Synthesis of 3,4,5-trimethoxybenzaldehyde

Synthetic Communications

Volumn 20, Issue 17, 1990, Pages 2659-2666

  Manchand, Percy S ^a   Belica, Peter S ^a   Wong, Harry S ^a  

^a HOFFMANN LA ROCHE INC   (United States)

Author keywords

[No Author keywords available]

Indexed keywords

EID: 84972990130     PISSN: 00397911     EISSN: 15322432     Source Type: Journal    
DOI: 10.1080/00397919008051474     Document Type: Article

References (9)

1. Roth, H. J. and Kleemann, A. “Pharmaceutical Chemistry” Vol. 1, Ellis Horwood, Chickester (U.K.), 1988, 286.
2. Peters, J. A. and vanBekkum, H., Reel. Trav. Chim. Pays-Bas 1981, 100. 21, and references cited therein.
3. Schwartz, A., J, Org. Chem. 1982, 47, 2213.
4. Subsequent to our patent [U.S. 4,218,567, August 19, 1980; filed May 30, 1978], which described, inter alia, the preparation of syringaldehyde from 5-bromovanillin, D. V. Rao and F. A. Stuber published (Synthesis. 1983, 308) a similar preparation using copper[11] chloride.
5. Bacon, R.G.R. and Rennison, S. C., J. Chem, Soc. (C) 1969. 312.
6. Organic Synth., Coll. Vol. 1. 1941, 163. Material prepared by this method was dried in vacuo and stored under argon.
7. Shriner, R. L. and McCutchan, P., J. Amer, Chem. Soc. 1929, 51, 2193.
8. Pearl, I. J. Amer. Chem. Soc. 1948, 70, 1746.
9. Slotta, K. H. and Heller, H., Ber. Dtsch. Chem. Ges. 1930, 63, 3042.