Production techniques of nanoparticles on a laboratory scale

Nanotechnology Commercialisation

Volumn , Issue , 2013, Pages 73-138

  Sudarsanam, Putla ^a   Reddy, Benjaram M ^a  

^a INDIAN INSTITUTE OF CHEMICAL TECHNOLOGY   (India)

Author keywords

[No Author keywords available]

Indexed keywords

NANOTECHNOLOGY;

PRODUCTION TECHNIQUES;

NANOSTRUCTURED MATERIALS;

EID: 84974686205     PISSN: None     EISSN: None     Source Type: Book    
DOI: 10.4032/9789814303293     Document Type: Chapter

References (201)

1. Abdelsayed, V., Aljarasah, A., El-Shall, M. S., Al-Othman, Z. A., and Alghamdi, A. H. (2009). Microwave synthesis of bimetallic nanoalloys and CO oxidation on ceria-supported nanoalloys, Chem. Mater., 21, pp. 2825-2834.
2. Abelló, S., and Pérez-Ramírez, J. (2006). Characteristics by a miniaturized in-line dispersion-precipitation method: application to hydrotalcite synthesis, Adv. Mater., 18, pp. 2436-2439.
3. Abelló, S., Mitchell, S., Santiago, M., Stoica, G., and Pérez-Ramírez, J. (2010). Perturbing the properties of layered double hydroxides by continuous coprecipitation with short residence time, J. Mater. Chem., 20, pp. 5878-5887.
4. Ajaal, T., Smith, R. W., and Yen, W. T. (2002). The development and characterization of a ball mill for mechanical alloying, Can. Metallurgical Q., 41, pp. 7-14.
5. 3 nanocatalyst at a low temperature using single reverse microemulsion, Catal. Today, 164, pp. 209-213.
6. Andersson, M., Pedersen, J., and Palmqvist, A. (2005). Silver nanoparticle formation in microemulsions acting both as template and reducing agent, Langmuir, 21, pp. 11387-11396.
7. Atkinso, A., and Sega, D. L. (1998). Some recent developments in aqueous sol-gel processing, J. Sol-Gel Sci. Technol., 13, pp. 133-139.
8. Baranwal, R., Villar, M. P., Garcia, R., and Laine, R. M. (2001). Flame spray pyrolysis of precursors as a route to nano-mullite powder:powder characterization and sintering behavior, J. Am. Ceram. Soc., 84, pp. 951-961.
9. Behrens, M., Kissner, S., Girsgdies, F., Kasatkin, I., Hermerschmidt, F., Mette, K., Ruland, H., Muhler, M., and Schlögl, R. (2011). Knowledgebased development of a nitrate-free synthesis route for Cu/ZnO methanol synthesis catalysts via formate precursors, Chem. Commun., 47, pp. 1701-1703.
10. Bitter, J. H., van der Lee, M. K., Slotboom, A. G. T., van Dillen, A. J., and de Jong, K. P. (2003). Synthesis of highly loaded highly dispersed nickel on carbon nanofibers by homogeneous deposition-precipitation, Catal. Lett., 89, pp. 139-142.
11. 2 (Me=B, Al, Ga, In) mixed oxide catalysts. Preparation by sol-gel method, Chem. Mater., 20, pp. 1585-1596.
12. 2 powders with high surface area and high-temperature stabilities, Langmuir, 20, pp. 11223-11233.
13. Burattin, P., Che, M., and Louis, C. (1997). Characterization of the Ni(II) phase formed on silica upon deposition-precipitation, J. Phys. Chem. B, 101, pp. 7060-7074.
14. Burda, C., Chen, X., Narayanan, R., and EI-Sayed, M. A. (2005). Chemistry and properties of nanocrystals of different shapes, Chem. Rev., 105, pp. 1025-1102.
15. Cabanas, A., and Poliakoff, M. (2001). The continuous hydrothermal synthesis of nano-particulate ferrites in near critical and supercritical water, J. Mater. Chem., 11, pp. 1408-1416.
16. Calandra, P., Longo, A., and Liveri, V. T. (2003). Synthesis of ultrasmall ZnS nanoparticles by solid-solid reaction in the confined space of AOT reversed micelles, J. Phys. Chem. B, 107, pp. 25-30.
17. 4 nanocrystals synthesized by a nonaqueous sol-gel route, Chem. Mater., 20, pp. 5781-578.
18. Carroll, K. J., Reveles, J. U., Shultz, M. D., Khanna, S. N., and Carpenter, E. E. (2011). Preparation of elemental Cu and Ni nanoparticles by the polyol method: an experimental and theoretical approach, J. Phys. Chem. C, 115, pp. 2656-2664.
19. Chaianansutcharit, S., Mekasuwandumrong, O., and Praserthdam. P. (2006). Effect of organic solvents on iron oxide nanoparticles by the solvothermal method, Cryst. Growth Des., 6, pp. 40-45.
20. Chen, J. S., Zhu, T., Hu, Q. H., Gao, J. J., Su, F. B., Qiao, S. Z., and Lou, X. W. (2010). Shape-controlled synthesis of cobalt-based nanocubes, nanodiscs, and nanoflowers and their comparative lithium-storage properties, ACS Appl. Mater. Interfaces, 2, pp. 3628-3635.
21. Chen, S., and Carroll, D. L. (2002). Synthesis and characterization of truncated triangular silver nanoplates, Nano Lett., 2, pp. 1003-1007.
22. 3+ hollow nanophosphors using carbon nanospheres as hard templates, J. Colloid Interf. Sci., 346, pp. 8-11.
23. Chervin, C. N., Clapsaddle, B. J., Chiu, H. W., Gash, A. E., Satcher, J. H., and Kauzlarich, S. M. (2006). Role of cyclic ether and solvent in a non-alkoxide sol-gel synthesis of Yttria-stabilized zirconia nanoparticles, Chem. Mater., 18, pp. 4865-4874.
24. Chytil, S., Glomm, W. R., Kvande, I., Zhao, T., Walmsley, J. C., and Blekkan, E. A. (2007). Platinum incorporated into the SBA-15 mesostructure via depositionprecipitation method: Pt nanoparticle size estimation and catalytic testing, Top. Catal., 45, pp. 93-99.
25. Cortie, M. B., and van der Lingen, E. (2002). Catalytic gold nanoparticles, Mater. Forum, 26, pp. 1-14.
26. 4 (A=Co, Ni, and Zn), J. Mater. Chem., 21, pp. 10206-10218.
27. Curri, M. L, Agostiano, A., Manna, L., Della, M. M., Catalano, M., Chiavarone, L., Spagnolo, V., and Lugara, M. (2000). Synthesis and characterization of CdS nanoclusters in a quaternary microemulsion:The role of the cosurfactant, J. Phys. Chem. B, 104, pp. 8391-8397.
28. Cushing, B. L., Kolesnichenko, V. L., and O'Connor, C. J. (2004). Recent advances in the liquid-phase syntheses of inorganic nanoparticles, Chem. Rev., 104, pp. 3893-3946.
29. Das, S. K., Bhunia, M. K., Sinha, A. K., and Bhaumik, A. (2009). Selfassembled mesoporous zirconia and sulfated zirconia nanoparticles synthesized by triblock copolymer as template, J. Phys. Chem. C, 113, pp. 8918-8923.
30. 3 nanoparticles with highly reactive surface and enhanced magnetization, J. Phys. Chem. C, 115, pp. 7209-7217.
31. + ion storage, Chem. Mater., 20, pp. 1841-1846.
32. Dingsheng, W., Ting, X., and Yadong, L. (2009). Nanocrystals: solutionbased synthesis and applications as nanocatalysts, Nano Res., 2, pp. 30-46.
33. Djerdj, I., Garnweitner, G., Su, D. S., and Niederberger, M. (2007). Morphology-controlled nonaqueous synthesis of anisotropic lanthanum hydroxide nanoparticles, J. Solid State Chem., 180, pp. 2154-2165.
34. Djerdj, I., Arcon, D., Jaglicic, Z., and Niederberger, M. (2008). Nonaqueous synthesis of metal oxide nanoparticles: Short review and doped titanium dioxide as case study for the preparation of transition metal-doped oxide nanoparticles, J. Solid State Chem., 181, pp. 1571-1581.
35. Duan, X., Lian, J., Ma, J., Kim, T., and Zheng, W. (2010). Shape-controlled synthesis of metal carbonate nanostructure via ionic liquid-assisted hydrothermal route: the case of manganese carbonate, Cryst. Growth Des., 10, 4449-4455.
36. Eastoe, J., Hollamby, M. J., and Hudson, L (2006). Recent advances in nanoparticle synthesis with reversed micelles, Adv. Colloid. Interface. Sci., 128-130, pp. 5-15.
37. Endres, F., and Abedin, S. Z. E. (2006). Air and water stable ionic liquids in physical chemistry, Phys. Chem. Chem. Phys., 8, pp. 2101-2116.
38. Estruga, M., Domingo, C., and Ayllón, J. A. (2010). Microwave radiation as heating method in the synthesis of titanium dioxide nanoparticles from hexafluorotitanate-organic salts, Mater. Res. Bull., 45, pp. 1224-1229.
39. Fang, X. L., Li, Y., Chen, C., Kuang, Q., Gao, X. Z., Xie, Z. X., Xie, S. Y., Huang, R. B., and Zheng, L. (2010). pH-Induced simultaneous synthesis and self-assembly of 3D layered β-FeOOH nanorods, Langmuir, 26, pp. 2745-2750.
40. Feldmann, C., and Metzmacher, C. (2001). Polyol mediated synthesis of nanoscale MS particles (M~Zn, Cd, Hg), J. Mater. Chem., 11, pp. 2603-2606.
41. Fernandez, C. A., and Wai, C. M. (2007). Continuous tuning of cadmium sulfide and zinc sulfide nanoparticle size in a water-in supercritical carbon dioxide microemulsion, Chem. Eur. J., 13, pp. 5838-5844.
42. Fischer, A., Müller, J. O., Antonietti, M., and Thomas, A. (2008). Synthesis of ternary metal nitride nanoparticles using mesoporous carbon nitride as reactive template, ACS Nano, 2, pp. 2489-2496.
43. Fonseca, G. S., Umpierre, A. P., Fichtner, P. F. P., Teixeira, S. R., and Dupont, J. (2003). The use of imidazolium ionic liquids for the formationand stabilization of Ir0 and Rh0 nanoparticles: efficient catalysts for the hydrogenation of arenas, Chem. Eur. J., 9, pp. 3263-3269.
44. 2 solid solutions by a citrate complexation route: a thermochemical and structural study, J. Phys. Chem. C, 113, pp. 914-924.
45. Gaffet, E., Bernard, F., Niepce, J. C., Charlot, F., Gras, C., Le Caer, G., Guichard, J. L., Delcroix, P., Mocellin, A., and Tillement, O. (1999). Some recent developments in mechanical activation and mechanosynthesis, J. Mater. Chem., 9, pp. 305-314.
46. Gao, X., Du, Y., Liu, X., and Xu, P. (2011). Synthesis and characterization of Co-Sn substituted barium ferrite particles by a reverse microemulsion technique, Mater. Res. Bull., 46, pp. 643-648.
47. Ge, J. P., Xu, S., Liu, L. P., and Li, Y. D. (2006). Formation of disperse nanoparticles at the oil/water Interface in normal microemulsions, Chem. Eur. J., 12, pp. 6552-6558.
48. Gerbec, J. A., Magana, D., Washington, A., and Strouse, G. F. (2005). Microwave-enhanced reaction rates for nanoparticle synthesis, J. Am. Chem. Soc., 127, pp. 15791-15800.
49. 2 prepared by deposition precipitation with urea: improved activity and stability in CO oxidation, J. Phys. Chem. C, 113, pp. 9710-9720.
50. Gonsalves, K. E., Rangarajan, S. P., and Wang, J. (2002). Nanostructured Materials and Nanotechnology, ed. Hari, S. N., Chapter 1 "Chemical synthesis of nanostructured metal, metal alloys, and semicoductors", (Academic Press, San Diego) pp. 1-56.
51. 2, J. Mater. Chem., 13, pp. 342-346.
52. 2 nanoparticles, Inorg. Chem., 42, pp. 7148-7155.
53. Grocholl, L., Wang, J., and Gillan, E. G. (2001). Solvothermal azide decomposition route to GaN nanoparticles, nanorods, and faceted crystallites, Chem. Mater., 13, pp. 4290-4296.
54. 2 by mechanochemical and water-in-oil microemulsion methods, Mater. Lett., 61, pp. 93-96.
55. 3 nanoparticles by hydrothermal synthesis, Ind. Eng. Chem. Res., 44, pp. 840-846.
56. Han, Y. C., Li, S. P., Wang, X. Y., and Chen, X. M. (2004). Synthesis and sintering of nanocrystalline hydroxyapatite powders by citric acid sol-gel combustion method, Mater. Res. Bull., 39, pp. 25-32.
57. Han, Y. S., Fuj, M., Shchukin, M., Mohwald, H., and Takahashi, M. (2009). A new model for the synthesis of hollow particles via the bubble templating method, Cryst. Growth Des., 9, pp. 3771-3775.
58. Haruta, M. (1997). Novel catalysis of gold deposited on metal oxides, Catal. Surv. Jpn, 1, pp. 161-173.
59. Hayashi, H., and Hakuta, Y. (2010). Hydrothermal synthesis of metal oxide nanoparticles in supercritical water, Materials, 3, pp. 3794-3817.
60. Jia, F. L., Zhang, L. Z., Shang, X. Y., and Yang, Y. (2008). Non-aqueous sol-gel approach towards the controllable synthesis of nickel nanospheres, nanowires, and nanoflowers, Adv. Mater., 20, pp. 1050-1054.
61. 3 nanostructures by an ionic liquidassisted templating route: Synthesis, formation mechanism, and properties, Chem. Mater., 17, pp. 6094-6100.
62. Jiang, J. Z., and Cai, C. (2006). In situ formation of dispersed palladium nanoparticles in microemulsion: efficient reaction system for ligand-free Heck reaction, J. Colloid Interf. Sci., 299, pp. 938-943.
63. Joo, S. H., Park, J. Y., Renzas, J. R., Butcher, D. R., Huang, W., and Somorjai, G. A. (2010). Size effect of ruthenium nanoparticles in catalytic carbon monoxide oxidation, Nano Lett., 10, pp. 2709-2713.
64. Kaneko, K., Inoke, K., Freitag, B., Hungria, A. B., Midgley, P. A., Hansen, T. W., Zhang, J., Ohara, S., and Adschiri, T. (2007). Structural and morphological characterization of cerium oxide nanocrystals prepared by hydrothermal synthesis, Nano Lett., 7, pp. 421-425.
65. Kapoor, M. P., and Matsumura, Y. (2000). Liquid phase methanol carbonylation catalysed over rhodium supported on hydrotalcite, Chem. Commun., pp. 95-96.
66. 2 mixed oxides, Micropor. Mesopor. Mater., 44-45, pp. 565-572.
67. 3 via forced precipitation in an organic solvent, Chem. Eur. J., 10, pp. 925-932.
68. Khodakov, A. Y., Chu, W., and Fongarland, P. (2007). Advances in the development of novel cobalt fischer-tropsch catalysts for synthesis of long-chain hydrocarbons and clean fuels, Chem. Rev., 107, pp. 1692-1744.
69. Kim, J. R., Myeong, W. J., and Ihm, S.K. (2007). Characteristics in oxygen storage capacity of ceria-zirconia mixed oxides prepared by continuous hydrothermal synthesis in supercritical water, Appl. Catal. B, 71, pp. 57-63.
70. Kim, K. S., Demberelnyamba, D., and Lee, H. (2004). Size-selective synthesis of gold and platinum nanoparticles using novel thiolfunctionalized ionic liquids, Langmuir, 20, pp. 556-560.
71. 3)1-x tie-line by liquid-feed flame spray pyrolysis (LF-FSP), Chem. Mater., 20, pp. 5154-5162.
72. 3] nanopowders via liquid-feed flame spray pyrolysis (LF-FSP), J. Am. Chem. Soc., 131, pp. 9220-9229.
73. Kloprogge, J. T., Weier, M. L., Duong, L. V., and Frost, R. L. (2004). Microwave-assisted synthesis and characterisation of divalent metal tungstate nanocrystalline minerals: ferberite, hübnerite, sanmartinite, scheelite and stolzite, Mater. Chem. Phys., 88, pp. 438-443.
74. Kominami, H., Miyakawa, M., Murakami, S., Yasuda, T., Kohno, M., Onoue, S., Kera, Y., and Ohtani, B. (2001). Solvothermal synthesis of tantalum(V) oxide nanoparticles and their photocatalytic activities in aqueous suspension systems, Phys. Chem. Chem. Phys., 3, pp. 2697-2703.
75. Kong, L. B., Ma, J., and Boey, F. (2002). Nanosized hydroxyapatite powders derived from coprecipitation process, J. Mater. Sci., 37, pp. 1131-1134.
76. Krumm, M., Pueyo, C. L., and Polarz, S. (2010). Monolithic zinc oxide aerogels from organometallic sol-gel precursors, Chem. Mater., 22, pp. 5129-5136.
77. Kwon, S. G., and Hyeon, T. (2008). Colloidal chemical synthesis and formation kinetics of uniformly sized nanocrystals of metals, oxides, and chalcogenides, Acc. Chem. Res., 41, pp. 1696-1709.
78. Lay, S., Qiu, Y., and Wang, S. (2006). Effects of the structure of ceria on the activity of gold/ceria catalysts for the oxidation of carbon monoxide and benzene, J. Catal., 237, pp. 303-313.
79. 2 synthesis of amorphous hydrous zirconia nanoparticles, and their calcination to zirconia, J. Am. Ceram. Soc., 89, pp. 3624-3630.
80. 2: using solution chemistry to access ternary intermetallic compounds as nanocrystals, J. Am. Chem Soc., 127, pp. 7326-7327.
81. Li, H., Liu, J., Xie, S., Qiao, M., Dai, W., and Li, H. (2008). Highly active Co-B amorphous alloy catalyst with uniform nanoparticles prepared in oil-in-water microemulsion, J. Catal., 259, pp. 104-110.
82. 2 and their gas sensor behaviors, Cryst. Growth Des., 8, pp. 4165-4172.
83. Li, Y., and Somorjai, G. A. (2010). Nanoscale advances in catalysis and energy applications, Nano Lett., 10, pp. 2289-2295.
84. Liang, H. W., Liu, S., and Yu, S. H. (2010). The controlled synthesis of one-dimensional inorganic nanostructures using pre-existing one-dimensional nanostructures as templates, Adv. Mater., 22, pp. 3925-3937.
85. 2, Langmuir, 20, pp. 2466-2471.
86. Lim, S. H., Phonthammachai, N., Zhong, Z. Y., Teo, J., and White, T. J. (2009). Robust gold-decorated silica-titania pebbles for lowtemperature CO catalytic oxidation, Langmuir, 25, pp. 9480-9486.
87. Longo, A., Liotta, L. F., Carlo, G. D., Giannici, F., Venezia, A. M., and Martorana, M. A. (2010). Structure and the metal support interaction of the Au/Mn oxide catalysts, Chem. Mater., 22, pp. 3952-3960.
88. Lv, J. P., Qu, L. Z., and Qu, B. J. (2004). Controlled growth of three morphological structures of magnesium hydroxide nanoparticles by wet precipitation method, J. Cryst. Growth, 267, pp. 676-684.
89. Ma, Y., and Qi, L. (2009). Solution-phase synthesis of inorganic hollow structures by templating strategies, J. Colloid Interf. Sci., 335, pp. 1-10.
90. Maedler, L., and Pratsinis, S. E. (2002). Bismuth oxide nanoparticles by flame spray pyrolysis, J. Am. Ceram. Soc., 85, pp. 1713-1718.
91. Mäkelä, J. M., Keskinen, H., Forsblom, T., and Keskinen, J. (2004). Generation of metal and metal oxide nanoparticles by liquid flame spray process, J. Mater. Sci., 39, pp. 2783-2788.
92. Mao, J., Li, X. L., Qin, W. J., Niu, K. Y., Yang, J., Ling, T., and Du, X. W. (2010). Control of the morphology and optical properties of ZnO nanostructures via hot mixing of reverse micelles, Langmuir, 26, pp. 13755-13759.
93. Maye, M. M., Lim, I. I. S., Luo, J., Rab, Z., Rabinovich, D., Liu, T., and Zhong, C. J. (2005). Mediator-template assembly of nanoparticles, J. Am. Chem. Soc., 127, pp. 1519-1529.
94. Migowski, P., Machado, G., Texeira, S. R., Alves, M. C. M., Morais, J., Traversec, A., and Dupont, J. (2007). Synthesis and characterization of nickel nanoparticles dispersed in imidazolium ionic liquids, Phys. Chem. Chem. Phys., 9, pp. 4814-4821.
95. Misra, N., Roy, M., Mohanta, D., Baruah, K. K., and Choudhury, A. (2008). Photochromism and magneto-optic response of ZnO:Mn semiconductor quantum dots fabricated by microemulsion route, Cent. Eur. J. Phys., 6, pp. 109-115.
96. Mohamed, M. B., AbouZeid, K. M., Abdelsayed, V., Aljarash, A., and El-Shall, M. S. (2010). Growth mechanism of anisotropic gold nanocrystals via microwave synthesis: Formation of dioleamide by gold nanocatalysis, ACS Nano, 4, pp. 2766-2772.
97. Mueller, R., Maedler, L., and Pratsinis, S. E. (2003). Nanoparticle synthesis at high production rates by fame spray pyrolysis, Chem. Eng. Sci., 58, pp. 1969-1976.
98. Mueller, R., Jossen, R., Pratsinis, E., Watson, M., and Akhtar, K. (2004). Zirconia nanoparticles made in spray flames at high production rates, J. Am. Ceram. Soc., 87, pp. 197-202.
99. Narayanan, R., and El-Sayed, M. A. (2005). Catalysis with transition metal nanoparticles in colloidal solution: Nanoparticle shape dependence and stability, J. Phys. Chem. B, 109, pp. 12663-12676.
100. Nares, R., Ramírez, J., Gutiérrez-Alejandre, A., Louis, C., and Klimova, T. (2002). Ni/Hβ-Zeolite catalysts prepared by depositionprecipitation, J. Phys. Chem. B, 106, pp. 13287-13293.
101. 3 from microto nanostructures and their upconversion luminescence, ACS Nano, 4, pp. 2263-2273.
102. Niederberger, M., and Garnweitner, G. (2006). Organic reaction pathways in the nonaqueous synthesis of metal oxide nanoparticles, Chem. Eur. J., 12, pp. 7282-7302.
103. Niederberger, M., Garnweitner, G., Buha, J., Polleux, J., Ba, J., and Pinna, N. (2006). Nonaqueous synthesis of metal oxide nanoparticles:review and indium oxide as case study for the dependence of particle morphology on precursors and solvents, J. Sol-Gel Sci. Technol., 40, pp. 259-266.
104. Niederberger, M. (2007). Sol-Gel routes to metal oxide nanoparticles, Acc. Chem. Res., 40, pp. 793-800.
105. 2 catalysts, Ind. Eng. Chem. Res., 50, pp. 2495-2500.
106. Oh, M. H., Lee, N., Kim, H., Park, S. P., Piao, Y., Lee, J., Jun, S. W., Moon, W. K., Choi, S. H., and Hyeon, T. (2011). Large-scale synthesis of bioinert tantalum oxide nanoparticles for X-ray computed tomography imaging and bimodal image-guided sentinel lymph node mapping, J. Am. Chem. Soc., 133, pp. 5508-5515.
107. 2 microemulsion, Chem. Commun., pp. 2353-2354.
108. Ohde, H., Hunt, F., and Wai, C. M. (2001). Synthesis of silver and copper nanoparticles in a water-in-supercritical-carbon dioxide microemulsion, Chem. Mater., 13, pp. 4130-4135.
109. 2 microemulsion, J. Am. Chem. Soc., 124, pp. 4540-4541.
110. 2 catalyst prepared by deposition-precipitation method, J. Catal., 208, pp. 485-489.
111. Patil, N. S., Uphade, B. S., McCulloh, D. G., Bhargava, S. K., and Choudhary, V. R. (2004). Styrene epoxidation over gold supported on different transition metal oxides prepared by homogeneous depositionprecipitation, Catal. Commun., 5, pp. 681-685.
112. Pinna, N., and Niederberger, M. (2008). Surfactant-free nonaqueous synthesis of metal oxide nanostructures, Angew. Chem. Int. Ed., 47, pp. 5292-5304.
113. Polshettiwar, V., Baruwati, B., and Varma, R. S. (2009). Self-assembly of metal oxides into three-dimensional nanostructures: Synthesis and application in catalysis, ACS Nano, 3, pp. 728-736.
114. Popa, A. F., Courtheoux, L., Gautron, E., Rossignol, S., and Kappenstein, C. (2005). Aerogel and xerogel catalysts based on θ-alumina doped with silicon for high temperature reactions, Eur. J. Inorg. Chem., pp. 543-554.
115. 4 nanoparticles, Mater. Lett., 60, pp. 3548-3552.
116. Rabenau, A. (1985). The role of hydrothermal synthesis in preparative chemistry, Angew. Chem. Int. Ed. Engl., 24, pp. 1026-1040.
117. Rajesh, K., Mukundan, P., Pillai P. K., Nair, V. R., and Warrier, K. G. K. (2004). High surface area nanocrystalline cerium phosphate through aqueous sol-gel route, Chem. Mater., 16, pp. 2700-2705.
118. Rao, K. J., Vaidhyanathan, B., Ganguli, M., and Ramakrishnan, P. A. (1999). Synthesis of inorganic solids using microwaves, Chem. Mater., 11, pp. 882-895.
119. Raveendran, P., Fu, J., and Wallen, S. L. (2003). Completely "green" synthesis and stabilization of metal nanoparticles, J. Am. Chem. Soc., 125, pp. 13940-13941.
120. 2 nanocomposite oxides, J. Phys. Chem. C, 111, pp. 10478-10483.
121. 2 (M=Zr & Hf) mixed oxides, J. Phys. Chem. C, 112, pp. 11729-11737.
122. Reddy, B. M., Saikia, P., Bharali, P., Yamada, Y., Kobayashi, T., Muhler, M., and Grünert, W. (2008). Structural characterization and catalytic activity of nanosized ceria-terbia solid solutions, J. Phys. Chem. C, 112, pp. 16393-16399.
123. Reddy, B. M., Bharali, P., and Saikia, P. (2009). New Nanotechniques, eds. Malik, A., and Rawat, R. J. Chapter 6 "A Comprehensive Overview Synthesis Techniques of Nanostructured Oxides," (Nova Science Publishers, New York), pp. 243-276.
124. Reddy, B. M., Gode, T., Lakshmi, K., Yamada, Y., and Park, S. E. (2009). Structural characterization and catalytic activity of nanocrystalline ceria-praseodymia solid solutions, J. Phys. Chem. C, 113, pp. 15882-15890.
125. 2 for CO oxidation, Catal. Lett., 130, pp. 227-234.
126. 3) by microwave-induced solution combustion synthesis-characterization and CO oxidation, J. Mater. Sci., 44, pp. 2743-2751.
127. 2) mixed oxides synthesized by microwave-induced solution combustion technique, J. Mater. Sci., 44, pp. 4874-4882.
128. 2-δ (x=0.2) solid solutions: Structural characteristics and catalytic performance, Chem. Mater., 22, pp. 467-475.
129. 2 mixed oxides prepared by a rapid microwave-assisted combustion synthesis method, J. Mol. Catal. A: Chem., 319, pp. 52-57.
130. 2-δ (M=Zr, Hf, Tb, and Pr) nanosized model solid solutions for CO oxidation, Catal. Lett., 141, pp. 572-581.
131. Richter, K., Birkner, A., and Mudring, A. V. (2010). Stabilizer-free metal nanoparticles and metal-metal oxide nanocomposites with long-term stability prepared by physical vapor deposition into ionic liquids, Angew. Chem. Int. Ed., 49, pp. 2431-2435.
132. 3, Mater. Res. Bull., 40, pp. 341-345.
133. Rosiyah, B. Y., Hiromichi, H., Takako, N., Takeo, E., Yoshio, O., and Norio, S. (2001). Hydrothermal synthesis of potassium hexatitanates under subcritical and supercritical water conditions and its application in photocatalysis, Chem. Mater., 13, pp. 842-847.
134. Roychowdhury, C., Matsumoto, F., Mutolo, P. F., Abruna, H. D., and DiSalvo, F. J. (2005). Synthesis, characterization, and electrocatalyticactivity of PtBi nanoparticles prepared by the polyol process, Chem. Mater., 17, pp. 5871-5876.
135. Ruckenstein, E. (1996). Microemulsions, macroemulsions, and the bancroft rule, Langmuir, 12, pp. 6351-6353.
136. Sagisaka, M., Iwama, S., Hasegawa, S., Yoshizawa, A., Mohamed, A., Cummings, S., Rogers, S. E., Heenan, R. K., and Eastoe, J. (2011). Super-efficient surfactant for stabilizing water-in-carbon dioxide microemulsions, Langmuir, 27, pp. 5772-5780.
137. Sanchez-Dominguez, M., Boutonnet, M., and Solans, C. (2009). A novel approach to metal and metal oxide nanoparticle synthesis: the oil-in-water microemulsion reaction method, J. Nanopart. Res., 11, pp. 1823-1829.
138. 2 nanoparticles by a novel oil-in-water microemulsion reaction method and their use as catalyst support for CO oxidation, Catal. Today, 158, pp. 35-43.
139. 4 nanoparticles by supercritical hydrothermal reaction, J. Supercritical Fluids, 53, pp. 92-94.
140. Schimmoeller, B., Schulz, H., Ritter, A., Reitzmann, A., Kraushaar, C. B., Baiker, A., and Pratsinis, S. E. (2008). Structure of flame-made vanadia/titania and catalytic behavior in the partial oxidation of o-xylene, J. Catal., 256, pp. 74-83.
141. Seo, D. J., Park, S. B., Kang, Y. C., and Choy, K. L. (2003). Formation of ZnO, MgO and NiO nanoparticles from aqueous droplets in flame reactor, J. Nanopart. Res., 5, pp. 199-210.
142. 4 prepared by a one-step mechanochemical route, Chem. Mater., 18, pp. 3057-3067.
143. 4 nanoparticles followed by 119Sn MAS NMR and 119Sn Mössbauer spectroscopy, Chem. Mater., 21, pp. 2518-2524.
144. Shchukin, D. G., and Caruso, R. A. (2004). Template synthesis and photocatalytic properties of porous metal oxide spheres formed by nanoparticle infiltration, Chem. Mater., 16, pp. 2287-2292.
145. Shen, L., Bao, N., Yanagisawa, K., Domen, K., Grimes, C. A., and Gupta, A. (2007). Controlled synthesis and assembly of nanostructured ZnO architectures by a solvothermal soft chemistry process, Cryst. Growth Des., 7, pp. 2742-2748.
146. 2 microemulsion for synthesis of carbon-nanotube-supported Pt electrocatalyst for the oxygen reduction reaction, Energy Fuels, 22, pp. 2543-2549.
147. Shylesh, S., Schünemann, V., and Thiel, W. R. (2010). Magnetically separable nanocatalysts: Bridges between homogeneous and heterogeneous catalysis, Angew. Chem. Int. Ed., 49, pp. 3428-3459.
148. Simentsova, I. I., Minyukova, T. P., Khassin, A. A., Dokuchits, E. V., Davydova, L. P., Yu, M. I., Plyasova, L. M., Kustova, G. N., and Yurieva, T. M. (2010). The effect of the precursor structure on the catalytic properties of the nickel-chromium catalysts of hydrogenation reactions, Russ. Chem. Bull., 59, pp. 2055-2060.
149. Smetana, A. B., Wang, J. S., Boeckl, J., Brown, G. J., and Wai, C. M. (2007). Fine-tuning size of gold nanoparticles by cooling during reverse micelle synthesis, Langmuir, 23, pp. 10429-10432.
150. Smolyakov, V. K., Lapshin, O. V., and Boldyrev, V. V. (2008). Mathematical simulation of mechanochemical synthesis in a macroscopic approximation, Theor. Found. Chem. Eng., 42, pp. 54-59.
151. 2 manostructures, J. Phys. Chem. B, 109, pp. 20207-20214.
152. Sue, K., Murata, K., Kimura, K., and Arai, K. (2003). Continuous synthesis of zinc oxide nanoparticles in supercritical water, Green Chem., 5, pp. 659-662.
153. Sue, K., Suzuki, M., Arai, K., Ohashi, T., Ura, H., Matsui, K., Hakuta, Y., Hayashi, H., Watanabe, M., and Hiaki, T. (2006). Size-controlled synthesis of metal oxide nanoparticles with a flow-through supercritical water method, Green Chem., 8, pp. 634-638.
154. Sun, Y., and Xia, Y. (2002). Shape-controlled synthesis of gold and silver nanoparticles, Science, 298, pp. 2176-2179.
155. Tago, T., Hatsuta, T., Miyajima, K., Kishida, M., Tashiro, S., and Wakabayashi, K. (2002). Novel synthesis of silica-coated ferrite nanoparticles prepared using water-in-oil microemulsion, J. Am. Ceram. Soc., 85, pp. 2188-2194.
156. Tan, G. L., and Yu, X. F. (2009). Capping the ball-milled CdSe nanocrystals for light excitation, J. Phys. Chem. C, 113, pp. 8724-8729.
157. Tang, E., Tian, B., Zheng, E., Fu, C., and Cheng, G. (2008). Preparation of zinc oxide nanoparticle via uniform precipitation method and its surface modification by methacryloxypropyltrimethoxysilane, Chem. Eng. Comm., 195, pp. 479-491.
158. 2 nanocrystals, Chem. Mater., 16, pp. 1336-1342.
159. Tani, T., Mädler, L., and Pratsinis, S. E. (2002). Homogeneous ZnO nanoparticles by flame spray pyrolysis, J. Nanopart. Res., 4, pp. 337-343.
160. Taniguchi, T., Watanabe, T., Sakamoto, N., Matsushita, N., and Yoshimura, M. (2008). Aqueous route to size-controlled and doped organophilic ceria nanocrystals, Cryst. Growth Des., 8, pp. 3725-3730.
161. Teoh, W. Y., Setiawan, R., Mädler, L., Grunwaldt, J. D., Amal, R., and Pratsinis, S. E. (2008). Ru-doped cobalt-zirconia nanocomposites by flame synthesis: Physicochemical and catalytic properties, Chem. Mater., 20, pp. 4069-4079.
162. 3 hollow nanoparticles: Size-related solid evacuation in Ostwald-ripeninginduced hollowing process, Cryst. Growth Des., 10, pp. 3990-3995.
163. Torimoto, T., Tsuda, T., Okazaki, K., and Kuwabata, S. (2010). New frontiers in materials science opened by ionic liquids, Adv. Mater., 22, pp. 1196-1221.
164. Tsuji, M., Hashimoto, M., Nishizawa, Y., Kubokawa, M., and Tsuji, T. (2005). Microwave-assisted synthesis of metallic nanostructures in solution, Chem. Eur. J., 11, pp. 440-452.
165. Tsuzuki, T., and McCormick, P. G. (2001). Synthesis of ultrafine ceria powders by mechanochemical processing, J. Am. Ceram. Soc., 84, pp. 1453-1458.
166. Tsuzuki, T., and McCormick, P. G. (2004). Mechanochemical synthesis of nanoparticles, J. Mater. Sci., 39, pp. 5143-5146.
167. Wang, C. J., Wu, Y. A., Jacobs, R. M. J., Warner, J. H., Williams, G. R., and O'Hare, D. (2011). Reverse micelle synthesis of Co-Al LDHs:Control of particle size and magnetic properties, Chem. Mater., 23, pp. 171-180.
168. Wang, H., Zhang, J. R., and Zhu, J. J. (2002). Sonochemical preparation of lead sulfide nanocrystals in an oil-in-water microemulsion, J. Cryst. Growth, 246, pp. 161-168.
169. Wang, H., Xu, X., Zhang, J., and Li, C. (2010). A Cost-effective coprecipitation method for synthesizing indium tin oxide nanoparticles without chlorine contamination, J. Mater. Sci. Technol., 26, pp. 1037-1040.
170. Wang, H. Q., and Nann, T. (2009). Monodisperse upconverting nanocrystals by microwave-assisted synthesis, ACS Nano, 3, pp. 3804-3808.
171. 2 nanorod supported gold nanoparticles with enhanced activity for solvent-free aerobic alcohol oxidation, J. Phys. Chem. C, 112, pp. 6981-6986.
172. Wang, Y., Wu, Q. S., and Ding, Y. P. (2004). Preparation of Group IIB selenide nanoparticles using soft-hard dual template method, J. Nanopart. Res., 6, pp. 253-257.
173. Wang, Y., and Yang, H. (2006). Oleic acid as the capping agent in the synthesis of noble metal nanoparticles in imidazolium-based ionic liquids, Chem. Commun., pp. 2545-2547.
174. Wang, Y., Maksimuk, S., Shen, R., and Yang, H. (2007). Synthesis of iron oxide nanoparticles using a freshly-made or recycled imidazoliumbased ionic liquid, Green Chem., 9, pp. 1051-1056.
175. Weidenhof, B., Reiser, M., Stöwe, K., Maier, W. F., Kim, M., Azurdia, J., Gulari, E., Seker, E., Barks, A., and Laine, R. M. (2009). Highthroughput screening of nanoparticle catalysts made by flame spray pyrolysis as hydrocarbon/NO oxidation catalysts, J. Am. Chem. Soc., 131, pp. 9207-9219.
176. Welton, T. (1999). Room temperature ionic liquids. Solvents for synthesis and catalysis, Chem. Rev., 99, pp. 2071-2083.
177. White, R. J., Luque, R., Budarin, V. L., Clark, J. H., and Macquarrie, D. J. (2009). Supported metal nanoparticles on porous materials. Methods and applications, Chem. Soc. Rev., 38, pp. 481-494.
178. 4 crystals in ultra-wide pH range conditions, J. Mater. Chem., 13, pp. 1223-1228.
179. Wu, M., Long, J., Huang, A., Luo, Y., Feng, S., and Xu, R. (1999). Microemulsion-mediated hydrothermal synthesis and characterization of nanosize rutile and anatase particles, Langmuir, 15, pp. 8822-8825.
180. Wu, M., Lin, G., Chen, D., Wang, G., He, D., Feng, S., and Xu, R. (2002). Sol-hydrothermal synthesis and hydrothermally structural evolution of nanocrystal titanium dioxide, Chem. Mater., 14, pp. 1974-1980.
181. 2 nanocrystal microspheres as novel adsorbents for wastewater treatment, J. Phys. Chem. C, 113, pp. 16625-16630.
182. 3+ phosphor, J. Phys. Chem. C, 113, pp. 21034-21041.
183. 3 nanocomposite materials, Chem. Mater., 19, pp. 4820-4826.
184. Xiong, L., and He, T. (2006). Synthesis and characterization of ultrafine tungsten and tungsten oxide nanoparticles by a reverse microemulsion-mediated method, Chem. Mater., 18, pp. 2211-2218.
185. 3 system with complex phase transitions: XRD and Raman studies, Phys. Chem. Chem. Phys., 6, pp. 5410-5418.
186. Xu, S., and Li, Y. (2003). Different morphology at different reactant molar ratios: synthesis of silver halide low-dimensional nanomaterials in microemulsions, J. Mater. Chem., 13, pp. 163-165.
187. 3: LDH formation mechanism, Chem. Mater., 17, pp. 1055-1062.
188. Yamauchi, T., Tsukahara, Y., Yamada, K., Sakata, T., and Wada, Y. (2011). Nucleation and growth of magnetic Ni-Co (core-shell) nanoparticles in a one-pot reaction under microwave irradiation, Chem. Mater., 23, pp. 75-84.
189. Yang, Y., Matsubara, S., Xiong, L., Hayakawa, T., and Nogami, M. (2007). Solvothermal synthesis of multiple shapes of silver nanoparticles and their SERS properties, J. Phys. Chem. C, 111, pp. 9095-9104.
190. Yu, C. H., Oduro, W., Tam, K., and Edman, S. C. T. (2009). Metallic Nanoparticles, ed. John, B., Chapter 10 "Some Applications of Nanoparticles," (Elsevier, Oxford, UK) pp. 365-378.
191. 2 prepared by deposition-precipitation with NaOH and urea, J. Catal., 222, pp. 357-367.
192. Zhang, D., Yan, T., Li, H., and Shia, L. (2011). Ionic liquid-assisted synthesis and photoluminescence property of mesoporous EuF3 nanospheres, Micropor. Mesopor. Mater., 141, pp. 110-118.
193. Zhang, H. W., and Swihart, M. T. (2007). Synthesis of tellurium dioxide nanoparticles by spray pyrolysis, Chem. Mater., 19, pp. 1290-1301.
194. 4 visible-light photocatalyst, Adv. Mater., 19, pp. 2083-2086.
195. Zhang, Q., and Saito, F. (2000). Mechanochemical synthesis of lanthanum aluminate by grinding lanthanum oxide with transition alumina, J. Am. Ceram. Soc., 83, pp. 439-441.
196. Zhang, X., and Chan, K. Y. (2003). Water-in-oil microemulsion synthesis of platinum-ruthenium nanoparticles, their characterization and electrocatalytic properties, Chem. Mater., 15, pp. 451-459.
197. 3 catalyst via gel-coprecipitation of oxalate precursors for low-temperature steam reforming of methanol, Catal. Lett., 102, pp. 183-190.
198. Zheng, N., and Stucky, G. (2006). A general synthetic strategy for oxide-supported metal nanoparticle catalysts, J. Am. Chem. Soc., 128, pp. 14278-14280.
199. Zhu, H. T., Zhang, H., Liang, J. K., Rao, G. H., Li, J. B., Liu, G. Y., Du, Z. M., Fan, H. M., and Luo, J. (2011). Controlled synthesis of Te nanostructures from nanotubes to nanorods and nanowires and their template applications, J. Phys. Chem. C, 115, pp. 6375-6380.
200. Zhu, J., Shen, Y., Xie, A., Qiu, L., Zhang, Q., and Zhang, S. (2007). Photoinduced synthesis of anisotropic gold nanoparticles in roomtemperature ionic liquid, J. Phys. Chem. C, 111, pp. 7629-7633.
201. xSe nanoparticles, J. Phys. Chem. B, 104, pp. 7344-7347.