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Angewandte Chemie International Edition in English

Volumn 13, Issue 2, 1974, Pages 141-142

The Synthesis of Tetradehydrobenzocyclotetradecenes(“Benzodidehydro[14]annulenes”). The Effect of Benzoannelation on the Diamagnetic Ring Current of Macrocyclic (4n + 2) π‐Electron Systems

(2) Weavers, Rex T a,b Sondheimer, Franz a

a UNIVERSITY COLLEGE LONDON (United Kingdom)

b UNIVERSITY OF OTAGO (New Zealand)

Author keywords

[No Author keywords available]

Indexed keywords

EID: 84982360156 PISSN: 05700833 EISSN: 15213773 Source Type: Journal
DOI: 10.1002/anie.197401411 Document Type: Article

Times cited : (14)

References (22)

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- 4, 100 MHz: τ = 2.88 (2H/m, benzenoid), 3.08 (2H/m, benzenoid), 3.68 (2H/d, J = 12.5 Hz, olefinic), 4.32 (2H/broad d, J = 12.5 Hz, olefinic), 7.65 (4H/m, allylic), 7.95 (4 H/m, allylic), and 8.3(8H/m, nonallylic)] showed it to be atropic, and it is presumably a nonplanar molecule.

15
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- 1H‐NMR spectrum of 4 was essentially temperature independent in the range −80 to 60°.

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