Preparations: Sections 11.11 - 11.20

Handbook of Fluorous Chemistry

Volumn , Issue , 2005, Pages 382-407

  Ishihara, Kazuaki ^a   Yamamoto, Hisashi ^b  

^a NAGOYA UNIVERSITY   (Japan)

^b UNIVERSITY OF CHICAGO   (United States)

Author keywords

Fluorous chemistry; Preparations

Indexed keywords

FLUOROUS; PREPARATIONS;

EID: 84958606577     PISSN: None     EISSN: None     Source Type: Book    
DOI: 10.1002/3527603905.ch11b     Document Type: Chapter

References (9)

1. B. Hungerhoff, H. Sonnenschein, F. Theil, J. Org. Chem. 2002, 67, 1781-1785.
2. The pH of 6 should be tested on wet pH paper after waiting for 5 min. If necessary, traces of acid that decrease enzyme activity are to removed on a large scale by simple silica gel filtration [see synthesis of 2,2,2-trifluoroethyl 2H,2H,3H,3Hperfluoroundecanoate (11.19)].
3. Before its use in esterification, the salt 4a has to be dried under reduced pressure over P2O5.
4. U. T. Bornscheuer, R. J. Kazlauskas, Hydrolases in Organic Synthesis, Wiley- VCH, Weinheim, 1999, 44-47.
5. J. S. Wallace, K. B. Reda, M. E. Williams, C. J. Morrow, J. Org. Chem. 1990, 55, 3544-3546.
6. L. J. Whalen, C. J. Morrow, Tetrahedron: Asymmetry 2000, 11, 1279-1298.
7. M. Bänzinger, G. J. Griffiths, J. F. McGarrity, Tetrahedron: Asymmetry 1993, 4, 723-726.
8. J. Roos, U. Stelzer, F. Effenberger, Tetrahedron: Asymmetry 1998, 9, 1043- 1049.
9. A. Córdova, M. R. Tremblay, B. Clapham, K. D. Janda, J. Org. Chem. 2001, 66, 5645-5648.