Mercury speciation in seawater by liquid chromatography-inductively coupled plasma-mass spectrometry following solid phase extraction pre-concentration by using an ionic imprinted polymer based on methyl-mercury-phenobarbital interaction

Journal of Chromatography A

Volumn 1391, Issue 1, 2015, Pages 9-17

  Rodríguez Reino, María Pilar ^a   Rodríguez Fernández, Roi ^a   Peña Vázquez, Elena ^a   Domínguez González, Raquel ^a   Bermejo Barrera, Pilar ^a   Moreda Piñeiro, Antonio ^a  

^a UNIVERSITY OF SANTIAGO DE COMPOSTELA   (Spain)

Author keywords

High performance chromatography; Inductively coupled plasma mass spectrometry; Ionic imprinted polymer; Mercury speciation; Seawater; Solid phase extraction

Indexed keywords

CHELATION; CHROMATOGRAPHY; COMPLEXATION; ETHYLENE; FLOW RATE; HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; INDUCTIVELY COUPLED PLASMA; INDUCTIVELY COUPLED PLASMA MASS SPECTROMETRY; LIGANDS; LIQUID CHROMATOGRAPHY; LIQUIDS; LOADING; MASS SPECTROMETERS; MASS SPECTROMETRY; MERCURY (METAL); MERCURY COMPOUNDS; METHANOL; PHASE SEPARATION; POLYMERS; SEAWATER; SPECTROMETRY; SYNTHESIS (CHEMICAL);

AZOBISISOBUTYRONITRILE; HIGH PERFORMANCE CHROMATOGRAPHIES; IMPRINTED POLYMERS; INDUCTIVELY COUPLED PLASMA MASS SPECTROMETRIES (ICPMS); MERCURY SPECIATIONS; MIXED LIGAND COMPLEXES; PRECIPITATION POLYMERIZATIONS; SOLID-PHASE EXTRACTION;

EXTRACTION;

2,2' AZOBISISOBUTYRONITRILE; ACETONITRILE; BUTYRONITRILE; ETHYLENE GLYCOL DIMETHACRYLATE; ETHYLMERCURY DERIVATIVE; IONIC IMPRINTED POLYMER; MERCAPTOETHANOL; MERCURY; METHACRYLIC ACID; METHANOL; METHYLMERCURY; PHENOBARBITAL; POLYMER; SEA WATER; UNCLASSIFIED DRUG; WATER; AZOBIS(ISOBUTYRONITRILE); CHELATING AGENT; MERCURY DERIVATIVE; METHYLMERCURY DERIVATIVE; NITRILE; POLY(METHYL METHACRYLATE); WATER POLLUTANT;

ADSORPTION; ARTICLE; ELUTION; ENVIRONMENTAL MONITORING; FLOW RATE; HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; LIMIT OF DETECTION; LIMIT OF QUANTITATION; LIQUID CHROMATOGRAPHY; MASS SPECTROMETRY; PH; POLYMERIZATION; PRECIPITATION; PRIORITY JOURNAL; QUANTITATIVE ANALYSIS; SEPARATION TECHNIQUE; SOLID PHASE EXTRACTION; WATER ANALYSIS; WATER QUALITY; WATER SAMPLING; ANALYSIS; CHEMISTRY; MOLECULAR IMPRINTING; PROCEDURES; WATER POLLUTANT;

CHELATING AGENTS; CHROMATOGRAPHY, HIGH PRESSURE LIQUID; ETHYLMERCURY COMPOUNDS; MASS SPECTROMETRY; MERCURY COMPOUNDS; METHYLMERCURY COMPOUNDS; MOLECULAR IMPRINTING; NITRILES; PHENOBARBITAL; POLYMETHYL METHACRYLATE; SEAWATER; SOLID PHASE EXTRACTION; WATER POLLUTANTS, CHEMICAL;

EID: 84933181486     PISSN: 00219673     EISSN: 18733778     Source Type: Journal    
DOI: 10.1016/j.chroma.2015.02.068     Document Type: Article

References (42)

1. WHO Environmental Health Criteria No. 86 - Mercury - Environmental Aspects 1989, World Health Organisation, Geneva.
2. Lamborg C.H., Hammerschmidt C.R., Gill G.A., Mason R.P., Gichuki S. An intercomparison of procedures for the determination of total mercury in seawater and recommendations regarding mercury speciation during GEOTRACES cruises. Limnol. Oceanogr.: Methods 2012, 10:90-100.
3. Mergler D., Anderson H.A., Chan H.M., Mahaffey K.R., Murray M., Sakamoto M., Stern A.H. Methylmercury exposure and health effects in humans: a worldwide concern. Ambio 2007, 36:3-11.
4. Scheuhammer A.M., Meyer M.W., Sandheinrich M.B., Murray M.W. Effects of environmental methylmercury on the health of wild birds, mammals and fish. Ambio 2007, 36:12-18.
5. Directive 2013/39/eu of the European Parliament and of the Council of 12 August 2013. Off. J. Eur. Union 2013, L 226/1-226/17.
6. Moreda-Piñeiro A., Moreda-Piñeiro J., Bermejo-Barrera P. Sample pre-treatment methods for organometallic species determination. Speciation Studies in Soil, Sediments and Environmental Samples 2014, 19-201. CRC, Press, Boca Raton. S. Bakirdere (Ed.).
7. Houserová P., Kubáň P., Kubáň V. Ion exchange preconcentration and separation of mercury species by CE with indirect contactless conductometric detection. Electrophoresis 2006, 27:4508-4515.
8. Cheng H., Wu C., Shen L., Liu J., Xu Z. Online anion exchange column preconcentration and high performance liquid chromatographic separation with inductively coupled plasma mass spectrometry detection for mercury speciation analysis. Anal. Chim. Acta 2014, 828:9-16.
9. Delgado A., Prieto A., Zuloaga O., de Diego A., Madariaga J.M. Production of artifact methylmercury during the analysis of certified reference sediments: use of ionic exchange in the sample treatment step to minimise the problem. Anal. Chim. Acta 2007, 582:109-115.
10. Jia X.-Y., Gong D.-R., Han Y., Wei C., Duan T.-C., Chen H.-T. Fast speciation of mercury in seawater by short-column high-performance liquid chromatography hyphenated to inductively coupled plasma spectrometry after on-line cation exchange column preconcentration. Talanta 2012, 88:724-729.
11. Cairns W.R.L., Ranaldo M., Hennebelle R., Turetta C., Capodaglio G., Ferrari C.F., Dommergue A., Cescon P., Barbante C. Speciation analysis of mercury in seawater from the lagoon of Venice by on-line pre-concentration HPLC-ICP-MS. Anal. Chim. Acta 2008, 622:62-69.
12. Houserová P., Matějíček D., Kubáň V. High-performance liquid chromatographic/ion-trap mass spectrometric speciation of aquatic mercury as its pyrrolidinedithiocarbamate complexes. Anal. Chim. Acta 2007, 596:242-250.
13. Muñoz J., Gallego M., Valcárcel M. Speciation analysis of mercury and tin compounds in water and sediments by gas chromatography-mass spectrometry following preconcentration on C60 fullerene. Anal. Chim. Acta 2005, 548:66-72.
14. Sánchez D.M., Martín R., Morante R., Marín J., Munuera M.L. Preconcentration speciation method for mercury compounds in water samples using solid phase extraction followed by reversed phase high performance liquid chromatography. Talanta 2000, 52:671-679.
15. Margetínová J., Houserová-Pelcová P., Kubáň V. Speciation analysis of mercury in sediments, zoobenthos and river water samples by high-performance liquid chromatography hyphenated to atomic fluorescence spectrometry following preconcentration by solid phase extraction. Anal. Chim. Acta 2008, 615:115-123.
16. Yong-Guang Y., Chen M., Jin-Feng P., Jing-Fu L., Gui-Bin J. Dithizone-functionalized solid phase extraction-displacement elution-high performance liquid chromatography-inductively coupled plasma mass spectrometry for mercury speciation in water samples. Talanta 2010, 81:1788-1792.
17. Hashempur T., Rofouei M.K., Khorrami A.R. Speciation analysis of mercury contaminants in water samples by RP-HPLC after solid phase extraction on modified C18 extraction disks with 1,3-bis(2-cyanobenzene)triazene. Microchem. J. 2008, 89:131-136.
18. dos Santos J.S., de la Guardia M., Pastor A., dos Santos M.L.P. Determination of organic and inorganic mercury species in water and sediment samples by HPLC on-line coupled with ICP-MS. Talanta 2009, 80:207-211.
19. Martin-Esteban A. Molecularly-imprinted polymers as a versatile, highly selective tool in sample preparation. Trends Anal. Chem. 2013, 45:169-181.
20. Chen L., Xu S., Li J. Recent advances in molecular imprinting technology: current status, challenges and highlighted applications. Chem. Soc. Rev. 2011, 40:2922-2942.
21. Rao T.P., Kala R., Daniel S. Metal ion-imprinted polymers - novel materials for selective recognition of inorganics. Anal. Chim. Acta 2006, 578:105-116.
22. Whitcombe M.J., Kirsch N., Nicholls I.A. Molecular imprinting science and technology: a survey of the literature for the years 2004-2011. J. Mol. Recognit. 2014, 27:297-401.
23. Liu Y., Zai Y., Chang X., Guo Y., Meng S., Feng F. Highly selective determination of methylmercury with methylmercury-imprinted polymers. Anal. Chim. Acta 2006, 575:159-165.
24. Xu S., Chen L., Li J., Guan Y., Lu H. Novel Hg2+-imprinted polymers based on thymine-Hg2+-thymine interaction for highly selective preconcentration of Hg2+ in water samples. J. Hazard. Mater. 2012, 237-238(237):347-350.
25. Andaç M., Mirel S., Şenel S., Say R., Ersöz A., Denizli A. Ion-imprinted beads for molecular recognition based mercury removal from human serum. Int. J. Biol. Macromol. 2007, 40:159-166.
26. Dakova I., Karadjova I., Georgieva V., Georgiev G. Ion-imprinted polymethacrylic microbeads as new sorbent for preconcentration and speciation of mercury. Talanta 2009, 78:523-529.
27. Dakova I., Yordanova T., Karadjova I. Non-chromatographic mercury speciation and determination in wine by new core-shell ion-imprinted sorbents. J. Hazard. Mater. 2012, 231-232(231):49-50.
28. Yordanova T., Dakova I., Balashev K., Karadjova I. Polymeric ion-imprinted nanoparticles for mercury speciation in surface waters. Microchem. J. 2014, 113:42-47.
29. Najafi E., Aboufazeli F., Reza H., Zhad L.Z., Sadeghi O., Amani V. A novel magnetic ion imprinted nano-polymer for selective separation and determination of low levels of mercury(II) ions in fish samples. Food Chem. 2013, 141:4040-4045.
30. Güney O., Cebeci F.Ç. Molecularly imprinted fluorescent polymers as chemosensors for the detection of mercury ions in aqueous media. J. Appl. Polym. Sci. 2010, 117:2373-2379.
31. Büyüktiryaki S., Say R., Denizli A., Ersöz A. Mimicking receptor for methylmercury preconcentration based on ion-imprinting. Talanta 2007, 71:699-705.
32. Hu S.G., Wang S.W., He S.W. An amobarbital molecularly imprinted microsphere for selective solid-phase extraction of phenobarbital from human urine and medicines and their determination by high-performance liquid chromatography. Analyst 2003, 128:1485-1489.
33. Chang L.-F., Jiang S.-J., Sahayam A.C. Speciation analysis of mercury and lead in fish samples using liquid chromatography-inductively coupled plasma mass spectrometry. J. Chromatogr. A 2007, 1176:143-148.
34. Castillo A., Roig-Navarro A.F., Pozo O.J. Method optimization for the determination of four mercury species by micro-liquid chromatography-inductively coupled plasma mass spectrometry coupling in environmental water samples. Anal. Chim. Acta 2006, 577:18-25.
35. Jia X., Han Y., Liu X., Duan T., Chen H. Speciation of mercury in water samples by dispersive liquid-liquid microextraction combined with high performance liquid chromatography-inductively coupled plasma mass spectrometry. Spectrochim. Acta B 2011, 66:88-92.
36. Ibáñez-Palomino C., López-Sánchez J.F., Sahuquillo À. Inorganic mercury and methylmercury determination in polluted waters by HPLC coupled to cold vapour atomic fluorescence spectroscopy. Int. J. Environ. Anal. Chem. 2012, 92:909-921.
37. Bermejo-Barrera P., Moreda-Piñeiro J., Moreda-Piñeiro A., Bermejo-Barrera A. Usefulness of the chemical modification and the multi-injection technique approaches in the electrothermal atomic absorption spectrometric determination of silver, arsenic, cadmium, chromium, mercury, nickel and lead in sea-water. J. Anal. At. Spectrom. 1998, 13:777-786.
38. Otero-Romaní J., Moreda-Piñeiro A., Bermejo-Barrera P., Martin-Esteban A. Synthesis, characterization and evaluation of ionic-imprinted polymers for solid-phase extraction of nickel from seawater. Anal. Chim. Acta 2008, 630:1-9.
39. Otero-Romaní J., Moreda-Piñeiro A., Bermejo-Barrera P., Martin-Esteban A. Inductively coupled plasma-optical emission spectrometry/mass spectrometry for the determination of Cu, Ni, Pb and Zn in seawater after ionic imprinted polymer based solid phase extraction. Talanta 2009, 79:723-729.
40. Otero-Romaní J., Moreda-Piñeiro A., Bermejo-Barrera P., Martin-Esteban A. Ionic imprinted polymer for nickel recognition by using the bi-functionalized 5-vinyl-8-hydroxyquinoline as a monomer: application as a new solid phase extraction support. Microchem. J. 2009, 93:225-231.
41. Chen X., Han C., Cheng H., Wang Y., Liu J., Xua Z., Hu L. Rapid speciation analysis of mercury in seawater and marine fish by cation exchange chromatography hyphenated with inductively coupled plasma mass spectrometry. J. Chromatogr. A 2013, 1314:86-93.
42. DRAFT Total and Dissolved Mercury in Water by Bromine Monochloride Digestion - PBM 2013, Available at http://www.elp.gov.bc.ca/epd/wamr/labsys/pdf/Draft_Hg_Water_22Feb2013.pdf (accessed 16.05.14).