plants.” Accessed August 8. http://herb.umd.umich.edu/.
33. Musah, Rabi A., Marek A. Domin, Maureen A. Walling, and Jason R. E. Shepard. 2012. “Rapid Identification of Synthetic Cannabinoids in Herbal Samples Via Direct Analysis in Real Time Mass Spectrometry.” Rapid Communications in Mass Spectrometry 26 (9): 1109–1114.
34. Selvius DeRoo, Cathy, and Ruth Ann Armitage. 2011. “Direct Identification of Dyes in Textiles by Direct Analysis in Real Time-Time of Flight Mass Spectrometry.” Analytical Chemistry 83 (18): 6924–6928.
35. Shetrone, Henry C., and Emerson F. Greenman. 1931. “Exploration of the Seip Group of Prehistoric Earthworks.” Ohio Archaeological and Historical Quarterly 40: 343–509.
36. Song, Chuensoon. 1991. “Variations in Fiber Morphology of Prehistoric Textiles from the Seip Group of Mounds: A Model for Explanation.”, Unpublished Ph.D. dissertation, Department of Textiles and Clothing, The Ohio State University, Columbus.
37. Song, Chuensoon, Kathryn A. Jakes, and Richard W. Yerkes. 1996. “Seip Hopewell Textile Analysis and Cultural Implications.” Midcontinental Journal of Archaeology 21: 247–266.
38. Steiner, Robert R., and Robyn L. Larson. 2009. “Validation of the Direct Analysis in Real Time Source for Use in Forensic Drug Screening.” Journal of Forensic Sciences 54 (3): 617–622.
39. Struever, Stuart, and Gail L. Houart. 1972. “An analysis of the Hopewell Interaction Sphere.” In Social Exchange and Interaction, edited by E. N. Wilmsen, 47–79. Ann Arbor: Museum of Anthropology, University of Michigan.
40. Surowiec, Izabella, Bogdan Szostek, and Marek Trojanowicz. 2007. “HPLC-MS of Anthraquinoids, Flavonoids, and Their Degradation Products in Analysis of Natural Dyes in Archeological Objects.” Journal of Separation Science 30: 2070–2079.
41. Swider, Joseph R. 2013. “Optimizing Accu Time-of-Flight/Direct Analysis in Real Time for Explosive Residue Analysis.” Journal of Forensic Sciences 58 (6): 1601–1606.
42. Thompson, Amanda J. 2003. “Textiles as Indicators of Hopewellian Culture Burial Practices.”, Unpublished Ph.D. dissertation, Department of Textiles and Clothing, The Ohio State University, Columbus.
43. Thompson, Amanda J., and Kathryn A. Jakes. 2005. “Textile Evidence for Ohio Hopewell Burial Practices.” Southeastern Archaeology 24 (2): 137–141.
44. Thompson, Amanda Jo, and Kathryn A. Jakes. 2002. “Replication of Textile Dyeing with Sumac and Bedstraw.” Southeastern Archaeology 21 (2): 252–256.
45. Valianou, Lemonia, Ioannis Karapanagiotis, and Yannis Chryssoulakis. 2009. “Comparison of Extraction Methods for the Analysis of Natural Dyes in Historical Textiles by High-Performance Liquid Chromatography.” Analytical and Bioanalytical Chemistry 395: 2175–2189.
46. Willoughby, Charles C. 1938. “Textile Fabrics from the Burial Mounds of the Great Earthwork Builders in Ohio.” Ohio State Archaeological and Historical Quarterly 47: 273–287.
47. Wouters, Jan, C. M. Grzywacz, and Ana Claro. 2011. “A Comparative Investigation of Hydrolysis Methods to Analyze Natural Organic Dyes by HPLC-PDA.” Studies in Conservation 56: 231–249.
48. Zhang, X., and Robert Laursen. 2009. “Application of LC-MS to the Analysis of Dyes in Objects of Historical Interest.” International Journal of Mass Spectrometry 284 (1-3): 108–114.
49. Zhang, X., and Robert A. Laursen. 2005. “Development of Mild Extraction Methods for the Analysis of Natural Dyes in Textiles of Historical Interest Using LC-Diode Array Detector-MS.” Analytical Chemistry 77 (7): 2022–2025.