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Volumn 41, Issue 4, 1994, Pages 467-471

Asymmetric Reduction Using Lithium Aluminum Hydride Modified with Chiral Ligands Prepared from (1R)‐(‐)‐β‐Pinene

Author keywords

(1R) ( ) pinene, (1R) ( ) myrtenyl bromide; Aminodiol; Asymmetric reduction; Lithium aluminum hydride

Indexed keywords

EID: 84986518905 PISSN: 00094536 EISSN: 21926549 Source Type: Journal
DOI: 10.1002/jccs.199400061 Document Type: Article

Times cited : (8)

References (25)

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- The enantiomeric excesses of the alcohols derived from acetophenone, propiophenone, and butyrophenone were also estimated by HPLC analysis of the corresponding 3,5‐dinitrobenzoates on a covalent D‐naphthylalanine column (Regis Pirkle, length 25 cm × 4.6 mm) using 2‐propanol/hexane (1/500) mixture as the mobile phase (flow rate: 1.0 mL/min), The retention times for the 3,5‐dinitrobenzoates for the alcohols are listed below: (S)‐(‐)‐1‐phenylethanol, 43.02 min; (R)‐(+)‐1‐phenylethanol, 44.16 min; (S)‐(‐)‐1‐phenylpropanol, 36.67 min; (R)‐(+)‐1‐phenylpropanol, 38.18 min; (S)‐(‐)‐1‐phenylbutanol, 32.45 min; (R)‐(+)‐1‐phenylbutanol, 33.80 min. UV detector was monitored at 254 nm.

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