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84984933756
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1H NMR spectrum was about 100
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1H NMR spectrum was about 100.
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23
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84984933757
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2Na (10 mM). Poly(methyl methacrylate) was used as the standard for calibration
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2Na (10 mM). Poly(methyl methacrylate) was used as the standard for calibration.
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24
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84984931032
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note
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Samples for DSC analyses were prepared as follows: A mixture (0.10 g) of poly(HMPA) 1 with commodity polymer at a desired ratio was dissolved in small amount of chloroform. The solution was then reprecipitated into large amount of n-hexane to give a pale yellow solid. After filtration and freeze-drying of the mixture, the resulting solid was dried in vacuo and the sample was obtained as a pale yellow powder or gum.
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