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Volumn 28, Issue 2, 2015, Pages 195-205

Development and performance of a 129-GHz dynamic nuclear polarizer in an ultra-wide bore superconducting magnet

Author keywords

Electron spin resonance; Free radicals; Hyperpolarization; Nuclear magnetic resonance

Indexed keywords

CARBON NUCLEAR MAGNETIC RESONANCE; COMPUTER AIDED DESIGN; DEVICE FAILURE ANALYSIS; DEVICES; ELECTRIC CONDUCTIVITY; EQUIPMENT DESIGN; MAGNET; MICROWAVE RADIATION; REFRACTOMETRY; REPRODUCIBILITY; SENSITIVITY AND SPECIFICITY;

EID: 84939888234     PISSN: 09685243     EISSN: None     Source Type: Journal    
DOI: 10.1007/s10334-014-0455-2     Document Type: Article
Times cited : (23)

References (37)
  • 2
    • 36149016620 scopus 로고
    • Polarization of nuclei in metals
    • COI: 1:CAS:528:DyaG2cXpvFSr
    • Overhauser AW (1953) Polarization of nuclei in metals. Phys Rev 92:411–415
    • (1953) Phys Rev , vol.92 , pp. 411-415
    • Overhauser, A.W.1
  • 3
    • 0001395845 scopus 로고
    • Experimental verification of the overhauser nuclear polarization effect
    • COI: 1:CAS:528:DyaG28Xns1Giuw%3D%3D
    • Carver TR, Slichter CP (1956) Experimental verification of the overhauser nuclear polarization effect. Phys Rev 102:975–981
    • (1956) Phys Rev , vol.102 , pp. 975-981
    • Carver, T.R.1    Slichter, C.P.2
  • 4
    • 0000633163 scopus 로고
    • Principles of dynamic nuclear polarization
    • COI: 1:CAS:528:DyaE1cXkvFOhsrk%3D
    • Abragam A, Goldman M (1978) Principles of dynamic nuclear polarization. Rep Prog Phys 41:395–467
    • (1978) Rep Prog Phys , vol.41 , pp. 395-467
    • Abragam, A.1    Goldman, M.2
  • 5
    • 0031474636 scopus 로고    scopus 로고
    • Solid polarized targets for nuclear and particle physics experiments
    • COI: 1:CAS:528:DyaK1cXhtVOjsLk%3D
    • Crabb DG, Meyer W (1997) Solid polarized targets for nuclear and particle physics experiments. Annu Rev Nucl Part Sci 47:67–109
    • (1997) Annu Rev Nucl Part Sci , vol.47 , pp. 67-109
    • Crabb, D.G.1    Meyer, W.2
  • 8
    • 70349753054 scopus 로고    scopus 로고
    • Biomedical applications of hyperpolarized 13C magnetic resonance imaging
    • COI: 1:CAS:528:DC%2BD1MXht1WmsrvK
    • Gallagher FA, Kettunen MI, Brindle KM (2009) Biomedical applications of hyperpolarized 13C magnetic resonance imaging. Prog Nucl Magn Reson Spectrosc 55:285–295
    • (2009) Prog Nucl Magn Reson Spectrosc , vol.55 , pp. 285-295
    • Gallagher, F.A.1    Kettunen, M.I.2    Brindle, K.M.3
  • 11
    • 62149110807 scopus 로고    scopus 로고
    • Dynamic nuclear polarization of [1-13C]pyruvic acid at 4.6 tesla
    • COI: 1:CAS:528:DC%2BD1MXjs1amtro%3D, PID: 19162518
    • Johannesson H, Macholl S, Ardenkjaer-Larsen JH (2009) Dynamic nuclear polarization of [1-13C]pyruvic acid at 4.6 tesla. J Magn Reson 197:167–175
    • (2009) J Magn Reson , vol.197 , pp. 167-175
    • Johannesson, H.1    Macholl, S.2    Ardenkjaer-Larsen, J.H.3
  • 12
    • 33750187238 scopus 로고    scopus 로고
    • Electron spin resonance and its implication on the maximum nuclear polarization of deuterated solid target materials
    • Heckmann J, Meyer W, Radtke E, Reicherz G, Goertz S (2006) Electron spin resonance and its implication on the maximum nuclear polarization of deuterated solid target materials. Phys Rev B 74:134418
    • (2006) Phys Rev B , vol.74 , pp. 134418
    • Heckmann, J.1    Meyer, W.2    Radtke, E.3    Reicherz, G.4    Goertz, S.5
  • 13
    • 84876901425 scopus 로고    scopus 로고
    • Influence of deuteration in the glassing matrix on 13C dynamic nuclear polarization
    • COI: 1:CAS:528:DC%2BC3sXmsVartLo%3D, PID: 23552448
    • Lumata L, Merritt ME, Kovacs Z (2013) Influence of deuteration in the glassing matrix on 13C dynamic nuclear polarization. Phys Chem Chem Phys 15:7032–7035
    • (2013) Phys Chem Chem Phys , vol.15 , pp. 7032-7035
    • Lumata, L.1    Merritt, M.E.2    Kovacs, Z.3
  • 18
    • 84864333382 scopus 로고    scopus 로고
    • A super-wide bore DNP system for multiple sample preparation: cryogenic performance and polarization at low temperature
    • Crémillieux Y, Goutailler F, Montcel B, Grand D, Vermeulen G, Wolf PE (2012) A super-wide bore DNP system for multiple sample preparation: cryogenic performance and polarization at low temperature. Appl Magn Reson 43:167–180
    • (2012) Appl Magn Reson , vol.43 , pp. 167-180
    • Crémillieux, Y.1    Goutailler, F.2    Montcel, B.3    Grand, D.4    Vermeulen, G.5    Wolf, P.E.6
  • 20
    • 80052861949 scopus 로고    scopus 로고
    • BDPA: an efficient polarizing agent for fast dissolution dynamic nuclear polarization NMR spectroscopy
    • COI: 1:CAS:528:DC%2BC3MXhtVOnu7nM, PID: 21919088
    • Lumata L, Ratnakar SJ, Jindal A, Merritt M, Malloy C, Sherry AD, Kovacs Z (2011) BDPA: an efficient polarizing agent for fast dissolution dynamic nuclear polarization NMR spectroscopy. Chem Eur J 17:10825–10827
    • (2011) Chem Eur J , vol.17 , pp. 10825-10827
    • Lumata, L.1    Ratnakar, S.J.2    Jindal, A.3    Merritt, M.4    Malloy, C.5    Sherry, A.D.6    Kovacs, Z.7
  • 22
  • 23
    • 84985803980 scopus 로고
    • Low-temperature NMR techniques
    • COI: 1:CAS:528:DyaK2cXhsFWlurc%3D
    • Conradi MS (1993) Low-temperature NMR techniques. Concepts Magn Reson 5:243–262
    • (1993) Concepts Magn Reson , vol.5 , pp. 243-262
    • Conradi, M.S.1
  • 24
    • 0034184074 scopus 로고    scopus 로고
    • Remote tuning of NMR probe circuits
    • COI: 1:CAS:528:DC%2BD3cXislaqtLY%3D, PID: 10783273
    • Kodibagkar V, Conradi MS (2000) Remote tuning of NMR probe circuits. J Magn Reson 144:53–57
    • (2000) J Magn Reson , vol.144 , pp. 53-57
    • Kodibagkar, V.1    Conradi, M.S.2
  • 25
    • 84939912512 scopus 로고    scopus 로고
    • Thomas Jefferson National Lab, Userweb Helium vapor pressure vs temperature
    • Thomas Jefferson National Lab, Userweb Helium vapor pressure vs temperature. https://userweb.jlab.org/~ckeith/TOOLS/HeVaporTable.html
  • 26
    • 84866743552 scopus 로고    scopus 로고
    • High field dynamic nuclear polarization at 6.7 T: carbon-13 polarization above 70 % within 20 min
    • COI: 1:CAS:528:DC%2BC38XhsVamsLfP
    • Jannin S, Bornet A, Melzi R, Bodenhausen G (2012) High field dynamic nuclear polarization at 6.7 T: carbon-13 polarization above 70 % within 20 min. Chem Phys Lett 549:99–102
    • (2012) Chem Phys Lett , vol.549 , pp. 99-102
    • Jannin, S.1    Bornet, A.2    Melzi, R.3    Bodenhausen, G.4
  • 27
    • 84861745664 scopus 로고    scopus 로고
    • Impact of Gd3+ on DNP of [1-13C]pyruvate doped with trityl OX063, BDPA, or 4-oxo-TEMPO
    • COI: 1:CAS:528:DC%2BC38XmslGqsLk%3D, PID: 22571288
    • Lumata L, Merritt ME, Malloy CR, Sherry AD, Kovacs Z (2012) Impact of Gd3+ on DNP of [1-13C]pyruvate doped with trityl OX063, BDPA, or 4-oxo-TEMPO. J Phys Chem A 116:5129–5138
    • (2012) J Phys Chem A , vol.116 , pp. 5129-5138
    • Lumata, L.1    Merritt, M.E.2    Malloy, C.R.3    Sherry, A.D.4    Kovacs, Z.5
  • 28
    • 84864358474 scopus 로고    scopus 로고
    • Fast dissolution dynamic nuclear polarization NMR of 13C-enriched 89Y-DOTA complex: experimental and theoretical considerations
    • COI: 1:CAS:528:DC%2BC38XhtVagurrO
    • Lumata L, Merritt ME, Malloy C, Sherry AD, Kovacs Z (2012) Fast dissolution dynamic nuclear polarization NMR of 13C-enriched 89Y-DOTA complex: experimental and theoretical considerations. Appl Magn Reson 43:69–79
    • (2012) Appl Magn Reson , vol.43 , pp. 69-79
    • Lumata, L.1    Merritt, M.E.2    Malloy, C.3    Sherry, A.D.4    Kovacs, Z.5
  • 29
    • 79957981420 scopus 로고    scopus 로고
    • DNP by thermal mixing under optimized conditions yields > 60,000-fold enhancement of 89Y NMR signal
    • COI: 1:CAS:528:DC%2BC3MXmtVWgtrg%3D, PID: 21539398
    • Lumata L, Jindal AK, Merritt ME, Malloy CR, Sherry AD, Kovacs Z (2011) DNP by thermal mixing under optimized conditions yields > 60,000-fold enhancement of 89Y NMR signal. J Am Chem Soc 133:8673–8680
    • (2011) J Am Chem Soc , vol.133 , pp. 8673-8680
    • Lumata, L.1    Jindal, A.K.2    Merritt, M.E.3    Malloy, C.R.4    Sherry, A.D.5    Kovacs, Z.6
  • 30
    • 4043177824 scopus 로고
    • Spin-temperature model of nuclear dynamic polarization using free radicals
    • COI: 1:CAS:528:DyaF1cXktFCiurw%3D
    • Borghini M (1968) Spin-temperature model of nuclear dynamic polarization using free radicals. Phys Rev Lett 20:419–421
    • (1968) Phys Rev Lett , vol.20 , pp. 419-421
    • Borghini, M.1
  • 31
    • 84864346993 scopus 로고    scopus 로고
    • Dynamic nuclear polarization by thermal mixing under partial saturation
    • COI: 1:CAS:528:DC%2BC38XhtVagurbK
    • Jannin S, Comment A, van der Klink JJ (2012) Dynamic nuclear polarization by thermal mixing under partial saturation. Appl Magn Reson 43:59–68
    • (2012) Appl Magn Reson , vol.43 , pp. 59-68
    • Jannin, S.1    Comment, A.2    van der Klink, J.J.3
  • 32
    • 79951888767 scopus 로고    scopus 로고
    • The effect of 13C enrichment in the glassing matrix on dynamic nuclear polarization of [1-13C]pyruvate
    • PID: 21285486
    • Lumata L, Kovacs Z, Malloy C, Sherry AD, Merritt M (2011) The effect of 13C enrichment in the glassing matrix on dynamic nuclear polarization of [1-13C]pyruvate. Phys Med Biol 56:N85–N92
    • (2011) Phys Med Biol , vol.56 , pp. 85-92
    • Lumata, L.1    Kovacs, Z.2    Malloy, C.3    Sherry, A.D.4    Merritt, M.5
  • 34
    • 84885948026 scopus 로고    scopus 로고
    • Automated transfer and injection of hyperpolarized molecules with polarization measurement prior to in vivo NMR
    • COI: 1:CAS:528:DC%2BC3sXhs1GkurnN, PID: 23893539
    • Cheng T, Mishkovsky M, Bastiaansen JAM, Ouari O, Hautle P, Tordo P, van der Brandt B, Comment A (2013) Automated transfer and injection of hyperpolarized molecules with polarization measurement prior to in vivo NMR. NMR Biomed 26:1582–1588
    • (2013) NMR Biomed , vol.26 , pp. 1582-1588
    • Cheng, T.1    Mishkovsky, M.2    Bastiaansen, J.A.M.3    Ouari, O.4    Hautle, P.5    Tordo, P.6    van der Brandt, B.7    Comment, A.8
  • 36
    • 84870055964 scopus 로고    scopus 로고
    • Effect of lanthanide ions on dynamic nuclear polarization enhancement and liquid-state T 1 relaxation
    • COI: 1:CAS:528:DC%2BC38Xhs12rs7nO, PID: 22367680
    • Gordon JW, Fain SB, Rowland IJ (2012) Effect of lanthanide ions on dynamic nuclear polarization enhancement and liquid-state T1 relaxation. Magn Reson Med 68:1949–1952
    • (2012) Magn Reson Med , vol.68 , pp. 1949-1952
    • Gordon, J.W.1    Fain, S.B.2    Rowland, I.J.3
  • 37
    • 84865836093 scopus 로고    scopus 로고
    • Optimisation of dynamic nuclear polarisation of [1-13C] pyruvate by addition of gadolinium-based contrast agents
    • Waldner LF, Chen A, Mander W, Scholl T, McKenzie C (2012) Optimisation of dynamic nuclear polarisation of [1-13C] pyruvate by addition of gadolinium-based contrast agents. J Magn Reson 223:85–89
    • (2012) J Magn Reson , vol.223 , pp. 85-89
    • Waldner, L.F.1    Chen, A.2    Mander, W.3    Scholl, T.4    McKenzie, C.5


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