Purity assessment of organic calibration standards using a combination of quantitative NMR and mass balance

Analytical and Bioanalytical Chemistry

Volumn 407, Issue 11, 2015, Pages 3103-3113

  Davies, Stephen R ^a   Jones, Kai ^a   Goldys, Anna ^a   Alamgir, Mahuiddin ^a   Chan, Benjamin K H ^a   Elgindy, Cecile ^a   Mitchell, Peter S R ^a   Tarrant, Gregory J ^a   Krishnaswami, Maya R ^a   Luo, Yawen ^a   Moawad, Michael ^a   Lawes, Douglas ^b   Hook, James M ^b  

^a NATIONAL MEASUREMENT INSTITUTE   (Australia)

^b UNIVERSITY OF NEW SOUTH WALES   (Australia)

Author keywords

Calibration standards; Mass fraction; Purity assessment; Quantitative NMR

Indexed keywords

COST EFFECTIVENESS; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY; STANDARDS;

CALIBRATION STANDARD; COST EFFECTIVE; FIT FOR PURPOSE; MASS FRACTION; MULTIPLE-PEAK; ORGANIC CALIBRATION; PURITY ASSESSMENT; STRUCTURAL COMPLEXITY;

CALIBRATION;

CALIBRATION; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY; PROCEDURES; STANDARD; STANDARDS; THEORETICAL MODEL;

CALIBRATION; MAGNETIC RESONANCE SPECTROSCOPY; MODELS, THEORETICAL; REFERENCE STANDARDS;

EID: 84940451308     PISSN: 16182642     EISSN: 16182650     Source Type: Journal    
DOI: 10.1007/s00216-014-7893-6     Document Type: Article

References (56)

1. King B, Westwood S (2001) Fresenius J Anal Chem 370:194-199
2. Duewer DL, Parris RM, White E, May WE, Elbaum H. (2004) An approach to the metrologically sound traceable assessment of the chemical purity of organic reference materials, NIST Special Publication 1012
3. Le Goff T, Wood S (2009) Anal Bioanal Chem 394:2183-2192
4. Westwood S, Daireaux A, Josephs RD, Weilgosz R (2012) Metrologia 49(1A):08014
5. Westwood S, Choteau T, Josephs RD, Daireaux A, Weilgosz RI (2013) Anal Chem 85:3118-3126, references cited therein
6. Maniara G, Rajamoorthi K, Rajanand S, Stockton GW (1998) Anal Chem 70:4921-4928
7. Saito T, Nakaie S, Kinoshita M, Ihara T, Kinugasa S, Nomura A, Maeda T (2004) Metrologia 41:213-218
8. Griffiths L, Irving AM (1998) Analyst 123:1061-1068
9. Wells RJ, Hook JM, Al-Deen TS, Hibbert DB (2002) J Agric Food Chem 50:3366-3374
10. Al Deen TS, Hibbert DB, Hook JM, Wells RJ (2002) Anal Chim Acta 474:125-135
11. Al Deen TS, Hibbert DB, Hook JM, Wells RJ (2004) Accred Qual Assur 9:55-63
12. Wells RJ, Cheung J, Hook JM (2004) Accred Qual Assur 9:450-456
13. Burton IW, Quilliam MA, Walter JA (2005) Anal Chem 77:3123-3131
14. Valverde J, This H (2008) J Agric Food Chem 56:314-320
15. Saito T, Ihara T, Miuraa T, Yamada Y, Chiba K (2011) Accred Qual Assur 16(8-9):421-428
16. Pierens GK, Carroll AR, Davis RA, Palframan ME, Quinn RJ (2008) J Nat Prod 71:810-813
17. Wells RJ, Cheung J, Hook JM (2008) In: Holzgrabe U (ed) NMR spectroscopy in pharmaceutical analysis, Elsevier, Amsterdam, pp 291-314
18. Pauli GF, Gödecke T, Jaki BU, Lankin DC (2012) J Nat Prod 75(4):834-851
19. Holzgrabe U, Deubner R, Schollmayer C, Waibel B (2005) J Pharm Biomed Anal 38(5):806-812
20. Wishart DS (2008) Trends Anal Chem 27(3):228-237
21. Wu Y, He Y, Zhang Y, Lu J, Dai Z, Ma S, Lin R (2014) J Pharm Biomed Anal 90:92-97
22. Borioni A, Gostoli G, Bossu E, Sestilli I (2014) J Pharm Biomed Anal 94:19-22
23. Weber M, Hellriegel C, Ruck A, Sauermoser R, Wuthrich J (2013) J Accred Qual Assur 18:91-98
24. Tatsis EC, Exarchou V, Troganis AN, Gerothanassis IP (2008) Anal Chim Acta 607:219-226
25. Ahvazi BC, Crestini C, Argyropoulos DS (1999) J Agric Food Chem 47:190-201
26. Spyros AD (2000) J Agric Food Chem 48:802-805
27. Rana FR, Mautone AJ, Dluhy RA (1993) Appl Spectrosc 47:1015-1023
28. Nouri-Sorkhabi MH, Wright LC, Sullivan DR, Kuchel PW (1996) Lipids 31:765-770
29. Henderson TJ (2002) Anal Chem 74(1):191-198
30. Lonnon DG, Hook JM (2003) Anal Chem 75(17):4659-4666
31. Giraudeau P, Tea I, Remaud GS, Akoka S (2013) J Pharm and Biomed Anal. doi: 10.1016/j.jpba.2013.07.020
32. Al-Deen TS (2002) Validation of quantitative nuclear magnetic resonance (qNMR) spectroscopy as a primary ratio analytical method for assessing the purity of organic compounds: a metrological approach. Ph.D. Thesis, University of NSW
33. Malz F, Jancke H (2005) J Pharm and Biomed Anal 38(5):813-823
34. Liu S-Y, Hu C-Q (2007) Anal Chim Acta 602:114-121
35. Rundlof T, Mathiasson M, Bekiroglu S, Hakkarainen B, Bowden T, Arvidsson T (2010) J Pharm and Biomed Anal 52:645-651
36. Nogueira R, Garrido BC, Borges RM, Silva GEB, Queiroz SM, Cunha VS (2013) Eur J Pharm Sci 48:502-513
37. Rundlof T, McEwen I, Johansson M, Arvidsson T (2013) J Pharm and Biomed Anal. doi: 10.1016/j.jpba.2013.09.010
38. Huang Y, Su B-N, Ye Q, Palaniswamy VA, Bolgar MS, Raglione TV (2014) J Pharm and Biomed Anal 88:1-6
39. Quan C (2014) Food Chem 153:378-386
40. Derome AE (1989) Modern NMR techniques for chemistry research. Pergamon, Elmsford
41. ISO (2009) ISO guide 34: 2009 general requirements for the competence of reference material producers, clause 3.5. International Organisation for Standardisation (ISO), Geneva
42. Rabenstein DL, Keire DA (1991) Practical Spectrosc 11:323-369
43. Malz F, Jancke H (2006) Anal Bioanal Chem 385:760-765
44. Hill HH, McMinn DG (1992) In: Detectors for capillary chromatography. Wiley, New York (121:7-20 and references cited therein)
45. Perkins G, Laramy RE, Lively LD (1963) Anal Chem 35(3):360-362
46. Edwards RWH (1978) J Chromatogr 153:1-6
47. Tong HY, Karasek FW (1984) Anal Chem 56:2124-2128
48. Jorgensen AD, Picel KC, Stamoudis VC (1990) Anal Chem 62:683-689
49. Yieru H, Quinyu O, Weile Y (1990) Anal Chem 62:2063-2064
50. ISO (2006) ISO guide 35: 2006(E) reference materials - general and statistical principles for certification, section 7, 15-19. International Organisation for Standardisation (ISO), Geneva
51. Coplen TB (1996) IUPAC Pure and Appl Chem 68:2339-2359
52. ISO (1995) ISO guide to the expression of uncertainty in measurement. International Organisation for Standardisation, Geneva, 1993 (corrected and re-printed, 1995). ISBN 92-67-10188-9, 1995
53. Bentley RE (2004) In: Uncertainty in measurement: the ISO guide. Monograph 1: NMI technology transfer series, Eighth edition, p 38. ISBN 0-9750744-0-7. National Measurement Laboratory, Lindfield
54. Hibbert DB, Gooding JJ (2006) In: Data analysis for chemistry: an introductory guide for students and laboratory chemists. University press, Oxford
55. Kestens V, Zeleny R, Auclair G, Held A, Roebben G, Linsinger TPJ (2011) Thermochim Acta 524:1-6
56. Saito T, Ihara T, Koike M, Kinugasa S, Fujimine Y, Nose K, Hirai T (2009) Accred Qual Assur 14:79-86