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Volumn 10, Issue 5, 1973, Pages 821-826

Bridgehead nitrogen heterocycles. VI. The reaction of 1‐amino‐ and 1,2‐diaminopyridinium salts with β‐dicarbonyl compounds

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EID: 84987336707     PISSN: 0022152X     EISSN: 19435193     Source Type: Journal    
DOI: 10.1002/jhet.5570100525     Document Type: Article
Times cited : (28)

References (17)
  • 16
    • 84987376793 scopus 로고    scopus 로고
    • Ir spectra were determined using either a Perkin‐Elmer Model 421 or Perkin‐Elmer Model 337 recording spectrophotometer. Uv spectra were measured on a Cary‐14 Spectrophotomer. Nmr spectra were determined using a Varian A‐60 spectrometer and chemical shifts are reported in δ units using tetramethylsilane as an internal standard and standard calibration procedures. Mass spectra were determined on a Hitachi Perkn‐Elmer RMU‐6E mass spectrometer at 70 eV unless stated otherwise, all samples being introduced via a direct inlet (ca. 200°) system. Microanalyses were performed by Galbraith Laboratories, Inc., Knoxville, Tennessee. The identity of products was established by means of superimposable infrared spectra and less than 2° depression in a mixture melting point determination. All evaporations were done under reduced pressure using a rotatory evaporator. All melting points were determined in capillaries.


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