Desirability functions as response in a d-optimal design for evaluating the extraction and purification steps of six tranquillizers and an anti-adrenergic by liquid chromatography-tandem mass spectrometry

Journal of Chemometrics

Volumn 30, Issue 2, 2016, Pages 58-69

  Rubio, Laura ^a   Oca, María Leticia ^a   Sarabia, Luis ^a   García, Inmaculada ^b   Ortiz, María Cruz ^a  

^a UNIVERSITY OF BURGOS   (Spain)

^b Servicio de Programas de Salud y Prevención de la Dirección Técnica de Recursos Humanos y Gestión de Centros Gerencia de Servicios Sociales   (Spain)

Author keywords

D optimal design; Desirability function; Internal standardization; Liquid chromatography tandem mass spectrometry; Tranquillizers

Indexed keywords

EXTRACTION; OPTIMAL SYSTEMS; PURIFICATION; STANDARDIZATION;

ANALYTES; D-OPTIMAL DESIGNS; DESIRABILITY FUNCTION; EXTRACTION AND PURIFICATIONS; INTERNAL STANDARDIZATION; INTERNAL STANDARDS; LIQUID CHROMATOGRAPHY-TANDEM MASS SPECTROMETRY; LIQUID CHROMATOGRAPHY/TANDEM MASS SPECTROMETRY; PEAKS AREAS; TRANQUILIZER;

MASS SPECTROMETRY;

EID: 84956931938     PISSN: 08869383     EISSN: 1099128X     Source Type: Journal    
DOI: 10.1002/cem.2767     Document Type: Article

References (42)

1. Delahaut P, Levaux C, Eloy P, Dubois M. Validation of a method for detecting and quantifying tranquillisers and a β-blocker in pig tissues by liquid chromatography-tandem mass spectrometry. Anal. Chim. Acta 2003; 483: 335-340.
2. Botsoglou NA, Fletouris DJ. Drug Residues in Foods: Pharmacology, Food Safety and Analysis, Marcel Dekker Inc.: New York, USA, 2001.
3. Turnipseed SB. Drug residues in meat: emerging issues. In Meat Science and Applications, (eds.). Marcel Dekker, Inc.: New York, 2001.
4. Commission Regulation (EU) No 37/2010 of 22 December 2009 on pharmacologically active substances and their classification regarding maximum residue limits in foodstuffs of animal origin. Off. J. Eur. Union, L 2010; 15: 1-72.
5. Regulation (EC) No 470/2009 of the European Parliament and of the Council of 6 May 2009 laying down Community procedures for the establishment of residue limits of pharmacologically active substances in foodstuffs of animal origin. Off. J. Eur. Union, L 2009; 152: 11-22.
6. Rattenberger E, Matzke P, Neudegger J. Development of a radioimmunoassay for the detection of residues of the beta adrenoreceptor blocking agent "carazolol" in blood and urine of pigs. J. Arch. Lebensmittelhyg 1985; 36: 85-87.
7. Meenagh SA, McEvoy JDG, Elliott CT. Determination of carazolol residues in porcine tissue by radioreceptor assay. Anal. Chim. Acta 2002; 462: 149-156.
8. Cooper J, Delahaut P, Fodey TL, Elliott CT. Development of a rapid screening test for veterinary sedatives and the beta-blocker carazolol in porcine kidney by ELISA. Analyst 2004; 129: 169-174.
9. Haagsma N, Bathelt ER, Engelsma JW. Thin-layer chromatographic screening method for the tranquillizers azaperone, propiopromazine and carazolol in pig tissues. J. Chromatogr. 1988; 436: 73-79.
10. Van Ginkel LA, Schwillens PLWJ, Olling M. Liquid chromatographic method with on-line UV spectrum identification and off-line thin-layer chromatographic confirmation for the detection of tranquillizers and carazolol in pig kidneys. Anal. Chim. Acta 1989; 225: 137-146.
11. Keukens HJ, Aerts MML. Determination of residues of carazolol and a number of tranquillizers in swine kidney by high-performance liquid chromatography with ultraviolet and fluorescence detection. J. Chromatogr. A 1991; 464: 149-161.
12. Aoki Y, Hakamata H, Igarashi Y, Uchida K, Kobayashi H, Hirayama N, Kotani A, Kusu F. Simultaneous determination of azaperone and azaperol in animal tissues by HPLC with confirmation by electrospray ionization mass spectrometry. J. Chromatogr. B 2009; 877: 166-172.
13. Cerkvenik-Flajs V. Determination of residues of azaperone in the kidneys by liquid chromatography with fluorescence detection. Anal. Chim. Acta 2007; 586: 374-382.
14. Kadir F, Zuidema J. High-performance liquid chromatographic method for the determination of carazolol in serum or plasma of pigs. J. Chromatogr. 1990; 527: 461-466.
15. Rose MD, Shearer G. Determination of tranquilisers and carazolol residues in animal tissue using high-performance liquid chromatography with electrochemical detection. J. Chromatogr. A 1992; 624: 471-477.
16. Commission Decision 2002/657/EC of 12 August 2002 implementing Council Directive 96/23/EC concerning the performance of analytical methods and the interpretation of results. Off. J. Eur. Commun. 2002; L 221: 8-36.
17. Olmos-Carmona ML, Hernández-Carrasquilla M. Gas chromatographic-mass spectrometric analysis of veterinary tranquillizers in urine: evaluation of method performance. J. Chromatogr. B 1999; 734: 113-120.
18. Govaert Y, Batjoens P, Tsilikas K, Degroodt JM, Srebrnik S. Multi-residue analysis of tranquillizers in meat: confirmatory assays using mass spectrometry. Analyst 1998; 123: 2507-2512.
19. Spyridaki MH, Lyris E, Georgoulakis I, Kouretas D, Konstantinidou M, Georgakopoulos CG. Determination of xylazine and its metabolites by GC-MS in equine urine for doping analysis. J. Pharm. Biomed. Anal. 2004; 35: 107-116.
20. Zhang J, Shao B, Yin J, Wu Y, Duan H. Simultaneous detection of residues of β-adrenergic receptor blockers and sedatives in animal tissues by high-performance liquid chromatography/tandem mass spectrometry. J. Chromatogr. B 2009; 877: 1915-1922.
21. Mitrowska K, Posyniak A, Zmudzki J. Rapid method for the determination of tranquilizers and a beta-blocker in porcine and bovine kidney by liquid chromatography with tandem mass spectrometry. Anal. Chim. Acta 2009; 637: 185-192.
22. Bock C, Stachel CS. Development and validation of a confirmatory method for the determination of tranquilisers and a β-blocker in porcine and bovine kidney by LC-MS/MS. Food Addit. Contam., Part A 2013; 30: 1000-1011.
23. Council Directive 96/23/EC of 29 April 1996 on measures to monitor certain substances and residues thereof in live animals and animal products. Off. J. Eur. Commun., L 1996; 125: 10-32.
24. Alan Xu Q, Madden TL (Eds.). LC-MS in Drug Bioanalysis, Springer Science & Business Media: New York, USA, 2012.
25. Tan A, Awaiye K. Use of internal standards in LC-MS bioanalysis. In Handbook of LC-MS Bioanalysis: Best Practices, Experimental Protocols, and Regulations, (eds.). John Wiley & Sons Inc.: Hoboken, USA, 2013; 217-227.
26. Bronsema KJ, Bischoff R, van de Merbel NC. Internal standards in the quantitative determination of protein biopharmaceuticals using liquid chromatography coupled to mass spectrometry. J. Chromatogr. B 2012; 893-894: 1-14.
27. Jalali-Heravi M, Parastar H, Ebrahimi-Najafabadi H. Characterization of volatile components of Iranian saffron using factorial-based response surface modeling of ultrasonic extraction combined with gas chromatography-mass spectrometry analysis. J. Chromatogr. A 2009; 1216: 6088-6097.
28. Sereshti H, Heidari R, Sadami S. Determination of volatile components of saffron by optimized ultrasound-assisted extraction in tandem with dispersive liquid-liquid microextraction followed by gas chromatography-mass spectrometry. Food Chem. 2014; 143: 499-505.
29. Pieraccini G, Furlanetto S, Orlandini S, Bartolucci G, Giannini I, Pinzauti S, Moneti G. Identification and determination of mainstream and sidestream smoke components in different brands and types of cigarettes by means of solid-phase microextraction-gas chromatography-mass spectrometry. J. Chromatogr. A 2008; 1180: 138-150.
30. Cortada C, Vidal L, Canals A. Determination of nitroaromatic explosives in water samples by direct ultrasound-assisted dispersive liquid-liquid microextraction followed by gas chromatography-mass spectrometry. Talanta 2011; 85: 2546-2552.
31. Beser MI, Beltrán J, Yusà V. Design of experiment approach for the optimization of polybrominated diphenyl ethers determination in fine airborne particulate matter by microwave-assisted extraction and gas chromatography coupled to tandem mass spectrometry. J. Chromatogr. A 2014; 1323: 1-10.
32. Gionfriddo E, Naccarato A, Sindona G, Tagarelli A. Determination of hydrazine in drinking water: development and multivariate optimization of a rapid and simple solid phase microextraction-gas chromatography-triple quadrupole mass spectrometry protocol. Anal. Chim. Acta 2014; 835: 37-45.
33. Feng D, Liu L, Zhao L, Zhou Q, Tan T. Determination of volatile nitrosamines in latex products by HS-SPME-GC-MS. Chromatographia 2011; 74: 817-825.
34. Cortada C, Vidal L, Tejada S, Romo A, Canals A. Determination of organochlorine pesticides in complex matrices by single-drop microextraction coupled to gas chromatography-mass spectrometry. Anal. Chim. Acta 2009; 638: 29-35.
35. Pérez Antón A, Casas Ferreira AM, García Pinto C, Moreno Cordero B, Pérez Pavón JL. Headspace generation coupled to gas chromatography-mass spectrometry for the automated determination and quantification of endogenous compounds in urine. Aldehydes as possible markers of oxidative stress. J. Chromatogr. A 2014; 1367: 9-15.
36. Lespes G, Desauziers V, Montigny C, Potin-Gautier M. Optimization of solid-phase microextraction for the speciation of butyl- and phenyltins using experimental designs. J. Chromatogr. A 1998; 826: 67-76.
37. Melo A, Aguiar A, Mansilha C, Pinho O, Ferreira IMPLVO. Optimisation of a solid-phase microextraction/HPLC/diode array method for multiple pesticide screening in lettuce. Food Chem. 2012; 130: 1090-1097.
38. Derringer G, Suich R. Simultaneous optimization of several response variables. J. Qual. Technol. 1980; 12: 214-219.
39. Sarabia LA, Ortiz MC. Response surface methodology. In Comprehensive Chemometrics: Chemical and Biochemical Data Analysis, (eds.). Elsevier: Amsterdam, Holland, 2009; 378-382.
40. Lewis GA, Mathieu D, Phan-Tan-Luu R. Pharmaceutical Experimental Design, Marcel Decker Inc.: New York, USA, 1999.
41. Mathieu D, Nony J, Phan-Tan-Luu R. NemrodW (Versión 2007_03), L.P.R.A.I.: Marseille, France, 2007.
42. Draper NR, Smit H. Applied Regression Analysis, (third edn). John Wiley & Sons Inc. New York: USA, 1998; 210-214.