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Volumn 25, Issue 7, 1986, Pages 640-642

Nickelacyclobutabenzene Compounds by Oxidative Addition of Cyclopropabenzene to Nickel(0) Compounds

Author keywords

[No Author keywords available]

Indexed keywords

EID: 84985520825 PISSN: 05700833 EISSN: 15213773 Source Type: Journal
DOI: 10.1002/anie.198606401 Document Type: Article

Times cited : (44)

References (26)

4
- 0002004273
- The Olefin Metathesis Reaction
- (1978) Prog. Inorg. Chem. , vol.24 , pp. 1
- Grubbs, R.H.¹

5
- 0000097544
- (1981) J. Am. Chem. Soc. , vol.103 , pp. 2448
- Tulip, T.H.¹ Thorn, D.L.²

11
- 0010902061
- Metallacyclische Vierringsysteme: Zwei unabhängige Wege zu Bis(cyclopentadienyl)titanacyclobutabenzol
- (1986) Angewandte Chemie , vol.98 , pp. 641
- de Boer, H.J.R.¹ Akkerman, O.S.² Bickelhaupt, F.³ Erker, G.⁴ Czisch, P.⁵ Mynott, R.⁶ Wallis, J.M.⁷ Krüger, C.⁸

14
- 0011563649
- Nickel-induzierte Cyclotetramerisierung von Cyclopropabenzol zu 1,6:7,12:13,18:19,24-Tetrakismethano[24]annulen
- (1986) Angewandte Chemie , vol.98 , pp. 374
- Mynott, R.¹ Neidlein, R.² Schwager, H.³ Wilke, G.⁴

17
- 84985523359
- 5a: 1 (0.5 mL, 4.85 mmol) was added to a vigorously stirred solution of 2a (1.67 g, 4.14 mmol) in 60 mL of pentane under argon at −20°C. The reaction mixture was then allowed to warm to room temperature and stirred for 30 min. After the reaction mixture had been concentrated to 20 mL and a slightly amorphous precipitate removed, the filtrate was cooled slowly to −78°C and allowed to stand for 1 week at this temperature. The crystals that separated out were filtered off, washed once with cold pentane, and dried at a maximum temperature of −20°C under high vacuum. Yield: 1.21 g (3.14 mmol, 76%) greenish brown crystals.

19
- 84985589974
- 4 frit, washed with ether, and then dried at room temperature under high vacuum. Yield: 936 g (1.39 mmol, 80%) of yellow microcrystals.

20
- 0001635157
- Tris(äthylen)nickel(0)
- (1973) Angewandte Chemie , vol.85 , pp. 620
- Fischer, K.¹ Jonas, K.² Wilke, G.³

22
- 84985589956
- 2O, and dried at −20°C under high vacuum. Yield: 770 mg (2.91 mmol, 70%) of greenish brown microcrystals.

23
- 84985580347
- The elemental analyses are in agreement with the empirical formulas.

24
- 84985580357
- NMR data collection, NMR‐Labor, Max‐Planck‐Institut für Kohlenforschung, Kaiser‐Wilhelm‐Platz 1, D‐4330 Mülheim a. d. Ruhr (FRG).

26
- 84982334957
- Übergangsmetallkomplexe, I. Olefin-Komplexe des Nickels(0)
- (1966) Justus Liebigs Annalen der Chemie , vol.699 , pp. 1
- Bogdanovic, B.¹ Kröner, M.² Wilke, G.³

* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.