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The resin used was purchased from Sigma (p-Alkoxybenzyl Alcohol Resin 0. 69 mmol per g resin, Cat. # A3039) 9. 3'-Th = 3'-Thiophene adduct, 2'-Th = 2'-Thiophene adduct and 3'Fu = 3'-furan adduct
-
The resin used was purchased from Sigma (p-Alkoxybenzyl Alcohol Resin 0. 69 mmol per g resin, Cat. # A3039) 9. 3'-Th = 3'-Thiophene adduct, 2'-Th = 2'-Thiophene adduct and 3'Fu = 3'-furan adduct.
-
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40
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85066088130
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All reactions were monitored by ir and gel-phase 13c nmr. Gel-phase 13c nmr spectra were obtained in cd2ci2
-
All reactions were monitored by IR and gel-phase 13C NMR. Gel-phase 13c NMR spectra were obtained in CD2CI2.
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85066075036
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So far, we have made no attempts to optimise this reaction, although we are aware of the fact that this yield is hardly applicable for solid phase synthesis
-
So far, we have made no attempts to optimise this reaction, although we are aware of the fact that this yield is hardly applicable for solid phase synthesis.
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44
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85066091466
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Attemps to influence the endo/exo ratio in the preparation of compounds 22 and 23 in solution using excess enolate in the condensation reaction failed
-
Attemps to influence the endo/exo ratio in the preparation of compounds 22 and 23 in solution using excess enolate in the condensation reaction failed.
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