Dispersion of Nanocrystalline Fe3O4 within Composite Electrodes: Insights on Battery-Related Electrochemistry

ACS Applied Materials and Interfaces

Volumn 8, Issue 18, 2016, Pages 11418-11430

  Bock, David C ^a   Pelliccione, Christopher J ^a   Zhang, Wei ^a   Wang, Jiajun ^a   Knehr, K W ^d   Wang, Jun ^a   Wang, Feng ^a   West, Alan C ^d   Marschilok, Amy C ^b,c   Takeuchi, Kenneth J ^b,c   Takeuchi, Esther S ^a,b,c  

^a BROOKHAVEN NATIONAL LABORATORY   (United States)

^b STONY BROOK UNIVERSITY   (United States)

^c Stony Brook University   (United States)

^d NONE   (United States)

Author keywords

aggregate; composite; EIS; EXAFS; lithium ion battery; magnetite; TXM

Indexed keywords

AGGLOMERATION; AGGREGATES; CARBON; CARBON BLACK; CHARGE TRANSFER; COMPOSITE MATERIALS; CONTINUUM MECHANICS; ELECTRIC BATTERIES; ELECTROCHEMICAL ELECTRODES; ELECTROCHEMISTRY; ELECTRODES; LITHIUM ALLOYS; LITHIUM-ION BATTERIES; MAGNETITE; NANOCRYSTALLINE MATERIALS; NANOCRYSTALS; OLEIC ACID; SECONDARY BATTERIES; X RAY ABSORPTION SPECTROSCOPY;

CHARGE TRANSFER RESISTANCE; COMPOSITE ELECTRODE; ELECTROCHEMICAL BEHAVIORS; ELECTROCHEMICAL TESTING; EXAFS; FUNCTIONAL CAPACITY; HEAT TREATMENT PROCESS; SURFACE FILM FORMATIONS;

DISPERSIONS;

EID: 84974527535     PISSN: 19448244     EISSN: 19448252     Source Type: Journal    
DOI: 10.1021/acsami.6b01134     Document Type: Article

References (75)

1. Bock, D. C.; Marschilok, A. C.; Takeuchi, K. J.; Takeuchi, E. S. Batteries Used to Power Implantable Biomedical Devices Electrochim. Acta 2012, 84, 155-164 10.1016/j.electacta.2012.03.057
2. Soloveichik, G. L. Battery Technologies for Large-Scale Stationary Energy Storage. In Annual Review of Chemical and Biomolecular Engineering; Prausnitz, J. M., Ed.; Annual Reviews: Palo Alto, CA, 2011; Vol. 2, pp 503-527.
3. 4 as a Cathode Material J. Power Sources 2005, 146, 319-322 10.1016/j.jpowsour.2005.03.130
4. 3 for Rechargeable Batteries J. Electrochem. Soc. 2010, 157, A60-A65 10.1149/1.3254160
5. 3 (0 < x < 2) Mater. Res. Bull. 1982, 17, 785-793 10.1016/0025-5408(82)90029-0
6. 4 J. Appl. Phys. 1986, 59, 1918-1926 10.1063/1.336420
7. 4 J. Solid State Chem. 1988, 77, 180-189 10.1016/0022-4596(88)90106-5
8. 4 Following Lithium Deintercalation Chem. Mater. 2013, 25, 1664-1672 10.1021/cm400106k
9. 4/C Composites Ionics 2014, 20, 23-28 10.1007/s11581-013-0965-3
10. Wagemaker, M.; Mulder, F. M. Properties and Promises of Nanosized Insertion Materials for Li-Ion Batteries Acc. Chem. Res. 2013, 46, 1206-1215 10.1021/ar2001793
11. 3 J. Electrochem. Soc. 2003, 150, A133-A139 10.1149/1.1528941
12. Tarascon, J. M.; Poizot, P.; Laruelle, S.; Grugeon, S.; Dupont, L. Nano-Sized Transition-Metal Oxides as Negative-Electrode Materials for Lithium-Ion Batteries Nature 2000, 407, 496-499 10.1038/35035045
13. 4 Electrochem. Solid-State Lett. 2009, 12, A91-A94 10.1149/1.3078076
14. Zhu, S.; Marschilok, A. C.; Takeuchi, E. S.; Yee, G. T.; Wang, G.; Takeuchi, K. J. Nanocrystalline Magnetite: Synthetic Crystallite Size Control and Resulting Magnetic and Electrochemical Properties J. Electrochem. Soc. 2010, 157, A1158-A1163 10.1149/1.3478667
15. Menard, M. C.; Marschilok, A. C.; Takeuchi, K. J.; Takeuchi, E. S. Variation in the Iron Oxidation States of Magnetite Nanocrystals as a Function of Crystallite Size: The Impact on Electrochemical Capacity Electrochim. Acta 2013, 94, 320-326 10.1016/j.electacta.2013.02.012
16. Menard, M. C.; Takeuchi, K. J.; Marschilok, A. C.; Takeuchi, E. S. Electrochemical Discharge of Nanocrystalline Magnetite: Structure Analysis Using X-Ray Diffraction and X-Ray Absorption Spectroscopy Phys. Chem. Chem. Phys. 2013, 15, 18539-18548 10.1039/c3cp52870g
17. Jassby, D.; Wiesner, M. Characterization of ZnS Nanoparticle Aggregation Using Photoluminescence Langmuir 2011, 27, 902-908 10.1021/la103470r
18. Maillard, F.; Schreier, S.; Hanzlik, M.; Savinova, E. R.; Weinkauf, S.; Stimming, U. Influence of Particle Agglomeration on the Catalytic Activity of Carbon-Supported Pt Nanoparticles in Co Monolayer Oxidation Phys. Chem. Chem. Phys. 2005, 7, 385-393 10.1039/B411377B
19. 3/Ac Catalyst for Acetylene Hydrochlorination Sci. Rep. 2015, 5, 10553 10.1038/srep10553
20. Kharissova, O. V.; Kharisov, B. I.; Jimenez-Perez, V. M.; Muñoz Flores, B. M.; Ortiz Mendez, U. O. Ultrasmall Particles and Nanocomposites: State of the Art RSC Adv. 2013, 3, 22648-22682 10.1039/c3ra43418d
21. Knehr, K. W.; Brady, N. W.; Cama, C. A.; Bock, D. C.; Lin, Z.; Lininger, C. N.; Marschilok, A. C.; Takeuchi, K. J.; Takeuchi, E. S.; West, A. C. Modeling the Mesoscale Transport of Lithium-Magnetite Electrodes Using Insight from Discharge and Voltage Recovery Experiments J. Electrochem. Soc. 2015, 162, A2817-A2826 10.1149/2.0961514jes
22. Wang, J.; Karen Chen, Y.-c.; Yuan, Q.; Tkachuk, A.; Erdonmez, C.; Hornberger, B.; Feser, M. Automated Markerless Full Field Hard X-Ray Microscopic Tomography at Sub-50 nm 3-Dimension Spatial Resolution Appl. Phys. Lett. 2012, 100, 143107 10.1063/1.3701579
23. Holt, M.; Harder, R.; Winarski, R.; Rose, V. Nanoscale Hard X-Ray Microscopy Methods for Materials Studies Annu. Rev. Mater. Res. 2013, 43, 183-211 10.1146/annurev-matsci-071312-121654
24. Bertsch, P. M.; Hunter, D. B. Applications of Synchrotron-Based X-Ray Microprobes Chem. Rev. 2001, 101, 1809-1842 10.1021/cr990070s
25. de Groot, F. M. F.; de Smit, E.; van Schooneveld, M. M.; Aramburo, L. R.; Weckhuysen, B. M. In-Situ Scanning Transmission X-Ray Microscopy of Catalytic Solids and Related Nanomaterials ChemPhysChem 2010, 11, 951-962 10.1002/cphc.200901023
26. Bruck, A. M.; Cama, C. A.; Gannett, C. N.; Marschilok, A. C.; Takeuchi, E. S.; Takeuchi, K. J. Nanocrystalline Iron Oxide Based Electroactive Materials in Lithium Ion Batteries: The Critical Role of Crystallite Size, Morphology, and Electrode Heterostructure on Battery Relevant Electrochemistry Inorg. Chem. Front. 2016, 3, 26-40 10.1039/C5QI00247H
27. Fu, L.; Dravid, V. P.; Johnson, D. L. Self-Assembled (Sa) Bilayer Molecular Coating on Magnetic Nanoparticles Appl. Surf. Sci. 2001, 181, 173-178 10.1016/S0169-4332(01)00388-9
28. Sahoo, Y.; Pizem, H.; Fried, T.; Golodnitsky, D.; Burstein, L.; Sukenik, C. N.; Markovich, G. Alkyl Phosphonate/Phosphate Coating on Magnetite Nanoparticles: A Comparison with Fatty Acids Langmuir 2001, 17, 7907-7911 10.1021/la010703+
29. Patterson, A. L. The Scherrer Formula for X-Ray Particle-Size Determination Phys. Rev. 1939, 56, 978-982 10.1103/PhysRev.56.978
30. Knehr, K. W.; Brady, N. W.; Lininger, C. N.; Cama, C. A.; Bock, D. C.; Lin, Z.; Marschilok, A. C.; Takeuchi, K. J.; Takeuchi, E. S.; West, A. C. Mesoscale Transport in Magnetite Electrodes for Lithium-Ion Batteries ECS Trans. 2015, 69, 7-19 10.1149/06901.0007ecst
31. Newville, M. IFEFFIT: Interactive XAFS Analysis and FEFF Fitting J. Synchrotron Radiat. 2001, 8, 322-324 10.1107/S0909049500016964
32. Ravel, B.; Newville, M. Athena, Artemis, Hephaestus: Data Analysis for X-Ray Absorption Spectroscopy Using IFEFFIT J. Synchrotron Radiat. 2005, 12, 537-541 10.1107/S0909049505012719
33. Mustre de Leon, J.; Rehr, J. J.; Zabinsky, S. I.; Albers, R. C. Ab Initio Curved-Wave X-Ray-Absorption Fine Structure Phys. Rev. B: Condens. Matter Mater. Phys. 1991, 44, 4146-4156 10.1103/PhysRevB.44.4146
34. Rehr, J. J.; Mustre de Leon, J.; Zabinsky, S. I.; Albers, R. C. Theoretical X-Ray Absorption Fine Structure Standards J. Am. Chem. Soc. 1991, 113, 5135-5140 10.1021/ja00014a001
35. 4 Acta Crystallogr., Sect. B: Struct. Sci. 1997, 53, 762-766 10.1107/S0108768197007842
36. 3: Synchrotron X-Ray Powder Diffraction and High-Resolution Electron Microscopy Studies J. Appl. Crystallogr. 1995, 28, 141-145 10.1107/S0021889894010113
37. 4 ACS Appl. Mater. Interfaces 2015, 7, 13457-13466 10.1021/acsami.5b02478
38. Zhang, W.; Bock, D. C.; Pelliccione, C. J.; Li, Y.; Wu, L.; Zhu, Y.; Marschilok, A. C.; Takeuchi, E. S.; Takeuchi, K. J.; Wang, F. Insights into Ionic Transport and Structural Changes in Magnetite During Multiple-Electron Transfer Reactions. Adv. Energy Mater. 2016, DOI: 10.1002/aenm.201502471.
39. Lee, J. E.; Yu, S. H.; Lee, D. J.; Lee, D. C.; Han, S. I.; Sung, Y. E.; Hyeon, T. Facile and Economical Synthesis of Hierarchical Carbon-Coated Magnetite Nanocomposite Particles and Their Applications in Lithium Ion Battery Anodes Energy Environ. Sci. 2012, 5, 9528-9533 10.1039/c2ee22792d
40. 4@Carbon Nanocomposites for High-Performance Lithium-Ion Batteries ACS Appl. Mater. Interfaces 2015, 7, 9709-9715 10.1021/acsami.5b01503
41. 4 Nanoparticle Clusters as High-Performance Anodes for Lithium Ion Batteries Via Geometric Confinement Nano Lett. 2013, 13, 4249-4256 10.1021/nl401952h
42. Hameed, A. S.; Reddy, M. V.; Chowdari, B. V. R.; Vittal, J. J. Preparation of RGO-Wrapped Magnetite Nanocomposites and Their Energy Storage Properties RSC Adv. 2014, 4, 64142-64150 10.1039/C4RA11948G
43. Li, X.; Zhang, Z.; Li, J.; Ma, Y.; Qu, Y. Structural Influence of Porous FeOx@C Nanorods on Their Performance as Anodes of Lithium-Ion Batteries J. Mater. Chem. A 2015, 3, 18649-18656 10.1039/C5TA05234C
44. Liu, H.; Wang, G.; Wang, J.; Wexler, D. Magnetite/Carbon Core-Shell Nanorods as Anode Materials for Lithium-Ion Batteries Electrochem. Commun. 2008, 10, 1879-1882 10.1016/j.elecom.2008.09.036
45. 4 Nanoparticles as a High-Rate Lithium Ion Battery Anode Material ACS Nano 2013, 7, 4459-4469 10.1021/nn401059h
46. 4) Microspheres: The Highly Powerful Storage Versus Lithium as an Anode for Lithium Ion Batteries J. Phys. Chem. C 2012, 116, 6495-6502 10.1021/jp3002178
47. 4 Submicron Spheroids as Anode Materials for Lithium-Ion Batteries with Stable and High Electrochemical Performance J. Power Sources 2010, 195, 5379-5381 10.1016/j.jpowsour.2010.03.035
48. Macdonald, D. D. Reflections on the History of Electrochemical Impedance Spectroscopy Electrochim. Acta 2006, 51, 1376-1388 10.1016/j.electacta.2005.02.107
49. Randles, J. E. B. Kinetics of Rapid Electrode Reactions Discuss. Faraday Soc. 1947, 1, 11-19 10.1039/df9470100011
50. 3 Cathode Material Electrochim. Acta 2010, 55, 2384-2390 10.1016/j.electacta.2009.11.096
51. 4 Microspheres Encapsulated in Hollow Graphene Shells J. Mater. Chem. A 2015, 3, 11847-11856 10.1039/C5TA01848J
52. 3 with Various Particle Sizes J. Electrochem. Soc. 2003, 150, A1643-A1650 10.1149/1.1622959
53. Balasubramanian, M.; Sun, X.; Yang, X. Q.; McBreen, J. In Situ X-Ray Diffraction and X-Ray Absorption Studies of High-Rate Lithium-Ion Batteries J. Power Sources 2001, 92, 1-8 10.1016/S0378-7753(00)00493-6
54. Sharkov, M. D.; Boiko, M. E.; Bobyl, A. V.; Ershenko, E. M.; Terukov, E. I.; Zubavichus, Y. V. X-Ray Diffraction and EXAFS Analysis of Materials for Lithium-Based Rechargeable Batteries Crystallogr. Rep. 2013, 58, 993-997 10.1134/S1063774513070171
55. Pelliccione, C. J.; Ding, Y.; Timofeeva, E. V.; Segre, C. U. In Situ XAFS Study of the Capacity Fading Mechanisms in ZnO Anodes for Lithium-Ion Batteries J. Electrochem. Soc. 2015, 162, A1935-A1939 10.1149/2.1011509jes
56. 2/Graphite Battery Anode Nanomaterials Chem. Mater. 2015, 27, 574-580 10.1021/cm504101h
57. Zhang, W.; Duchesne, P.; Gong, Z. L.; Wu, S. Q.; Ma, L.; Jiang, Z.; Zhang, S.; Zhang, P.; Mi, J. X.; Yang, Y. In Situ Electrochemical XAFS Studies on an Iron Fluoride High-Capacity Cathode Material for Rechargeable Lithium Batteries J. Phys. Chem. C 2013, 117, 11498-11505 10.1021/jp401200u
58. Galoisy, L.; Calas, G.; Arrio, M. A. High-Resolution XANES Spectra of Iron in Minerals and Glasses: Structural Information from the Pre-Edge Region Chem. Geol. 2001, 174, 307-319 10.1016/S0009-2541(00)00322-3
59. Wilke, M.; Farges, F.; Petit, P.-E.; Brown, G. E., Jr; Martin, F. Oxidation State and Coordination of Fe in Minerals: An Fe K-XANES Spectroscopic Study Am. Mineral. 2001, 86, 714-730 10.2138/am-2001-5-612
60. Fleet, M. E. The Structure of Magnetite: Symmetry of Cubic Spinels J. Solid State Chem. 1986, 62, 75-82 10.1016/0022-4596(86)90218-5
61. Basinski, Z. S.; Hume-Rothery, W.; Sutton, A. L. The Lattice Expansion of Iron Proc. R. Soc. London, Ser. A 1955, 229, 459-467 10.1098/rspa.1955.0102
62. Beale, A. M.; Weckhuysen, B. M. EXAFS as a Tool to Interrogate the Size and Shape of Mono and Bimetallic Catalyst Nanoparticles Phys. Chem. Chem. Phys. 2010, 12, 5562-5574 10.1039/b925206a
63. Zhang, W. M.; Wu, X. L.; Hu, J. S.; Guo, Y. G.; Wan, L. J. Carbon Coated Fe3o4 Nanospindles as a Superior Anode Material for Lithium-Ion Batteries Adv. Funct. Mater. 2008, 18, 3941-3946 10.1002/adfm.200801386
64. Chae, B.-M.; Oh, E.-S.; Lee, Y.-K. Conversion Mechanisms of Cobalt Oxide Anode for Li-Ion Battery: In Situ X-Ray Absorption Fine Structure Studies J. Power Sources 2015, 274, 748-754 10.1016/j.jpowsour.2014.10.108
65. Poizot, P.; Laruelle, S.; Grugeon, S.; Dupont, L.; Tarascon, J. M. Searching for New Anode Materials for the Li-Ion Technology: Time to Deviate from the Usual Path J. Power Sources 2001, 97-98, 235-239 10.1016/S0378-7753(01)00508-0
66. Sina, M.; Thorpe, R.; Rangan, S.; Pereira, N.; Bartynski, R. A.; Amatucci, G. G.; Cosandey, F. Investigation of SEI Layer Formation in Conversion Iron Fluoride Cathodes by Combined STEM/EELS and XPS J. Phys. Chem. C 2015, 119, 9762-9773 10.1021/acs.jpcc.5b02058
67. 4 as a Case Example J. Power Sources 2012, 212, 233-246 10.1016/j.jpowsour.2012.04.005
68. Pinson, M. B.; Bazant, M. Z. Theory of SEI Formation in Rechargeable Batteries: Capacity Fade, Accelerated Aging and Lifetime Prediction J. Electrochem. Soc. 2013, 160, A243-A250 10.1149/2.044302jes
69. Gmitter, A. J.; Badway, F.; Rangan, S.; Bartynski, R. A.; Halajko, A.; Pereira, N.; Amatucci, G. G. Formation, Dynamics, and Implication of Solid Electrolyte Interphase in High Voltage Reversible Conversion Fluoride Nanocomposites J. Mater. Chem. 2010, 20, 4149-4161 10.1039/b923908a
70. 3 J. Mater. Chem. A 2015, 3, 14173-14177 10.1039/C5TA02499D
71. Grugeon, S.; Laruelle, S.; Dupont, L.; Tarascon, J. M. An Update on the Reactivity of Nanoparticles Co-Based Compounds Towards Li Solid State Sci. 2003, 5, 895-904 10.1016/S1293-2558(03)00114-6
72. 4 as Negative Electrodes for Rechargeable Lithium Batteries Phys. Chem. Chem. Phys. 2007, 9, 1837-1842 10.1039/B617519H
73. 4 in a Lithium Cell J. Electrochem. Soc. 2002, 149, A234-A241 10.1149/1.1435358
74. 4 Electrodes: Electrochemical Impedance Spectroscopy Study Nanoscale Res. Lett. 2008, 3, 390-394 10.1007/s11671-008-9176-7
75. Grugeon, S.; Laruelle, S.; Herrera-Urbina, R.; Dupont, L.; Poizot, P.; Tarascon, J. M. Particle Size Effects on the Electrochemical Performance of Copper Oxides toward Lithium J. Electrochem. Soc. 2001, 148, A285-A292 10.1149/1.1353566